3D reticulated ceramics (3DRCs) with the composition containing SrFe12O19-SiC-TiO2 were prepared by a replication process with polyurethane sponges as the template in ceramic slurry. The electrical conductivity, diele...3D reticulated ceramics (3DRCs) with the composition containing SrFe12O19-SiC-TiO2 were prepared by a replication process with polyurethane sponges as the template in ceramic slurry. The electrical conductivity, dielectric and magnetic parameters of 3D reticulated ceramics (3DRCs) were measured with changes in cell size of the sponges, contents in the slurry and sintering temperature in this paper. Discussions about the influential factors of those parameters were focused on their electrical conductivity. The experimental results indicated that the electrical conductivity of 3DRCs raised with the increase of cell size, SiC/SrO 6Fe2O3 with weight ratio and sintering temperature. X-ray diffractions and SEM were used to investigate the relationship between electrical conductivity and sintering temperature. Deoxidizing reactions of SrO 6Fe2O3 caused the increasing electrical conductivity. The real part of permittivity (ε') and imaginary part of permeability (μ') raised with the increase of electrical conductivity (σ). The imaginary part of permittivity (ε') has a maximum at 10o S/cm with the increase of a, and the real part of permeability (μ') changes slightly with the increase of a. When a is at the range of 10-4 S/cm to 10o S/cm (a semi conductive state), both the imagine part of permittivity and permeability raises with increasing a, therefore, the 3DRCs present their high electromagnetic loss properties.展开更多
3-dimensional reticulated ceramics (3DRCs) and their same composition ceramic disks(SCCDs) were fabricated by sol-gel method, with the composition of SrO-6Fe203(30%), SiC(35%) and Ti02(35%), sintered at 1200C in N2. T...3-dimensional reticulated ceramics (3DRCs) and their same composition ceramic disks(SCCDs) were fabricated by sol-gel method, with the composition of SrO-6Fe203(30%), SiC(35%) and Ti02(35%), sintered at 1200C in N2. The dielectric and magnetic parameters of such 3DRCs and their SCCDs were measured respectively in a temperature range from room temperature to 800癈 and in a frequency range from 2.6 GHz to 18 GHz. The results showed that the dielectric and magnetic loss of 3DRCs were obviously larger than those of their SCCDs in a wide range of temperature and the whole range of measuring frequency. The increase of dielectric loss of SDRCs was much higher than that of magnetic loss compared to their SCCDs, which was found due to the 3D net structure extrinsic characteristics.展开更多
文摘3D reticulated ceramics (3DRCs) with the composition containing SrFe12O19-SiC-TiO2 were prepared by a replication process with polyurethane sponges as the template in ceramic slurry. The electrical conductivity, dielectric and magnetic parameters of 3D reticulated ceramics (3DRCs) were measured with changes in cell size of the sponges, contents in the slurry and sintering temperature in this paper. Discussions about the influential factors of those parameters were focused on their electrical conductivity. The experimental results indicated that the electrical conductivity of 3DRCs raised with the increase of cell size, SiC/SrO 6Fe2O3 with weight ratio and sintering temperature. X-ray diffractions and SEM were used to investigate the relationship between electrical conductivity and sintering temperature. Deoxidizing reactions of SrO 6Fe2O3 caused the increasing electrical conductivity. The real part of permittivity (ε') and imaginary part of permeability (μ') raised with the increase of electrical conductivity (σ). The imaginary part of permittivity (ε') has a maximum at 10o S/cm with the increase of a, and the real part of permeability (μ') changes slightly with the increase of a. When a is at the range of 10-4 S/cm to 10o S/cm (a semi conductive state), both the imagine part of permittivity and permeability raises with increasing a, therefore, the 3DRCs present their high electromagnetic loss properties.
文摘3-dimensional reticulated ceramics (3DRCs) and their same composition ceramic disks(SCCDs) were fabricated by sol-gel method, with the composition of SrO-6Fe203(30%), SiC(35%) and Ti02(35%), sintered at 1200C in N2. The dielectric and magnetic parameters of such 3DRCs and their SCCDs were measured respectively in a temperature range from room temperature to 800癈 and in a frequency range from 2.6 GHz to 18 GHz. The results showed that the dielectric and magnetic loss of 3DRCs were obviously larger than those of their SCCDs in a wide range of temperature and the whole range of measuring frequency. The increase of dielectric loss of SDRCs was much higher than that of magnetic loss compared to their SCCDs, which was found due to the 3D net structure extrinsic characteristics.
