C_(60) single crystals grown by a single-temperature-gradient technique were characterized by synchrotron radiation white beam x-ray topography and x-ray double crystal diffraction with Cu K_(α1) radiation on convent...C_(60) single crystals grown by a single-temperature-gradient technique were characterized by synchrotron radiation white beam x-ray topography and x-ray double crystal diffraction with Cu K_(α1) radiation on conventional x-ray source.The results show that the crystal is rather well crystallized.The x-ray topographies give an evidence of dendritic growth mechanism of C_(60) single crystal,and x-ray double crystal diffraction rocking curve shows that there are mosaic structural defects in the sample.A phase transition at 249±1.5K from a simple cubic to a face centered cubic structure is confirmed by in situ observation of synchrotron radiation white beam x-ray topography with the temperature varing from 230 to 295K.展开更多
基金Supported by BSRFBEPCthe Chinese National Committee of Science and Technology。
文摘C_(60) single crystals grown by a single-temperature-gradient technique were characterized by synchrotron radiation white beam x-ray topography and x-ray double crystal diffraction with Cu K_(α1) radiation on conventional x-ray source.The results show that the crystal is rather well crystallized.The x-ray topographies give an evidence of dendritic growth mechanism of C_(60) single crystal,and x-ray double crystal diffraction rocking curve shows that there are mosaic structural defects in the sample.A phase transition at 249±1.5K from a simple cubic to a face centered cubic structure is confirmed by in situ observation of synchrotron radiation white beam x-ray topography with the temperature varing from 230 to 295K.
