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粘结层真空退火处理对热障涂层热循环寿命的影响研究 被引量:5
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作者 刘贺 李帅 +4 位作者 余春堂 蒋成洋 鲍泽斌 朱圣龙 王福会 《表面技术》 EI CAS CSCD 北大核心 2020年第1期35-40,共6页
目的研究粘结层真空退火处理对热障涂层热循环条件下服役性能的影响。方法在某二代镍基单晶高温合金上涂覆铂铝粘结层,然后采用电子束物理气相沉积法沉积氧化钇稳定的氧化锆陶瓷层,构建热障涂层体系,在1100℃下可自动升降的循环氧化炉... 目的研究粘结层真空退火处理对热障涂层热循环条件下服役性能的影响。方法在某二代镍基单晶高温合金上涂覆铂铝粘结层,然后采用电子束物理气相沉积法沉积氧化钇稳定的氧化锆陶瓷层,构建热障涂层体系,在1100℃下可自动升降的循环氧化炉中进行热循环测试,通过高精度电子天平对涂层样品进行称量并绘制质量变化曲线,采用拍摄宏观照片的方式观察样品表面陶瓷层剥落情况,利用扫描电子显微镜观察沉积态及热循环后的样品截面微观组织结构形貌。结果与沉积态粘结层相比,在高真空中进行退火处理后,热障涂层的热循环寿命几乎增加一倍,且陶瓷层与热生长氧化膜结合良好。未经过真空处理的铂铝涂层表面陶瓷层发生明显剥落,且热生长氧化膜质量较差,出现了明显裂纹。结论真空退火处理可使铂铝涂层表面更加平整,在高温氧化过程中生成的低缺陷氧化膜有更好的质量,陶瓷层与粘结层的结合力更强,热障涂层体系的服役性能和寿命得到有效提升。 展开更多
关键词 热障涂层 铂铝涂层 循环氧化 热生长氧化膜
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Effect of strain,strain rate and temperature on workability of AZ80 wrought magnesium alloy 被引量:2
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作者 Lü Wen-quan QUAN Guo-zheng +2 位作者 yu chun-tang ZHAO Lei ZHOU Jie 《中国有色金属学会会刊:英文版》 CSCD 2012年第S3期650-655,共6页
The hot deformation behavior of AZ80 wrought magnesium alloy was studied in the temperature range of 523-673 K and the strain rate range of 0.01-10 s-1 using hot compression tests.Through the flow stresses behavior,th... The hot deformation behavior of AZ80 wrought magnesium alloy was studied in the temperature range of 523-673 K and the strain rate range of 0.01-10 s-1 using hot compression tests.Through the flow stresses behavior,the processing maps were calculated and analyzed according to the dynamic materials model.The stable,metastable and unstable regimes were clarified.The optimum processing conditions were suggested as following:the DRX regions in Domain #1-0.25,Domain #2-0.25,Domain #1-0.45,Domain #2-0.45,Domain #3-0.45,Domain #1-0.65 and Domain #1-0.85,and the DRV regions in Domain #3-0.25 and Domain #4-0.45.In each "safe" DRX domain,it is preferable to conduct hot working in the small region around efficiency peak point.The strain has a great influence on the processing maps.The whole area of the "safe" domains increases with the increase of true strain from 0.25 to 0.65,while it decreases with the increase of true strain from 0.65 to 0.85.The results of kinetic analysis reveal that the values of apparent activation energy in all the domains are higher than that for self-diffusion in pure magnesium (135kJ/mol),and the deformation mechanism in all the domains is likely to be cross-slip. 展开更多
关键词 AZ80 MAGNESIUM alloy strain rate KINETIC analysis processing map flow behavior
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