The hot deformation behavior of Fe-26Mn-6.2A1-0.05C steel was studied by experimental hot compression tests in the temperature range of 800-1050℃ and strain rate range of 0.01-30 s-1 on a Gleeble-3500 thermal simulat...The hot deformation behavior of Fe-26Mn-6.2A1-0.05C steel was studied by experimental hot compression tests in the temperature range of 800-1050℃ and strain rate range of 0.01-30 s-1 on a Gleeble-3500 thermal simulation machine.The microstructural evolution during the corresponding thermal process was observed in situ by confocal laser scanning microscopy.Electron backscattered diffraction and transmission electron microscopy analyses were carried out to observe the microstructural morphology before and after the hot deformation.Furthermore,interrupted compression tests were conducted to correlate the microstructural characteristics and softening mechanisms at different deformation stages.The results showed that hot compression tests of this steel were all carried out on a duplex matrix composed of austenite and fi-ferrite.As the deformation temperature increased from 800 to 1050℃,the volume fraction of austenite decreased from 70.9% to 44.0%,while that of 6-ferrite increased from 29.1% to 56.0%.Due to the different stress exponents(n)and apparent activation energies(Q),the generated strain was mostly accommodated by δ-ferrite at the commencement of deformation,and then both dynamic recovery and dynamic recrystallization occurred earlier in δ-ferrite than in austenite.This interaction of strain partitioning and unsynchronized softening behavior caused an abnormal hot deformation behavior profile in the Fe-Mn-A1 duplex steel,such as yield-like behavior,peculiar work-hardening behavior,and dynamic softening behavior,which are influenced by not only temperature and strain rate but also by microstructural evolution.展开更多
Nickel-free high-manganese austenitic Fe–24.4Mn–4.04Al–0.057C steel was produced by smelting,and the homogenized forged billet was hot-rolled.The plastic deformation mechanism was investigated through tensile testi...Nickel-free high-manganese austenitic Fe–24.4Mn–4.04Al–0.057C steel was produced by smelting,and the homogenized forged billet was hot-rolled.The plastic deformation mechanism was investigated through tensile testing of the hot-rolled sample.Different characterization techniques such as scanning electron microscopy,transmission electron microscopy,electron backscattered diffraction,and X-ray diffraction were used to analyze the microstructural evolution of steel under different strain levels.The steel had a single austenite phase,which was stable during deformation.After hot rolling,annealing twins were observed in the microstructure of the steel.The steel showed an excellent combination of mechanical properties,like a tensile strength of 527 MPa,impact energy of 203 J at−196℃,and an elongation of 67%till fracture.At the initial deformation stage,the dislocations were generated within the austenite grains,entangled and accumulated at the grain boundaries and annealing twin boundaries.Annealing twins participated in plastic deformation and hindered the dislocation movement.As the deformation progressed,the dislocation slip was hindered and produced stress concentration,and the stacking faults evolved into mechanical twins,which released the stress concentration and delayed the necking.展开更多
基金financially supported by the National Natural Science Foundation of China(No.51474031)
文摘The hot deformation behavior of Fe-26Mn-6.2A1-0.05C steel was studied by experimental hot compression tests in the temperature range of 800-1050℃ and strain rate range of 0.01-30 s-1 on a Gleeble-3500 thermal simulation machine.The microstructural evolution during the corresponding thermal process was observed in situ by confocal laser scanning microscopy.Electron backscattered diffraction and transmission electron microscopy analyses were carried out to observe the microstructural morphology before and after the hot deformation.Furthermore,interrupted compression tests were conducted to correlate the microstructural characteristics and softening mechanisms at different deformation stages.The results showed that hot compression tests of this steel were all carried out on a duplex matrix composed of austenite and fi-ferrite.As the deformation temperature increased from 800 to 1050℃,the volume fraction of austenite decreased from 70.9% to 44.0%,while that of 6-ferrite increased from 29.1% to 56.0%.Due to the different stress exponents(n)and apparent activation energies(Q),the generated strain was mostly accommodated by δ-ferrite at the commencement of deformation,and then both dynamic recovery and dynamic recrystallization occurred earlier in δ-ferrite than in austenite.This interaction of strain partitioning and unsynchronized softening behavior caused an abnormal hot deformation behavior profile in the Fe-Mn-A1 duplex steel,such as yield-like behavior,peculiar work-hardening behavior,and dynamic softening behavior,which are influenced by not only temperature and strain rate but also by microstructural evolution.
基金supported by the National Key Research and Development Program of China(No.2017YFB0304900).
文摘Nickel-free high-manganese austenitic Fe–24.4Mn–4.04Al–0.057C steel was produced by smelting,and the homogenized forged billet was hot-rolled.The plastic deformation mechanism was investigated through tensile testing of the hot-rolled sample.Different characterization techniques such as scanning electron microscopy,transmission electron microscopy,electron backscattered diffraction,and X-ray diffraction were used to analyze the microstructural evolution of steel under different strain levels.The steel had a single austenite phase,which was stable during deformation.After hot rolling,annealing twins were observed in the microstructure of the steel.The steel showed an excellent combination of mechanical properties,like a tensile strength of 527 MPa,impact energy of 203 J at−196℃,and an elongation of 67%till fracture.At the initial deformation stage,the dislocations were generated within the austenite grains,entangled and accumulated at the grain boundaries and annealing twin boundaries.Annealing twins participated in plastic deformation and hindered the dislocation movement.As the deformation progressed,the dislocation slip was hindered and produced stress concentration,and the stacking faults evolved into mechanical twins,which released the stress concentration and delayed the necking.