The production of low-temperature reheated grain-oriented silicon steel is mainly based on the acquired inhibitor method.Due to the additional nitriding process,a high nitrogen content exists in the oxide layer,which ...The production of low-temperature reheated grain-oriented silicon steel is mainly based on the acquired inhibitor method.Due to the additional nitriding process,a high nitrogen content exists in the oxide layer,which changes the structure of the oxide layer.In this study,the structure of the surface oxide layer after nitriding was analyzed by scanning electron microscopy(SEM),electron back-scattered diffraction(EBSD),glow discharge spectrometry(GDS),and X-ray diffraction(XRD).The size and orientation of ferritic grains in the oxide layer were characterized,and the distribution characteristics of the key elements along the thickness direction were determined.The results show that the oxide layer of the steel sample mainly comprised particles of Fe2SiO4 and spherical and lamellar SiO2,and Fe4N and fcc-Fe phases were also detected.Moreover,the size and orientation of ferritic grains in the oxide layer were different from those of coarse matrix ferritic grains beneath the oxide layer;however,some ferritic grains exhibited same orientations as those in the neighboring matrix.Higher nitrogen content was detected in the oxide layer than that in the matrix beneath the oxide layer.The form of nitrogen enrichment in the oxide layer was analyzed,and the growth mechanism of ferritic grains during the oxide layer formation is proposed.展开更多
Dynamic states in mutual-coupled mid-infrared quantum cascade lasers(QCLs) were numerically investigated in the parameter space of injection strength and detuning frequency based on the Lang-Kobayashi equations model....Dynamic states in mutual-coupled mid-infrared quantum cascade lasers(QCLs) were numerically investigated in the parameter space of injection strength and detuning frequency based on the Lang-Kobayashi equations model. Three types of period-one states were found, with different periods of injection time delay τ_(inj), 2τ_(inj), and reciprocal of the detuning frequency. Besides, square-wave, quasi-period, pulse-burst and chaotic oscillations were also observed. It is concluded that external-cavity periodic dynamics and optical modes beating are the mainly periodic dynamics. The interaction of the two periodic dynamics and the high-frequency dynamics stimulated by strong injection induces the dynamic states evolution.This work helps to understand the dynamic behaviors in QCLs and shows a new way to mid-infrared wide-band chaotic laser.展开更多
We report an index-coupled distributed feedback quantum cascade laser by employing an equivalent phase shift(EPS) of quarter-wave integrated with a distributed Bragg reflector(DBR) at λ~5.03 μm. The EPS is fabricate...We report an index-coupled distributed feedback quantum cascade laser by employing an equivalent phase shift(EPS) of quarter-wave integrated with a distributed Bragg reflector(DBR) at λ~5.03 μm. The EPS is fabricated through extending one sampling period by 50% in the center of a sampled Bragg grating. The key EPS and DBR pattern are fabricated by conventional holographic exposure combined with the optical photolithography technology, which leads to improved flexibility, repeatability, and cost-effectiveness. Stable single-mode emission can be obtained by changing the injection current or heat sink temperature even under the condition of large driving pulse width.展开更多
基金financially supported by the Fundamental Research Funds for the Central Universities (No. FRF-IC-18-006)
文摘The production of low-temperature reheated grain-oriented silicon steel is mainly based on the acquired inhibitor method.Due to the additional nitriding process,a high nitrogen content exists in the oxide layer,which changes the structure of the oxide layer.In this study,the structure of the surface oxide layer after nitriding was analyzed by scanning electron microscopy(SEM),electron back-scattered diffraction(EBSD),glow discharge spectrometry(GDS),and X-ray diffraction(XRD).The size and orientation of ferritic grains in the oxide layer were characterized,and the distribution characteristics of the key elements along the thickness direction were determined.The results show that the oxide layer of the steel sample mainly comprised particles of Fe2SiO4 and spherical and lamellar SiO2,and Fe4N and fcc-Fe phases were also detected.Moreover,the size and orientation of ferritic grains in the oxide layer were different from those of coarse matrix ferritic grains beneath the oxide layer;however,some ferritic grains exhibited same orientations as those in the neighboring matrix.Higher nitrogen content was detected in the oxide layer than that in the matrix beneath the oxide layer.The form of nitrogen enrichment in the oxide layer was analyzed,and the growth mechanism of ferritic grains during the oxide layer formation is proposed.
基金Project supported by the National Key Research and Development Program of China (Grant No. 2019YFB1803500)the National Natural Science Foundation of China (Grant No. 61805168)+4 种基金the Natural Science Foundation of Shanxi Province, China (Grant Nos. 201801D221183 and 20210302123185)International Cooperation of Key Research and Development Program of Shanxi Province (Grant No. 201903D421012)Research Project Supported by Shanxi Scholarship Council of China (Grant No. 2021-032)Scientific and Technological Innovation Programs of Higher Education Institutions in Shanxi (Grant No. 2019L0133)Fund for Shanxi “1331 Project” Key Innovative Research Team。
文摘Dynamic states in mutual-coupled mid-infrared quantum cascade lasers(QCLs) were numerically investigated in the parameter space of injection strength and detuning frequency based on the Lang-Kobayashi equations model. Three types of period-one states were found, with different periods of injection time delay τ_(inj), 2τ_(inj), and reciprocal of the detuning frequency. Besides, square-wave, quasi-period, pulse-burst and chaotic oscillations were also observed. It is concluded that external-cavity periodic dynamics and optical modes beating are the mainly periodic dynamics. The interaction of the two periodic dynamics and the high-frequency dynamics stimulated by strong injection induces the dynamic states evolution.This work helps to understand the dynamic behaviors in QCLs and shows a new way to mid-infrared wide-band chaotic laser.
基金National Basic Research Program of China(2013CB632800)National Key Research and Development Program(2016YFB0402303)+2 种基金National Natural Science Foundation of China(NSFC)(61404131,61435014,61674144,61574136,61627822)Chinese Academy of Sciences Key Project(CAS Key Project)(QYZDJ-SSWJSC027,ZDRW-XH-2016-4)Natural Science Foundation of Beijing Municipality(4162060,4172060)
文摘We report an index-coupled distributed feedback quantum cascade laser by employing an equivalent phase shift(EPS) of quarter-wave integrated with a distributed Bragg reflector(DBR) at λ~5.03 μm. The EPS is fabricated through extending one sampling period by 50% in the center of a sampled Bragg grating. The key EPS and DBR pattern are fabricated by conventional holographic exposure combined with the optical photolithography technology, which leads to improved flexibility, repeatability, and cost-effectiveness. Stable single-mode emission can be obtained by changing the injection current or heat sink temperature even under the condition of large driving pulse width.