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氧气和硫化钠对赤铜矿浮选的影响及作用机理 被引量:2
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作者 贾晓东 宋凯伟 +5 位作者 蔡锦鹏 苏超 徐晓会 马印禹 申培伦 刘殿文 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2023年第4期1233-1243,共11页
通过浮选试验、场发射扫描电子显微镜(FESEM)、电子探针(EPMA)以及X射线光电子能谱(XPS)等研究氧气和硫化钠对赤铜矿浮选的影响。浮选试验表明,用适量的硫化钠预处理赤铜矿表面后可大幅提升赤铜矿的可浮性。FESEM显示硫化后的赤铜矿表... 通过浮选试验、场发射扫描电子显微镜(FESEM)、电子探针(EPMA)以及X射线光电子能谱(XPS)等研究氧气和硫化钠对赤铜矿浮选的影响。浮选试验表明,用适量的硫化钠预处理赤铜矿表面后可大幅提升赤铜矿的可浮性。FESEM显示硫化后的赤铜矿表面覆盖有大量碎片,在Na_(2)S浓度为5.0×10^(−4)mol/L时,这些碎片的形状更加规则和完整。结合EPMA和EDS分析发现,这些碎片是新形成的铜硫化物,是促进赤铜矿高效浮选的关键。XPS分析表明,赤铜矿暴露于空气中表面极易被氧化成CuO,硫化钠优先与表面的CuO膜发生氧化还原反应,此过程中,Cu^(2+)被还原为Cu^(+),S^(2-)主要被氧化为(S_(2))^(2-)和(S_(n))^(2−)。 展开更多
关键词 赤铜矿 硫化浮选 硫化机理 氧化 硫化铜
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Increased Prevalence of Thyroid Nodules Across Nearly 10 Years in Shanghai,China 被引量:1
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作者 Meng-ying QU Wei TANG +6 位作者 Xue-ying CUI Yu-xiang JIN Zheng-yuan WANG Chang-yi GUO xiao-dong jia Yong-quan SHI jia-jie ZANG 《Current Medical Science》 SCIE CAS 2023年第1期191-197,共7页
Objective This study aimed to determine whether the prevalence of thyroid nodules(TNs)increased due to modern lifestyles or other factors,despite the advances in screening and diagnostic tools.Methods This study inclu... Objective This study aimed to determine whether the prevalence of thyroid nodules(TNs)increased due to modern lifestyles or other factors,despite the advances in screening and diagnostic tools.Methods This study included 3474 pairs of participants,who were matched by gender and age(±3 years)from two cross-sectional sampling surveys:(1)the program on the iodine nutritional status and related health status of residents in Shanghai in 2009;(2)the thyroid disease screening program for adults in Shanghai between 2017 and 2018.The prevalence of TNs and thyroid diseases in 2009 and 2017–2018 were compared,and the potential risk factors of TNs were detected.Results The prevalence of TNs in 2009 was 28.9%:22.5%in males and 34.5%in females.In 2017,this increased to 43.8%:37.9%in males and 49.1%in females.The prevalence of TNs significantly increased from 2009 to 2017(odds ratio,1.486;95%confidence interval,1.238–1.786).In addition,female gender,thyroid disease history,and age were the main risk factors for TNs after adjusting for confounders in the logistic regression across the time period.Conclusion The prevalence of TNs significantly increased across nearly 10 years in Shanghai. 展开更多
关键词 thyroid nodules PREVALENCE period difference detection technology thyroid disease
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Effect of thermal deformation parameters on the microstructure, texture, and microhardness of 5754 aluminum alloy 被引量:4
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作者 Chang-qing Huang jia-xing Liu xiao-dong jia 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2019年第9期1140-1150,共11页
The evolution of the microstructure, texture, and microhardness of 5754 aluminum alloy subjected to high-temperature plastic deformation under different deformation conditions was studied on the basis of thermal simul... The evolution of the microstructure, texture, and microhardness of 5754 aluminum alloy subjected to high-temperature plastic deformation under different deformation conditions was studied on the basis of thermal simulations and electron-backscattered diffraction and Vickers microhardness experiments. The results of a misorientation angle study show that an increase in the deformation temperature and strain rate promoted the transformation of low-angle grain boundaries to high-angle grain boundaries, which contributed to dynamic recrystallization. The effect of the deformation parameters on the texture and its evolution during the recrystallization process was explored on the basis of the orientation distribution function. The results demonstrate that the deformed samples mainly exhibited the features of type A, B, and B textures. The formation and growth of the recrystallized grains clearly affected the texture evolution. The microhardness results show that the variation of the microhardness was closely related to the temperature, strain rate, and dynamic recrystallization. 展开更多
关键词 MICROSTRUCTURE TEXTURE MISORIENTATION dynamic RECRYSTALLIZATION MICROHARDNESS
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Triphenylphosphine-m-sulfonate/carbon tetrabromide as an easily recoverable catalyst system for the efficient synthesis of xanthene and xanthenone derivatives under solvent-free conditions
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作者 Cong-De Huo Xia-Zhen Bao +3 位作者 Dong-Cheng Hu xiao-dong jia Chou-Gu Sun Cheng Wang 《Chinese Chemical Letters》 SCIE CAS CSCD 2014年第5期699-701,共3页
A solid complex,readily prepared from commercially available sodium triphenylphosphine-m-sulfonate(TPPMS) and carbon tetrabromide,can be used as an easily recoverable and reusable catalyst system for one-pot condens... A solid complex,readily prepared from commercially available sodium triphenylphosphine-m-sulfonate(TPPMS) and carbon tetrabromide,can be used as an easily recoverable and reusable catalyst system for one-pot condensation of 2-naphthol with aldehydes to construct 14-aryl(alkyl)-14H-dibenzo[a j]-xanthene derivatives and one-pot condensation of 2-naphthol with aldehydes and cyclic 1 3-dicarbonyl compounds to construct 12-aryl(alkyl)-8 9 10 12-tetrahydrobenzo[a]xanthen-11-one derivatives. 展开更多
关键词 Xanthene Xanthenone Naphthol Aldehyde
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