Microstructure transformation and aging hardening behavior of 15-5 PH stainless steel were studied by optical microscopy (OM), X-ray diffraction (XRD) and transmission electron microscopy (TEM). The results show...Microstructure transformation and aging hardening behavior of 15-5 PH stainless steel were studied by optical microscopy (OM), X-ray diffraction (XRD) and transmission electron microscopy (TEM). The results showed that the 15-5 PH stainless steel consists of NbC precipitates and lath matensite with a high dislocation density after solution treatment. With increasing aging temperature and aging time, the martensitic laths were resolved gradually. Meanwhile, the nanometric-sized Cu precipitates gradually coarsened and lost their coherency with'the martensite matrix, which exhibited an elliptical shape finally. Fine Cu precipitates can lead to significant dispersion hardening effect, while the coarsened Cu precipitates have no contribution to strengthening. The reversed austenite was observed in the speci- mens aged at 550 ℃ and above; moreover, the amount of reversed austenite increased as aging temperature in- creased. The precipitation hardening behavior of 15-5 PH stainless steel may depend on the balance between the softening caused by the formation of reversed austenite and the hardening caused by the precipitation of copper.展开更多
基金Item Sponsored by National High Technology Research and Development Program of China(2012AA03A507)Key Laboratory Foundation of Metal Material Microstructure Control of Jiangxi Province of China(JW201223001)Foundation of Jiangxi Educational Committee of China(GJJ14534)
文摘Microstructure transformation and aging hardening behavior of 15-5 PH stainless steel were studied by optical microscopy (OM), X-ray diffraction (XRD) and transmission electron microscopy (TEM). The results showed that the 15-5 PH stainless steel consists of NbC precipitates and lath matensite with a high dislocation density after solution treatment. With increasing aging temperature and aging time, the martensitic laths were resolved gradually. Meanwhile, the nanometric-sized Cu precipitates gradually coarsened and lost their coherency with'the martensite matrix, which exhibited an elliptical shape finally. Fine Cu precipitates can lead to significant dispersion hardening effect, while the coarsened Cu precipitates have no contribution to strengthening. The reversed austenite was observed in the speci- mens aged at 550 ℃ and above; moreover, the amount of reversed austenite increased as aging temperature in- creased. The precipitation hardening behavior of 15-5 PH stainless steel may depend on the balance between the softening caused by the formation of reversed austenite and the hardening caused by the precipitation of copper.