We report the growth of high quality Fe excess and Co doped,FeTxSe single crystals in nominal ratio via slow cooling method of high temperature solution growth technique and,their structural and physical properties th...We report the growth of high quality Fe excess and Co doped,FeTxSe single crystals in nominal ratio via slow cooling method of high temperature solution growth technique and,their structural and physical properties through the X‐ray diffraction,Raman spectroscopy,magnetic and transports measurements.Selective area electron diffraction(SAED)patterns and X‐ray diffraction of cleavage piece confirm the growth of single crystals in(h0l)orientations.Observations of phonon vibration modes(A_(1g) and B_(1g))in Raman spectroscopy measurements mark the qualitative analysis of these single crystals.Low temperature magnetic and electrical transport studies manifest the superconducting nature of both single crystals.展开更多
基金support through the project No.F.30‐303/2016(BSR).
文摘We report the growth of high quality Fe excess and Co doped,FeTxSe single crystals in nominal ratio via slow cooling method of high temperature solution growth technique and,their structural and physical properties through the X‐ray diffraction,Raman spectroscopy,magnetic and transports measurements.Selective area electron diffraction(SAED)patterns and X‐ray diffraction of cleavage piece confirm the growth of single crystals in(h0l)orientations.Observations of phonon vibration modes(A_(1g) and B_(1g))in Raman spectroscopy measurements mark the qualitative analysis of these single crystals.Low temperature magnetic and electrical transport studies manifest the superconducting nature of both single crystals.
