A general pre-processing procedure of the measured SAXS patterns for reducing the effect of beam stop and beam stop holder is described. A proper method for automatically choosing the regularization parameter is imple...A general pre-processing procedure of the measured SAXS patterns for reducing the effect of beam stop and beam stop holder is described. A proper method for automatically choosing the regularization parameter is implemented. The method works out on the two-dimensional SAXS patterns. After deblurring, the corresponding two-dimensional patterns will be converted into one-dimensional integrated intensity distribution curves. We tested the program using both calculated artificial data and real experimental data such as polystyrene and poly（methyl methacrylate） latices. The deblurred results are satisfactory showing the effectiveness of the method. The deblurring process of a typical two-dimensional SAXS pattern using the Matlab based program can be completed in few seconds on normal personal computers.展开更多
基金financially supported by the National Natural Science Foundation of China(Nos.21134006 and 51275504)Dutch Polymer Institute(DPI project:779)Science and Technology Development Plane of Jilin(No.20140519007JH)
文摘A general pre-processing procedure of the measured SAXS patterns for reducing the effect of beam stop and beam stop holder is described. A proper method for automatically choosing the regularization parameter is implemented. The method works out on the two-dimensional SAXS patterns. After deblurring, the corresponding two-dimensional patterns will be converted into one-dimensional integrated intensity distribution curves. We tested the program using both calculated artificial data and real experimental data such as polystyrene and poly（methyl methacrylate） latices. The deblurred results are satisfactory showing the effectiveness of the method. The deblurring process of a typical two-dimensional SAXS pattern using the Matlab based program can be completed in few seconds on normal personal computers.
