A high-speed counter-current chromatography(HSCCC)method was successfully developed for the preparative separation and purification of deoxyschizandrin from Schisandrae Sphenantherae Fructus in one step.The purity of ...A high-speed counter-current chromatography(HSCCC)method was successfully developed for the preparative separation and purification of deoxyschizandrin from Schisandrae Sphenantherae Fructus in one step.The purity of deoxyschizandrin was 98.5%,and the structure was identified by MS,UV and NMR.This method was simple,fast,convenient and appropriate to prepare pure compound as reference substances for related research on Schisandrae Sphenantherae Fructus.展开更多
基金supported by the International Scientific and Technological Cooperation Program of China(No.2009DFA31230)the Industry-University-Research Cooperation Program from Science and Technology Department of Guangdong Province(No.2010B090400533)
文摘A high-speed counter-current chromatography(HSCCC)method was successfully developed for the preparative separation and purification of deoxyschizandrin from Schisandrae Sphenantherae Fructus in one step.The purity of deoxyschizandrin was 98.5%,and the structure was identified by MS,UV and NMR.This method was simple,fast,convenient and appropriate to prepare pure compound as reference substances for related research on Schisandrae Sphenantherae Fructus.
