Ultrafine-grained(UFG) high purity aluminum exhibits a variety of attractive mechanical properties and special deformation behavior. Equal channel angular pressing(ECAP) process can be used to easily and effectively r...Ultrafine-grained(UFG) high purity aluminum exhibits a variety of attractive mechanical properties and special deformation behavior. Equal channel angular pressing(ECAP) process can be used to easily and effectively refine metals. The microstructure and microtexture evolutions and grain boundary characteristics of the high purity aluminum(99.998%) processed by ECAP at room temperature are investigated by means of TEM and EBSD. The results indicate that the shear deformation resistance increases with repeated EACP passes, and equiaxed grains with an average size of 0.9 μm in diameter are formed after five passes. Although the orientations distribution of grains tends to evolve toward random orientations, and microtextures(80°, 35°, 0°),(40°, 75°, 45°) and(0°, 85°, 45°) peak in the sample after five passes. The grain boundaries in UFG aluminum are high-angle geometrically necessary boundaries. It is suggested that the continuous dynamic recrystallization is responsible for the formation of ultrafine grains in high purity aluminum. Microstructure evolution in the high purity aluminum during ECAP is proposed.展开更多
基金Project(12JJ2028)supported by the Hunan Provincial Natural Science Foundation of ChinaProject(201308430093)supported by the China Scholarship CouncilProjects(201012200006,2013zzts185,2012zzts066)supported by the Freedom Explore Program of Central South University,China
文摘Ultrafine-grained(UFG) high purity aluminum exhibits a variety of attractive mechanical properties and special deformation behavior. Equal channel angular pressing(ECAP) process can be used to easily and effectively refine metals. The microstructure and microtexture evolutions and grain boundary characteristics of the high purity aluminum(99.998%) processed by ECAP at room temperature are investigated by means of TEM and EBSD. The results indicate that the shear deformation resistance increases with repeated EACP passes, and equiaxed grains with an average size of 0.9 μm in diameter are formed after five passes. Although the orientations distribution of grains tends to evolve toward random orientations, and microtextures(80°, 35°, 0°),(40°, 75°, 45°) and(0°, 85°, 45°) peak in the sample after five passes. The grain boundaries in UFG aluminum are high-angle geometrically necessary boundaries. It is suggested that the continuous dynamic recrystallization is responsible for the formation of ultrafine grains in high purity aluminum. Microstructure evolution in the high purity aluminum during ECAP is proposed.