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研究型分析化学综合实验教学模式探究——以“海藻酸盐微胶囊的制备、药物包封及缓控释分析实验”为例
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作者 胡国梁 颜鑫灏 +4 位作者 陈睿希 刘红瑜 姚奇志 李娇 李玲玲 《大学化学》 CAS 2024年第1期134-141,共8页
“海藻酸盐微胶囊的制备、药物包封及缓控释分析实验”是II型分析化学实验中非常典型的一个研究型实验,它涵盖了微胶囊形成原理探究、实验条件设计、微胶囊性能表征等科研基本能力的训练。将海藻酸钠与亚甲基蓝混合溶液分别滴加至3%CaCl... “海藻酸盐微胶囊的制备、药物包封及缓控释分析实验”是II型分析化学实验中非常典型的一个研究型实验,它涵盖了微胶囊形成原理探究、实验条件设计、微胶囊性能表征等科研基本能力的训练。将海藻酸钠与亚甲基蓝混合溶液分别滴加至3%CaCl2溶液和1%壳聚糖溶液中,从而制备出两种不同性能的微胶囊。通过分光光度法测得不同时间溶液的浓度,从而得到缓释曲线,并对两种胶囊的缓释性进行对比分析。后续探究实验采用一步法和两步法制备微胶囊,将两种体系的优点结合起来,得到缓释性和稳定性均较好的微胶囊。 展开更多
关键词 海藻酸盐 微胶囊 缓释曲线 一步法 两步法
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Distributed Privacy-Preserving Fusion Estimation Using Homomorphic Encryption
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作者 xinhao yan Siqin Zhuo +1 位作者 yancheng Wu Bo Chen 《Journal of Beijing Institute of Technology》 EI CAS 2022年第6期551-558,共8页
The privacy-preserving problem for distributed fusion estimation scheme is concerned in this paper.When legitimate user wants to obtain consistent information from multiple sensors,it always employs a fusion center(FC... The privacy-preserving problem for distributed fusion estimation scheme is concerned in this paper.When legitimate user wants to obtain consistent information from multiple sensors,it always employs a fusion center(FC)to gather local data and compute distributed fusion estimates(DFEs).Due to the existence of potential eavesdropper,the data exchanged among sensors,FC and user imperatively require privacy preservation.Hence,we propose a distributed confidentiality fusion structure against eavesdropper by using Paillier homomorphic encryption approach.In this case,FC cannot acquire real values of local state estimates,while it only helps calculate encrypted DFEs.Then,the legitimate user can successfully obtain the true values of DFEs according to the encrypted information and secret keys,which is based on the homomorphism of encryption.Finally,an illustrative example is provided to verify the effectiveness of the proposed methods. 展开更多
关键词 eavesdropping attack distributed fusion estimation(DFE) homomorphic encryption computational privacy
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Catalysis and deactivation of montmorillonite K10 in the aryl O-glycosylation of glycosyl trichloroacetoimidates
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作者 Xiaoliu LI xinhao yan +2 位作者 Zhiwei LI Hua CHEN Pingzhu ZHANG 《Frontiers of Chemical Science and Engineering》 SCIE EI CSCD 2010年第3期342-347,共6页
The catalysis of montmorillonite K10(MK10)for aryl O-glycosylation of glycosyl trichloroacetimidates was investigated.It was found that the catalyst MK10 is deactivated gradually in the recycle glycosylation.The fresh... The catalysis of montmorillonite K10(MK10)for aryl O-glycosylation of glycosyl trichloroacetimidates was investigated.It was found that the catalyst MK10 is deactivated gradually in the recycle glycosylation.The fresh and the deactivated catalysts were characterized by X-ray diffraction(XRD),X-ray photoelectron spectroscopy(XPS),Thermogravimetric analysis(TGA),and N_(2)adsorption-desorption.The results show that the eliminated trichloroacetamide molecule deposits on the MK10,which blocks and poisons the active sites,resulting in the deactivation of the catalyst.The regeneration of the deactivated MK10 by calcination was studied preliminarily. 展开更多
关键词 aryl O-glycosides montmorillonite K10 DEACTIVATION
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