A high-Ti 6061 alloy was rolled with strains up to 0. 8 - 2. 0 and at 350 - 550 ℃ . Microstructures that developed during deformation and subsequent solution heat treatment (SHT) were observed by using optical and tr...A high-Ti 6061 alloy was rolled with strains up to 0. 8 - 2. 0 and at 350 - 550 ℃ . Microstructures that developed during deformation and subsequent solution heat treatment (SHT) were observed by using optical and transmission electron microscopy. Microstructure evolution during SHT depends mainly on the initial rolling temperature,and it was found that the higher this temperature is,the coarser the grains are. After rolling at 400 ℃ ,well-defined cells and subgrains were formed, which induced further sites for recrystallization nucleation during subsequent SHT. The recrystallization mechanism was found to be subgrain rotation,with a final grain size smaller than 200 μm. Increasing the rolling temperature to 500 ℃ results in a low density of dislocations distributed uniformly in the deformed matrix and fewer nucleation sites during subsequent SHT. The recrystallization mechanism is grain boundary bulging,while the final grain size approaches several millimeters. Finally,a hot forming process of high-Ti 6061 alloy for inhibiting grain coarsening was proposed,and verified by experiments.展开更多
The dilatometric curves of B1500HS high-strength steel at different heating rates were measured by a Gleeble-3800 thermal simulator and analyzed to investigate the effect of heating rate on austenitization.Results sho...The dilatometric curves of B1500HS high-strength steel at different heating rates were measured by a Gleeble-3800 thermal simulator and analyzed to investigate the effect of heating rate on austenitization.Results show that the value of starting temperature and ending temperature of austenite transformation increase with the rise of heating rates,whereas the temperature interval of austenite formation decreases.The kinetic equation of austenite transformation was solved using the Johnson–Mehl–Avrami model,and the related parameters of the equation were analyzed by the Kissinger method.For those calculations,the activation energy of austenite transformation is 1.01×10^6 J/mol,and the values of kinetic parameters n and ln k0 are 0.63 and 103.03,respectively.The relationship between the volume fraction of austenite and the heating time at different heating rates could be predicted using the kinetic equation.The predicted and experimental results were compared to verify the accuracy of the kinetic equation.The microstructure etched by different corrosive solutions was analyzed,and the reliability of kinetic equation was further verified from the microscopic perspective.展开更多
Research on the formability of tailor rolled blank (TRB) is of good practical significance and application value because of the enormous potential of TRB in the aspect of automobile lightweight. However, the forming...Research on the formability of tailor rolled blank (TRB) is of good practical significance and application value because of the enormous potential of TRB in the aspect of automobile lightweight. However, the forming of TRB is problematic because of the varying properties; especially, springback is a main challenge. The transverse bending (bending axis is perpendicular to the rolling direction) of TRB U channel was studied through simulation and experiment. The forming characteristics of TRB U channel during transverse bending were analyzed. The mechanisms of forming defects, including bending springback and thickness transition zone (TTZ) movement, were revealed. On this basis, effects of blank geometric parameters on springbaek and TTZ movement were discussed. The results indicate that springback and TTZ movement happen during transverse bending of TRB U-channel. Nonuni form stress distribution is the most fundamental reason for the occurrence of springback of TRB during transverse bending. Annealing can eliminate nonuniform stress distribution, and thus diminish springbaek of TRB, especially springback on the thinner side. Therefore, springback of the whole TRB becomes more uniform. However, annealing can increase the TTZ movement. Blank thickness and TTZ position are the main factors affecting the formability of TRB U-channel during transverse bending.展开更多
The phase diagram of an Nb- and V-containing 18Mnl8Cr0.5N steel was investigated using thermodynam ic calculation. The compositions and characteristics of precipitates were investigated by scanning electron microsco- ...The phase diagram of an Nb- and V-containing 18Mnl8Cr0.5N steel was investigated using thermodynam ic calculation. The compositions and characteristics of precipitates were investigated by scanning electron microsco- py, energy dispersive spectrometry, X-ray diffraction, and differential scanning calorimetry. Under equilibrium con- ditions, MX precipitates at 1 350 ℃. MX is a substitutional solid solution of Nb4 N3.38, and its composition (at. %) is approximately.. Nb 40, N 40, V 8, and Fe, Cr, and Mn balance. The precipitates, with shapes including irregular bulk, rod, and ellipsoid, are primarily distributed at grain boundaries and triple junctions, and their size is approxi- mately 5 10 μm. Finally, the microalloying of high nitrogen CrMn austenite steels, control of precipitate size, and the effect of precipitate on hot formin~ were discussed.展开更多
Hot deformation behavior of the annealed ZK61 M magnesium alloy sheet was explored using tensile tests with strain rates varying from 0.001 to 0.030 s^(-1) in temperatures range of 423-513 K.The obtained results indic...Hot deformation behavior of the annealed ZK61 M magnesium alloy sheet was explored using tensile tests with strain rates varying from 0.001 to 0.030 s^(-1) in temperatures range of 423-513 K.The obtained results indicate that the flow stress increased with deformation temperature decreasing and strain rate increasing.Dynamic recrystallization(DRX)occurs when the temperature is higher than 423 K,and the recrystallization volume fraction increases with temperature rising.At a given temperature,the measured DRX volume fraction at a higher strain rate is smaller than that at a lower strain rate.Dimples are observed throughout the tested temperature range.Moreover,they grow larger as temperature increases.An average absolute relative error(AARE)of 2.65%proves that the peak stress predicted by the constitutive model is in good agreement with the experimental results.The correlation coefficient(R’)obtained for the predicted stress and the experimental value considering the strain on the material constant are between 0.9831 and 0.9977.In addition,AARE and root mean square error(RMSE)are less than 6.5%and 8.5 MPa,respectively.This indicates that the deviation of the predicted value from the experimental value is small and the predictions of the proposed model are reliable.展开更多
基金Sponsored by the Project of High-level Talent of Hebei Province (Post-Doctoral Research Project of Hebei Province)
文摘A high-Ti 6061 alloy was rolled with strains up to 0. 8 - 2. 0 and at 350 - 550 ℃ . Microstructures that developed during deformation and subsequent solution heat treatment (SHT) were observed by using optical and transmission electron microscopy. Microstructure evolution during SHT depends mainly on the initial rolling temperature,and it was found that the higher this temperature is,the coarser the grains are. After rolling at 400 ℃ ,well-defined cells and subgrains were formed, which induced further sites for recrystallization nucleation during subsequent SHT. The recrystallization mechanism was found to be subgrain rotation,with a final grain size smaller than 200 μm. Increasing the rolling temperature to 500 ℃ results in a low density of dislocations distributed uniformly in the deformed matrix and fewer nucleation sites during subsequent SHT. The recrystallization mechanism is grain boundary bulging,while the final grain size approaches several millimeters. Finally,a hot forming process of high-Ti 6061 alloy for inhibiting grain coarsening was proposed,and verified by experiments.
基金This work was financially supported by the Natural Science Foundation of Hebei Province of China(No.E2018203254)the Scientific Research Program of Hebei Province Education Department,China(No.ZD2019013).
文摘The dilatometric curves of B1500HS high-strength steel at different heating rates were measured by a Gleeble-3800 thermal simulator and analyzed to investigate the effect of heating rate on austenitization.Results show that the value of starting temperature and ending temperature of austenite transformation increase with the rise of heating rates,whereas the temperature interval of austenite formation decreases.The kinetic equation of austenite transformation was solved using the Johnson–Mehl–Avrami model,and the related parameters of the equation were analyzed by the Kissinger method.For those calculations,the activation energy of austenite transformation is 1.01×10^6 J/mol,and the values of kinetic parameters n and ln k0 are 0.63 and 103.03,respectively.The relationship between the volume fraction of austenite and the heating time at different heating rates could be predicted using the kinetic equation.The predicted and experimental results were compared to verify the accuracy of the kinetic equation.The microstructure etched by different corrosive solutions was analyzed,and the reliability of kinetic equation was further verified from the microscopic perspective.
基金Item Sponsored by National Natural Science Foundation of China(51475086)Natural Science Foundation of Hebei Province of China(E2016501118,E2015501073)China Postdoctoral Science Foundation(2016M591404)
文摘Research on the formability of tailor rolled blank (TRB) is of good practical significance and application value because of the enormous potential of TRB in the aspect of automobile lightweight. However, the forming of TRB is problematic because of the varying properties; especially, springback is a main challenge. The transverse bending (bending axis is perpendicular to the rolling direction) of TRB U channel was studied through simulation and experiment. The forming characteristics of TRB U channel during transverse bending were analyzed. The mechanisms of forming defects, including bending springback and thickness transition zone (TTZ) movement, were revealed. On this basis, effects of blank geometric parameters on springbaek and TTZ movement were discussed. The results indicate that springback and TTZ movement happen during transverse bending of TRB U-channel. Nonuni form stress distribution is the most fundamental reason for the occurrence of springback of TRB during transverse bending. Annealing can eliminate nonuniform stress distribution, and thus diminish springbaek of TRB, especially springback on the thinner side. Therefore, springback of the whole TRB becomes more uniform. However, annealing can increase the TTZ movement. Blank thickness and TTZ position are the main factors affecting the formability of TRB U-channel during transverse bending.
基金Item Sponsored by Natural Science Foundation of Hebei Province for Distinguished Young Scholars of China(E2011203131)Natural Science Foundation-Steel and Iron Foundation of Hebei Province of China(E2013203110)
文摘The phase diagram of an Nb- and V-containing 18Mnl8Cr0.5N steel was investigated using thermodynam ic calculation. The compositions and characteristics of precipitates were investigated by scanning electron microsco- py, energy dispersive spectrometry, X-ray diffraction, and differential scanning calorimetry. Under equilibrium con- ditions, MX precipitates at 1 350 ℃. MX is a substitutional solid solution of Nb4 N3.38, and its composition (at. %) is approximately.. Nb 40, N 40, V 8, and Fe, Cr, and Mn balance. The precipitates, with shapes including irregular bulk, rod, and ellipsoid, are primarily distributed at grain boundaries and triple junctions, and their size is approxi- mately 5 10 μm. Finally, the microalloying of high nitrogen CrMn austenite steels, control of precipitate size, and the effect of precipitate on hot formin~ were discussed.
基金financially supported by the National Natural Science Foundation of China(No.51275444)the Natural Science Foundation of Hebei Province(No.E2018203254)the Innovative Research Assistant Project for Graduate Students of Yanshan University(No.CXZS202001)。
文摘Hot deformation behavior of the annealed ZK61 M magnesium alloy sheet was explored using tensile tests with strain rates varying from 0.001 to 0.030 s^(-1) in temperatures range of 423-513 K.The obtained results indicate that the flow stress increased with deformation temperature decreasing and strain rate increasing.Dynamic recrystallization(DRX)occurs when the temperature is higher than 423 K,and the recrystallization volume fraction increases with temperature rising.At a given temperature,the measured DRX volume fraction at a higher strain rate is smaller than that at a lower strain rate.Dimples are observed throughout the tested temperature range.Moreover,they grow larger as temperature increases.An average absolute relative error(AARE)of 2.65%proves that the peak stress predicted by the constitutive model is in good agreement with the experimental results.The correlation coefficient(R’)obtained for the predicted stress and the experimental value considering the strain on the material constant are between 0.9831 and 0.9977.In addition,AARE and root mean square error(RMSE)are less than 6.5%and 8.5 MPa,respectively.This indicates that the deviation of the predicted value from the experimental value is small and the predictions of the proposed model are reliable.