In this paper,radiate MgO whiskers were fabricated in the system of Mg-B-NaCl-Ar at relatively low temperature. The Mg vapor reacted with trace O_2 contained in the reaction system and formed MgO vapor.On appropriate ...In this paper,radiate MgO whiskers were fabricated in the system of Mg-B-NaCl-Ar at relatively low temperature. The Mg vapor reacted with trace O_2 contained in the reaction system and formed MgO vapor.On appropriate conditions,the MgO vapor could reach supersaturation and grow into highly radiate structure.They were characterized by means of field emission scanning electronic microscopy (FE-SEM),transmission electronic microscopy (TEM) and energy dispersive spectrometer (EDS).The mechanism of the morphologies of MgO was discussed.展开更多
An optical fiber dual Fabry-Perot interferometric carbon monoxide gas sensor based on PANI/Co3 O4/GO(PCG)sensing membrane coated on the end face of the optical fiber is proposed and fabricated.One end face of photonic...An optical fiber dual Fabry-Perot interferometric carbon monoxide gas sensor based on PANI/Co3 O4/GO(PCG)sensing membrane coated on the end face of the optical fiber is proposed and fabricated.One end face of photonic crystal fiber(PCF)without cut-off wavelength is fused with a single-mode fiber(SMF),and the other end face of the PCF is coated with PCG sensing membrane.The collapsed layer formed during the air hole fusion of PCF is used as the first reflector,the interface between PCF and sensing membrane is used as the second reflector,and the interface between the sensing membrane and the air is used as the third reflector,thus the dual Fabry-Pe rot structure sensor is formed.The results show that the sensor has excellent sensitivity and selectivity to carbon monoxide.With the increasing concentration of carbon monoxide gas in the range of 0-60 ppm,the intensity of interference spectrum decreases.The sensitivity of the sensor is 0.3473 dB m/ppm,and its linearity is good.The response time and recovery time are 68 s and 106 s,respectively.The sensor has the advantages of the compact size,low cost,high sensitivity,strong selectivity and simple structure.It is suitable for the sensing detection of low concentration carbon monoxide gas.展开更多
文摘In this paper,radiate MgO whiskers were fabricated in the system of Mg-B-NaCl-Ar at relatively low temperature. The Mg vapor reacted with trace O_2 contained in the reaction system and formed MgO vapor.On appropriate conditions,the MgO vapor could reach supersaturation and grow into highly radiate structure.They were characterized by means of field emission scanning electronic microscopy (FE-SEM),transmission electronic microscopy (TEM) and energy dispersive spectrometer (EDS).The mechanism of the morphologies of MgO was discussed.
基金supported by the National Natural Science Foundation of China(No.51574054)the University Innovation Team Building Program of Chongqing(No.CXTDX201601030)+2 种基金Scientific and Technological Research Program of Chongqing Municipal Education Commission(No.KJZD-M201901102)Chongqing Science and Technology Bureau(Nos.cstc2017shmsA20017,cstc2018jcyjAX0294,CSTCCXLJRC 201905)the Innovation Leader Project of Chongqing Science and Technology Bureau(No.CSTCCXLJRC201905)。
文摘An optical fiber dual Fabry-Perot interferometric carbon monoxide gas sensor based on PANI/Co3 O4/GO(PCG)sensing membrane coated on the end face of the optical fiber is proposed and fabricated.One end face of photonic crystal fiber(PCF)without cut-off wavelength is fused with a single-mode fiber(SMF),and the other end face of the PCF is coated with PCG sensing membrane.The collapsed layer formed during the air hole fusion of PCF is used as the first reflector,the interface between PCF and sensing membrane is used as the second reflector,and the interface between the sensing membrane and the air is used as the third reflector,thus the dual Fabry-Pe rot structure sensor is formed.The results show that the sensor has excellent sensitivity and selectivity to carbon monoxide.With the increasing concentration of carbon monoxide gas in the range of 0-60 ppm,the intensity of interference spectrum decreases.The sensitivity of the sensor is 0.3473 dB m/ppm,and its linearity is good.The response time and recovery time are 68 s and 106 s,respectively.The sensor has the advantages of the compact size,low cost,high sensitivity,strong selectivity and simple structure.It is suitable for the sensing detection of low concentration carbon monoxide gas.