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Microstructural evolution and superelastic properties of ultrafine-graine d NiTi-base d shape memory alloy via sintering of amorphous ribbon precursor 被引量:2
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作者 w.s.cai H.Z.Lu +4 位作者 H.Z.Li Z.Liu H.B.Ke W.H.Wang C.Yang 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2023年第7期80-92,共13页
NiTi-based shape memory alloys(SMAs)are considered as cutting-edge intelligent functional materials.However,it remains a great challenge to obtain ultrafine-grained(UFGed)bulk materials with mm-scale size as well as o... NiTi-based shape memory alloys(SMAs)are considered as cutting-edge intelligent functional materials.However,it remains a great challenge to obtain ultrafine-grained(UFGed)bulk materials with mm-scale size as well as outstanding superelastic properties.Here,UFGed bulk Ti_(35)Zr_(15)Ni_(35)Cu_(15)NiTi-based SMA is successfully prepared via spark plasma sintering of amorphous ribbon precursor at different sintering temperatures,and microstructural evolution and superelastic properties are symmetrically investigated.It is found that its grain size ranges from UFG to micro-grain with increased sintering temperature regard-less of the predominant B2 matrix in all bulk samples.Interestingly,the orientation relationships between B2 matrix and nano-scale fcc(Ti,Zr)_(2)Ni precipitate evolve from coherent to incoherent.Consequently,the UFGed samples exhibit perfect superelasticity with the high recoverable strain of∼5.8%,the stable recov-ery rate above 99%,and the great critical stress inducing martensitic transformation higher than 1 GPa,far superior to the corresponding ones of suction-cast micro-grained TiZrNiCu SMAs.Fundamentally,the perfect superelasticity is attributed to the good resistance to dislocation slip or grain boundary slip by residual nano-scale amorphous phase or secondary phase of coherent and semi-coherent fcc(Ti,Zr)_(2)Ni precipitate.In addition,the gentle superelastic plateau is associated to the favorable transfer stress and the strong ability to accommodate dislocation movement,which is generated by the coherent interface between nano-scale fcc(Ti,Zr)_(2)Ni and UFGed B2 matrix.These results suggest that spark plasma sintering of amorphous alloy precursor is a feasible route to obtaining excellent superelasticity in NiTi-based SMAs. 展开更多
关键词 Shape memory alloy Amorphous alloy Microstructure SUPERELASTICITY
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