Hot compression tests of Fe-Cr-Ni-Mo-N super-austenitic stainless steel were carried out in the temperature range of 950-1150℃with a strain rate of 0.01-10 s-1,in which dynamic recrystallization(DRX)mechanisms and co...Hot compression tests of Fe-Cr-Ni-Mo-N super-austenitic stainless steel were carried out in the temperature range of 950-1150℃with a strain rate of 0.01-10 s-1,in which dynamic recrystallization(DRX)mechanisms and coincident site lattice(CSL)boundary evolution in consideration of adiabatic heating were investigated.The results show that discontinuous DRX was the main DRX mechanism.Due to the high stacking fault energy(162-173 mJ/m2),subgrain evolution occurring in dynamic recovery process was stimulated at high temperatures and high strain rates.DRX behavior was accelerated by higher strain rate and adiabatic heating.Also,amounts of fine annealing twin boundaries were observed in the specimens deformed at higher strain rates and higher temperatures.By analyzing the length fractions of∑3 boundary in overall boundaries and in CSL boundaries,the results indicate that∑3 regeneration mechanism and new twinning mechanism take effect concurrently for twin-related grain boundary when the specimens were deformed at 950℃with a strain rate of 0.01-10 s-1.With increasing strain rate or deformation temperature,the propagation of∑3 boundaries was mainly dominated by new twinning mechanism.展开更多
Hot compression tests were carried out with specimens of 20Cr-24Ni-6Mo super-austenitic stainless steel at strain rate from 0.01 to 10 s^-1 in the temperature range from 950 to 1150 ℃,and flow behavior was analyzed.M...Hot compression tests were carried out with specimens of 20Cr-24Ni-6Mo super-austenitic stainless steel at strain rate from 0.01 to 10 s^-1 in the temperature range from 950 to 1150 ℃,and flow behavior was analyzed.Microstructure analysis indicated that dynamic recrystallization（DRX）behavior was more sensitive to the temperature than strain rate,and full DRX was obtained when the specimen deformed at 1150℃.When the temperature reduced to 1050 ℃,full DRX was completed at the highest strain rate 10 s-l rather than at the lowest strain rate 0.01 s-1 because the adiabatic heating was pronounced at higher strain rate.In addition,flow behavior reflected in flow curves was inconsistent with the actual microstructural evolution during hot deformation,especially at higher strain rates and lower temperatures.Therefore,flow curves were revised in consideration of the effects of adiabatic heating and friction during hot deformation.The results showed that adiabatic heating became greater with the increase of strain level,strain rate and the decrease of temperature,while the frictional effect cannot be neglected at high strain level.Moreover,based on the revised flow curves,strain-dependent constitutive modeling was developed and verified by comparing the predicted data with the experimental data and the modified data.The result suggested that the developed constitutive modeling can more adequately predict the flow behavior reflected by corrected flow curves than that reflected by experimental flow curves,even though some difference existed at 950℃ and 0.01 s^-1.The main reason was that plenty of precipitates generated at this deformation condition and affected the DRX behavior and deformation behavior,eventually resulted in dramatic increase of deformation resistance.展开更多
基金The authors would like to acknowledge the financial supports from the National Natural Science Foundation of China(U1460204,U1660117).
文摘Hot compression tests of Fe-Cr-Ni-Mo-N super-austenitic stainless steel were carried out in the temperature range of 950-1150℃with a strain rate of 0.01-10 s-1,in which dynamic recrystallization(DRX)mechanisms and coincident site lattice(CSL)boundary evolution in consideration of adiabatic heating were investigated.The results show that discontinuous DRX was the main DRX mechanism.Due to the high stacking fault energy(162-173 mJ/m2),subgrain evolution occurring in dynamic recovery process was stimulated at high temperatures and high strain rates.DRX behavior was accelerated by higher strain rate and adiabatic heating.Also,amounts of fine annealing twin boundaries were observed in the specimens deformed at higher strain rates and higher temperatures.By analyzing the length fractions of∑3 boundary in overall boundaries and in CSL boundaries,the results indicate that∑3 regeneration mechanism and new twinning mechanism take effect concurrently for twin-related grain boundary when the specimens were deformed at 950℃with a strain rate of 0.01-10 s-1.With increasing strain rate or deformation temperature,the propagation of∑3 boundaries was mainly dominated by new twinning mechanism.
基金supported financially by the National Natural Science Foundation of China(No.U1460204)
文摘Hot compression tests were carried out with specimens of 20Cr-24Ni-6Mo super-austenitic stainless steel at strain rate from 0.01 to 10 s^-1 in the temperature range from 950 to 1150 ℃,and flow behavior was analyzed.Microstructure analysis indicated that dynamic recrystallization（DRX）behavior was more sensitive to the temperature than strain rate,and full DRX was obtained when the specimen deformed at 1150℃.When the temperature reduced to 1050 ℃,full DRX was completed at the highest strain rate 10 s-l rather than at the lowest strain rate 0.01 s-1 because the adiabatic heating was pronounced at higher strain rate.In addition,flow behavior reflected in flow curves was inconsistent with the actual microstructural evolution during hot deformation,especially at higher strain rates and lower temperatures.Therefore,flow curves were revised in consideration of the effects of adiabatic heating and friction during hot deformation.The results showed that adiabatic heating became greater with the increase of strain level,strain rate and the decrease of temperature,while the frictional effect cannot be neglected at high strain level.Moreover,based on the revised flow curves,strain-dependent constitutive modeling was developed and verified by comparing the predicted data with the experimental data and the modified data.The result suggested that the developed constitutive modeling can more adequately predict the flow behavior reflected by corrected flow curves than that reflected by experimental flow curves,even though some difference existed at 950℃ and 0.01 s^-1.The main reason was that plenty of precipitates generated at this deformation condition and affected the DRX behavior and deformation behavior,eventually resulted in dramatic increase of deformation resistance.
