The crystal structure of the title compound was determined by X-ray diffraction method at room temperature.The crystal belongs to triclinic space group P1 with the following crystallographic parameters:a=13.942(2),b=1...The crystal structure of the title compound was determined by X-ray diffraction method at room temperature.The crystal belongs to triclinic space group P1 with the following crystallographic parameters:a=13.942(2),b=15.540(2),c=10.007(1) A,a=105.16(1)°,β=92.42(1)°,γ=88.12(1)°,V=2090.2(4) Z=4,Dc=1.23g cm-3,F(000)=820,μ(MoKα)=0.74 cm-1,and final R= 0.054 for 3208 observations.Two molecules , which are slightly different in conformation,coexist in an asymmetric unit. Some intermolecular distances are fairly short.The packing arrangement of the molecules in the crystal is also discussed.展开更多
文摘The crystal structure of the title compound was determined by X-ray diffraction method at room temperature.The crystal belongs to triclinic space group P1 with the following crystallographic parameters:a=13.942(2),b=15.540(2),c=10.007(1) A,a=105.16(1)°,β=92.42(1)°,γ=88.12(1)°,V=2090.2(4) Z=4,Dc=1.23g cm-3,F(000)=820,μ(MoKα)=0.74 cm-1,and final R= 0.054 for 3208 observations.Two molecules , which are slightly different in conformation,coexist in an asymmetric unit. Some intermolecular distances are fairly short.The packing arrangement of the molecules in the crystal is also discussed.
