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均匀化前预处理对7150铝合金中Al_3Zr相析出及再结晶的影响 被引量:6
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作者 郭占英 丛福官 +2 位作者 赵刚 x.-grant chen 田妮 《轻合金加工技术》 CAS 北大核心 2016年第2期21-27,共7页
用透射电子显微镜(TEM)及电子背散射(EBSD)技术,研究了均匀化前进行250℃~400℃预处理对7150铝合金中Al3Zr相析出行为及变形后固溶处理过程再结晶抗力的影响。结果表明,7150铝合金是否进行均匀化前预处理,其经470℃24 h的均匀化后... 用透射电子显微镜(TEM)及电子背散射(EBSD)技术,研究了均匀化前进行250℃~400℃预处理对7150铝合金中Al3Zr相析出行为及变形后固溶处理过程再结晶抗力的影响。结果表明,7150铝合金是否进行均匀化前预处理,其经470℃24 h的均匀化后其合金中Al3Zr析出相与Al基体均为共格关系。随均匀化前预处理温度降低,Al3Zr析出相的尺寸变小、密度提高;在250℃预处理,随预处理时间延长,最终Al3Zr析出相的尺寸变小、密度提高;当预处理温度超过300℃时,随预处理时间延长,Al3Zr析出相的尺寸变大、密度降低,但预处理时间超过24 h后其影响不明显。7150铝合金铸锭经470℃均匀化前预处理能显著提高其变形后再结晶抗力,经470℃2h固溶处理后,其组织为未再结晶的回复组织;而直接经470℃均匀化处理后的变形样品经470℃2h固溶处理后,其组织为部分再结晶组织。 展开更多
关键词 7150铝合金 均匀化 Al3Zr弥散相 高分辨TEM 再结晶
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均匀化前预处理对Al-Zn-Mg-Cu合金中含V相析出及再结晶的影响
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作者 郭占英 丛福官 +2 位作者 赵刚 x.-grant chen 田妮 《轻合金加工技术》 CAS 北大核心 2016年第3期24-30,42,共8页
用透射电子显微镜(TEM)及扫描电镜电子背散射(EBSD)技术,研究了均匀化前250℃~400℃的预处理对w(V)=0.11%的超高强Al-Zn-Mg-Cu合金中Al21V2弥散相析出行为及变形后再结晶抗力的影响,并计算了V在铝基体中的扩散常数和扩散距离。结... 用透射电子显微镜(TEM)及扫描电镜电子背散射(EBSD)技术,研究了均匀化前250℃~400℃的预处理对w(V)=0.11%的超高强Al-Zn-Mg-Cu合金中Al21V2弥散相析出行为及变形后再结晶抗力的影响,并计算了V在铝基体中的扩散常数和扩散距离。结果表明,铸锭均匀化处理过程形成Al21V2弥散相,并在晶界附近形成明显的无析出区,其宽度基本不受均匀化处理前预处理的影响;在普通均匀化处理前预处理能明显提高Al21V2弥散相的密度、减小其尺寸;在铝基体中,V在300℃及400℃的扩散常数分别为9.81×10-31m2/s、5.32×10-24m2/s。在300℃预处理合金能获得尺寸最小、密度最高的Al21V2弥散相,而且其热变形后再结晶抗力最大。 展开更多
关键词 超高强Al-Zn-Mg-Cu合金 均匀化 Al21V2相 弥散相 再结晶
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Improvement of elevated-temperature strength and recrystallization resistance via Mn-containing dispersoid strengthening in Al-Mg-Si 6082 alloys 被引量:7
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作者 chen Li Kun Liu x.-grant chen 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2020年第4期135-143,共9页
The precipitation behavior of Mn-containing dispersoids in Al-Mg-Si 6082 alloys with different Mn contents(0,0.5 and 1.0 wt%)during various heat treatments(300–500℃)was investigated.The effects of dispersoids on ele... The precipitation behavior of Mn-containing dispersoids in Al-Mg-Si 6082 alloys with different Mn contents(0,0.5 and 1.0 wt%)during various heat treatments(300–500℃)was investigated.The effects of dispersoids on elevated-temperature strength and recrystallization resistance during hot-rolling and post-rolling annealing were evaluated.The results showed that the dispersoids in the Mn-containing alloys(0.5 and 1.0%)began to precipitate at 350℃and reached the optimum conditions after 2–4 h at 400℃.However,the dispersoids coarsened with increasing holding time at temperatures above450℃.After the peak precipitation treatment at 400℃for 2 h,the yield strength at 300℃increased from 28 MPa(base alloy free of Mn)to 55 MPa(alloy with 0.5%Mn)and 70 MPa(alloy with 1%Mn),respectively,demonstrating a significant dispersoid strengthening effect at elevated temperature.In addition,the dispersoids were thermally stable at 300℃for up to 1000 h holding owing to its relative high precipitation temperature(350–400℃),leading to the superior constant mechanical performance at elevated temperature during the long service life.During hot rolling and post-rolling annealing,the presence of a large amount of dispersoids results in the higher Zener drag PZcompared with base alloy and then significantly improved the recrystallization resistance.The alloy containing 0.5%Mn exhibited the highest recrystallization resistance among three experimental alloys studied during the post-rolling process,likely resulted from the lower coarsening rate of dispersoids and the lower dispersoids free zone. 展开更多
关键词 AL-MG-SI 6082 alloy Mn addition DISPERSOID precipitation ELEVATED-TEMPERATURE STRENGTH RECRYSTALLIZATION RESISTANCE
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Effects of Mn content on recrystallization resistance of AA6082 aluminum alloys during post-deformation annealing 被引量:6
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作者 xiaoming Qian Nick Parson x.-grant chen 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2020年第17期189-197,共9页
The microstructural evolutions under as-homogenized and as-deformed conditions and after the postdeformation annealing of AA6082 aluminum alloys with different Mn content(0.05 wt.%-1 wt.%)were studied by optical,scann... The microstructural evolutions under as-homogenized and as-deformed conditions and after the postdeformation annealing of AA6082 aluminum alloys with different Mn content(0.05 wt.%-1 wt.%)were studied by optical,scanning electron,and transmission electron microscopies.The results showed that the presence of a large amount ofα-Al(Mn,Fe)Si dispersoids induced by Mn addition significantly improved the recrystallization resistance.In the base alloy free of Mn,static recrystallization occurred after 2 h of annealing,and grain growth commenced after 4 h of annealing,whereas in Mn-containing alloys,the recovered grain structure was well-retained after even 8 h of annealing.The alloy with 0.5%Mn exhibited the best recrystallization resistance,and a further increase of the Mn levels to 1%resulted in a gradual reduction of the recrystallization resistance,the reason for which was that recrystallization occurred only in the dispersoid-free zones(DFZs)and the increased DFZ fraction with Mn content led to an increase in the recrystallization fraction.The variation in the dispersoid number density and a coarsening of dispersoids during annealing have a limited influence on the static recrystallization in Mn-containing alloys. 展开更多
关键词 AA6082 alloys Mn effects Recrystallization resistance Dispersoid precipitation Post-deformation annealing
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