TEMPERATURE EFFECT ON LOW-CYCLE FATIGUE BEHAVIOR OF NICKEL-BASED SINGLE CRYSTALLINE SUPERALLOY

The low-cycle fatigue （LCF） behavior of a nickel-based single crystal superalloy with [001] orientation was studied at an intermediate temperature of T0℃ and a higher temperature of To ＋ 250℃ under a constant low strain rate of 10^-3 s^-1 in ambient atmosphere. The superalloy exhibited cyclic tension-compression asymmetry which is dependent on the temperature and applied strain amplitude. Analysis on the fracture surfaces showed that the surface and subsurface casting micropores were the major crack initiation sites. Interior Ta-rich carbides were frequently observed in all specimens. Two distinct types of fracture were suggested by fractogaphy. One type was characterized by Mode-I cracking with a microscopically rough surface at To ＋ 250℃. Whereas the other type at lower temperature T0℃ favored either one or several of the octahedral {111} planes, in contrast to the normal Mode-I growth mode typically observed at low loading frequencies （several Hz）. The failure mechanisms for two cracking modes are shearing of γ＇ precipitates together with the matrix at T0℃ and cracking confined in the matrix and the γ/γ＇interface at To - 250℃.

Citron C-05 inhibits both the penetration and colonization of Xanthomonas citri subsp.citri to achieve resistance to citrus canker disease

Citrus canker,caused by Xanthomonas citri subsp.citri(Xcc),is a serious bacterial disease that affects citrus production worldwide.Citron C-05(Citrus medica)is the only germplasm in the Citrus genus that has been identified to exhibit strong resistance to Xcc.However,it has not been determined when,where,and how Xcc is restricted in the tissues of Citron C-05 during the infection process.In the present study,we investigated the spatiotemporal growth dynamics of an eGFP-labeled virulent Xcc(eGFP-Xcc)strain in Citron C-05 along with five susceptible biotypes(i.e.,lemon,pummelo,sour orange,sweet orange,and ponkan mandarin)upon inoculation via the spraying or leaf infiltration of a bacterial suspension.The results from extensive confocal laser scanning microscopy analyses showed that while Xcc grew rapidly in plants of all five susceptible genotypes,Xcc was severely restricted in the epidermal and mesophyll cell layers of the leaves of Citron C-05 in the early stage of infection.Not surprisingly,resistance against Xcc in Citron C-05 was found to be associated with the production of reactive oxygen species and hypersensitive response-like cell death,as well as greater upregulation of several defense-related genes,including a pathogenesis-related gene(PR1)and a glutathione S-transferase gene(GST1),compared with sweet orange as a susceptible control.Taken together,our results not only provide further valuable details of the spatiotemporal dynamics of the host entry,propagation,and spread of Xcc in both resistant and susceptible citrus plants but also suggest that resistance to Xcc in Citron C-05 may be attributed to the activation of multiple defense mechanisms.

Microstructure evolution of T91 steel after heavy ion irradiation at 550℃

Fe-Cr ferritic/martensitic(F/M)steels have been proposed as one of the candidate materials for the Generation IV nuclear technologies.In this study,a widely-used ferritic/martensitic steel,T91 steel,was irradiated by 196-MeV Kr^(+)ions at 550℃.To reveal the irradiation mechanism,the microstructure evolution of irradiated T91 steel was studied in details by transmission electron microscope(TEM).With increasing dose,the defects gradually changed from black dots to dislocation loops,and further to form dislocation walls near grain boundaries due to the production of a large number of dislocations.When many dislocation loops of primary a0/2<111>type with high migration interacted with other defects or carbon atoms,it led to the production of dislocation segments and other dislocation loops of a0<100>type.Lots of defects accumulated near grain boundaries in the irradiated area,especially in the high-dose area.The grain boundaries of martensite laths acted as important sinks of irradiation defects in T91.Elevated temperature facilitated the migration of defects,leading to the accumulation of defects near the grain boundaries of martensite laths.

Numerical study on the seismic response of the underground subway station-surrounding soil mass-ground adjacent building system

Ground buildings constructed above metro station have increased very quickly due to the limited land resources in urban areas. In this paper, the seismic response of the Underground subway station-Surrounding soil mass- Ground adjacent buildings （USG） system subjected to various seismic loading is studied through numerical analysis. The numerical model is established in terms of the calculation domain, boundary condition, and contact property between soil and structure based on the real project. The reciprocal influence between subway station and ground adjacent building, and their effects on the dynamic characteristics of surrounding soil mass are also investigated. Through the numerical study, it is found that the impact of underground structure on the dynamic characteristics of the surrounding soil mass depends on its own dimension, and the presence of underground structure has certain impact on the seismic response of ground adjacent building. Due to the presence of underground structure and ground adjacent building, the vertical acceleration generated by the USG system cannot be ignored. The outcomes of this study can provide references for seismic design of structures in the USG system.

Novel hard materials with controlled (W_(0.5)Al_(0.5))C grain shapes: in-situ high pressure preparation and mechanical properties

A novel hard material with various （W0.5Al0.5）C grain shapes was successfully prepared through mechanical alloying and in-situ high-pressure sintering process. X-ray diffraction apparatus and scanning electron microscopy were used to characterize the phase and the microstructures of the samples. The novel hard materials with ＂fibrous＂, ＂rounded＂ and ＂plate-like＂ grains, which do not contain sharp edges, have the improved mechanical properties. The bulk boundless （W0.5Al0.5）C hard material with various （W0.5Al0.5）C grain shapes possesses good mechanical properties and light weight. The formation mechanism for the non-equilibrium （W0.5Al0.5）C grains during in-situ high-pressure sintering is also discussed.

Review of Hydrogen Embrittlement in Metals: Hydrogen Diffusion, Hydrogen Characterization, Hydrogen Embrittlement Mechanism and Prevention

Hydrogen dissolved in metals as a result of internal and external hydrogen can affect the mechanical properties of the metals, principally through the interactions between hydrogen and material defects. Multiple phenomena such as hydrogen dissolution, hydrogen diffusion, hydrogen redistribution and hydrogen interactions with vacancies, dislocations, grain boundaries and other phase interfaces are involved in this process. Consequently, several hydrogen embrittlement(HE) mechanisms have been successively proposed to explain the HE phenomena, with the hydrogen-enhanced decohesion mechanism, hydrogenenhanced localized plasticity mechanism and hydrogen-enhanced strain-induced vacancies being some of the most important. Additionally, to reduce the risk of HE for engineering structural materials in service, surface treatments and microstructural optimization of the alloys have been suggested. In this review, we report on the progress of the studies on HE in metals, with a particular focus on steels. It focuses on four aspects:(1) hydrogen diffusion behavior;(2) hydrogen characterization methods;(3) HE mechanisms;and(4) the prevention of HE. The strengths and weaknesses of the current HE mechanisms and HE prevention methods are discussed, and specific research directions for further investigation of fundamental HE mechanisms and methods for preventing HE failure are identified.

Ground movements due to deep excavations in Shanghai： Design charts

Recent research has clarified the sequence of ground deformation mechanisms that manifest themselves when excavations are made in soft ground. Furthermore, a new framework to describe the deformability of clays in the working stress range has been devised using a large database of previously published soil tests. This paper aims to capitalize on these advances, by analyzing an expanded database of ground movements associated with braced excavations in Shanghai. It is shown that conventional design charts fail to take account either of the characteristics of soil deformability or the relevant deformation mechanisms, and therefore introduce significant scatter. A new method of presentation is found which provides a set of design charts that clarify the influence of soil deformability, wall stiffness, and the geometry of the excavation in relation to the depth of soft ground.

In-situ observation and finite element analysis of fretting fatigue crack propagation behavior in 1045 steel

In this paper fretting fatigue crack behavior in 1045 steel is studied by in-situ observation and finite element analysis.in-situ fretting fatigue experiments are conducted to capture real-time fretting fatigue crack formation and propagation process.The fretting fatigue tests under different load conditions are carried out,then the lifetime and fracture surface are obtained.The crack propagation rates under different loading conditions are measured by in-situ observations.With in-situ observation,crack initiation location and direction are analyzed.Finite element model is used to calculate J-integral which then is applied to fitting with experimental crack growth rate,and establishing crack growth rate model.From fitted S-N curve,it turns out that smaller load ratio leads to higher lifetime.Crack initiates slightly below the point equivalent to line contact of the contact surface in different test conditions,and crack direction shows no obvious relationship with load parameters.The established crack growth rate model well agrees with the test results.

Simultaneous enhancement of strength and ductility in friction stir processed 2205 duplex stainless steel with a bimodal structure:experiments and crystal plasticity modeling

Achieving excellent strength-ductility synergy is a long-lasting research theme for structural materials.However,attempts to enhance strength usually induce a loss of ductility,i.e.,the strength-ductility trade-off.In the present study,the strength-ductility trade-off in duplex stainless steel(DSS)was overcome by developing a bimodal structure using friction stir processing(FSP).The ultimate tensile strength and elongation were improved by 140%and 109%,respectively,compared with those of the asreceived materials.Plastic deformation and concurrent dynamic recrystallization(DRX)during FSP were responsible for the formation of bimodal structure.Incompatible deformation resulted in the accumulation of dislocations at the phase boundaries,which triggered interpenetrating nucleation between the austenite and ferrite phases during DRX,leading to a bimodal structure.The in situ mechanical responses of the bimodal structure during tensile deformation were investigated by crystal plasticity finite element modeling(CPFEM).The stress field distribution obtained from CPFEM revealed that the simultaneous enhancement of strength and ductility in a bimodal structure could be attributed to the formation of a unique dispersion-strengthened system with the austenite and ferrite phases.It is indicated that the present design of alternating fine austenite and coarse ferrite layers is a promising strategy for optimizing the mechanical properties of DSSs.