Small Angle X-ray Scattering (SAXS) experiment using Synchrotron Radiation as X-ray source was used to determine the average wall thickness of mesoporous silica prepared by condensation of tetraethylorthosilicate (TEO...Small Angle X-ray Scattering (SAXS) experiment using Synchrotron Radiation as X-ray source was used to determine the average wall thickness of mesoporous silica prepared by condensation of tetraethylorthosilicate (TEOS) using non-ionic alkylpolyethyleneoxide (AEO(9)) surfactant as templates. The results agreed with that of high-resolution TEM (HRTEM) measurement.展开更多
A new furostanol component glycosylated only at C-26 was isolated from the rhizomes of Polygonatum odoratum (Mill.) Druce, and its structure was characterized as 22-hydroxy-25(R and S) furost-5-en-12-on-3b, 22, 26-tri...A new furostanol component glycosylated only at C-26 was isolated from the rhizomes of Polygonatum odoratum (Mill.) Druce, and its structure was characterized as 22-hydroxy-25(R and S) furost-5-en-12-on-3b, 22, 26-triol 26-O-b-D-glucopyranoside on the basis of spectroscopic techniques and chemical methods.展开更多
Composite membranes and sponge scaffolds consisting chitosan (CS) and acellular derm matrix (ADM) in six ratios were prepared by solvent evaporation technique and freeze-drying method, respectively. The composite mate...Composite membranes and sponge scaffolds consisting chitosan (CS) and acellular derm matrix (ADM) in six ratios were prepared by solvent evaporation technique and freeze-drying method, respectively. The composite materials were characterized by water contact angle measurement, scanning electron microscopy (SEM), water absorption and HaCat cells compatibility. The SEM result showed that CS/ADM three-dimensional (3D) micro-porous structures were successfully produced. The water absorption value of all scaffolds was over 18 times of its initial weight, which is high enough for skin regeneration scaffold, but there were no significant differences of water absorption ratio between deionized water and PBS solution for same scaffold (P > 0.05). HaCat cells were distributed uniformly on the surfaces of membrane 4-6, and an almost confluent monolayer was formed on membrane 6 on the fifth day, whereas cells maintained round and spherical in shape on the surface of membrane 1. The results showed that the cell compatibility of pure CS membrane needed to be improved, and addition of ADM realized this purpose. The results of compatibility of HaCat cells on scaffolds showed that the cell proliferated well on the scaffolds 3 and 4. In our study, the cell’s attachment and growth on the composite membranes was mainly determined by the content of the membrane, whereas the cell’s attachment and growth in the scaffolds was determined by both the content and structure of the scaffolds.展开更多
Spectroscopic factor elucidates the overlap between the initial and final states as well as the occupancy of a given singleparticle orbit.It plays an important role in nuclear reactions and nuclear astrophysics.Single...Spectroscopic factor elucidates the overlap between the initial and final states as well as the occupancy of a given singleparticle orbit.It plays an important role in nuclear reactions and nuclear astrophysics.Single-nucleon transfer reactions such as(J,p)and(d,n)have been used extensively to extract the spectroscopic information of the single-nucleon orbits in nuclei located at or near the stability line[1-3],by comparing the experimental and theoretical differential cross sections as expressed by eq.(1).The uncertainties of the extracted spectroscopic factors are from the statistics of the measurements(3%),the uncertainties of the target thickness(5%),the optical potential parameters for both entrance(15%)and exit channels(15%),the geometrical parameters for the bound states(20%),as well as the spectroscopic factor in d(15%).展开更多
文摘Small Angle X-ray Scattering (SAXS) experiment using Synchrotron Radiation as X-ray source was used to determine the average wall thickness of mesoporous silica prepared by condensation of tetraethylorthosilicate (TEOS) using non-ionic alkylpolyethyleneoxide (AEO(9)) surfactant as templates. The results agreed with that of high-resolution TEM (HRTEM) measurement.
基金Project 02-03zp09 was supported by the Science Foundation of State Administration of Traditional Chinese Medicine,P.R.China
文摘A new furostanol component glycosylated only at C-26 was isolated from the rhizomes of Polygonatum odoratum (Mill.) Druce, and its structure was characterized as 22-hydroxy-25(R and S) furost-5-en-12-on-3b, 22, 26-triol 26-O-b-D-glucopyranoside on the basis of spectroscopic techniques and chemical methods.
文摘Composite membranes and sponge scaffolds consisting chitosan (CS) and acellular derm matrix (ADM) in six ratios were prepared by solvent evaporation technique and freeze-drying method, respectively. The composite materials were characterized by water contact angle measurement, scanning electron microscopy (SEM), water absorption and HaCat cells compatibility. The SEM result showed that CS/ADM three-dimensional (3D) micro-porous structures were successfully produced. The water absorption value of all scaffolds was over 18 times of its initial weight, which is high enough for skin regeneration scaffold, but there were no significant differences of water absorption ratio between deionized water and PBS solution for same scaffold (P > 0.05). HaCat cells were distributed uniformly on the surfaces of membrane 4-6, and an almost confluent monolayer was formed on membrane 6 on the fifth day, whereas cells maintained round and spherical in shape on the surface of membrane 1. The results showed that the cell compatibility of pure CS membrane needed to be improved, and addition of ADM realized this purpose. The results of compatibility of HaCat cells on scaffolds showed that the cell proliferated well on the scaffolds 3 and 4. In our study, the cell’s attachment and growth on the composite membranes was mainly determined by the content of the membrane, whereas the cell’s attachment and growth in the scaffolds was determined by both the content and structure of the scaffolds.
基金supported by the National Natural Science Foundation of China(Grant Nos.11490563,11575292,and 11505302)the National Key Research and Development Program of China(Grant No.2016YFA0400502)
文摘Spectroscopic factor elucidates the overlap between the initial and final states as well as the occupancy of a given singleparticle orbit.It plays an important role in nuclear reactions and nuclear astrophysics.Single-nucleon transfer reactions such as(J,p)and(d,n)have been used extensively to extract the spectroscopic information of the single-nucleon orbits in nuclei located at or near the stability line[1-3],by comparing the experimental and theoretical differential cross sections as expressed by eq.(1).The uncertainties of the extracted spectroscopic factors are from the statistics of the measurements(3%),the uncertainties of the target thickness(5%),the optical potential parameters for both entrance(15%)and exit channels(15%),the geometrical parameters for the bound states(20%),as well as the spectroscopic factor in d(15%).
