To study the chemical constituents of Hedysarum gmelinii. Methods Theconstituents were separated and purified by different methods of chromatography, and theirstructures were elucidated by DR, MS and NMR. Results Eigh...To study the chemical constituents of Hedysarum gmelinii. Methods Theconstituents were separated and purified by different methods of chromatography, and theirstructures were elucidated by DR, MS and NMR. Results Eight compounds were isolated from Hedysarumgmelinii, including three triteipenoids, two flavonoids and two other compounds. Their structureswere identified as squasapogenol (1), soyasapogenol (2), lupeol (3), 3, 9-dihydroxy coumestan (4),3-hydroxy-9-me-thoxy pterocarpan (5), β-sitosterol (6), palmatic acid (7), and hexadecanoic acid 2,3-dihydroxypropyl ester (8). Conclusion All the compounds have been isolated from this plant forthe first time. Compounds 1 — 4 and 8 were obtained from this genus for the first time. The NMRdata of 1 are reported for the first time.展开更多
The nutritive quality in plant organs is related to the different partitioning patterns of nutrient resources among the organs under various environmental conditions.This study examined the relationship between the nu...The nutritive quality in plant organs is related to the different partitioning patterns of nutrient resources among the organs under various environmental conditions.This study examined the relationship between the nutritive quality of pods and seeds in Zanthoxylum and environmental factors, such as temperature and preciptation by using numerous samples collected from Southwest China to the East China of Shandong peninsula. The increasing accumulations of N, P and C in seeds implied that the nutritive quality in seeds was higher at the regions with relative higher mean annual temperature(MAT) and mean annual precipitation(MAP), while that in pods was on the contrary. By contrast, pod nutritive content was relatively high, but seed nutritive content was relatively low at the regions with relative high MAT and MAP. In addition, C:N ratio in pods was significantly and negatively correlated with MAT and MAP, while that in seed was significantly and positively correlated with MAT and MAP. The partitioning patterns of N-compounds between pods and seeds reflected different nitrogen translocations in the plant organs under various climate condition. The N:P ratios were negatively correlated with MAP, implying a higher proportional allocation of P to seeds than that of N in the areas with a relative high MAP. Therefore, the strategies to assess pod nutritional quality should be taken into accountfor nutritive translocation under various environmental conditions.展开更多
The effect of low methyl pectin, guar and K-carrageenan at concentrations of 1, 2 and 3% and their combinations at concentrations of 2 and 3% on quality attributes and staling of gluten free bread was studied. Among i...The effect of low methyl pectin, guar and K-carrageenan at concentrations of 1, 2 and 3% and their combinations at concentrations of 2 and 3% on quality attributes and staling of gluten free bread was studied. Among investigated samples, control (starch) bread with no added展开更多
Investigations were conducted to establish effects of fermentation and drying on the fermentation index (FI) and cut test of pulp pre-conditioned Ghanaian cocoa beans using a 4 x 3 full factorial experimental design...Investigations were conducted to establish effects of fermentation and drying on the fermentation index (FI) and cut test of pulp pre-conditioned Ghanaian cocoa beans using a 4 x 3 full factorial experimental design with the principal factors being pod storage (0, 3, 7 and 10 d) and fermentation time (0, 3 and 6 d) to study the changes occurring during the fermentation process. The study also used a 4 x 3 full factorial design with pod storage (0, 3, 7 and 10 d) and drying time (0, 3 and 7 d) being the principal factors investigated to study the changes occurring during the drying process. FI and cut test of the beans were studied during fermentation as well as the drying process. FI of the beans increased significantly with pod storage and fermentation but decreased slightly during drying. FI of the unfermented beans increased slightly from 0.674 for the unstored pods to 0.763 after 10 days of pod storage. The FI of the fermented beans (six days fermentation) also increased from 1.390 for the unstored pods to 1.424 for pods stored for 10 days. It decreased from 1.389 at the start of drying for the unstored pods to 1.105 for pods stored for 10 days at the end of drying (seven days). FI of all the beans were however, above 1.0 at the end of fermentation and drying for all pod storage treatments. Cut test revealed that storage of pods for 3, 7 and 10 days increased the percentage of brown beans by 66%, 94% and 72%, respectively, by the sixth day of fermentation. Percentage of brown beans decreased to 61%, 76% and 63%, respectively, for pods stored for 3, 7 and 10 d at the end of drying (seven days). Cocoa pods can be stored for up to 10 days, fermented for six days and dried for seven days with the necessary formation of brown pigments characteristics of well fermented and dried cocoa beans.展开更多
Using Undaria pinnatifida juice and soya bean as main material, glucono delta lactone (GDL) as coagulant, we produced light green and very nourishing Undaria pinnatifida bean curd. Using the single factor experiment...Using Undaria pinnatifida juice and soya bean as main material, glucono delta lactone (GDL) as coagulant, we produced light green and very nourishing Undaria pinnatifida bean curd. Using the single factor experiment to determine the quantity and concentration of Undaria pinnatifida juice milk, process conditions of coagulation is determined by three factors three levels experiment, the best formulation of Undaria pinnatifida tofu is determined by test of four factors and three levels, process conditions are: the addition of Undaria pinnatifida is 20%, soya-bean milk concentration is1:4.5, the amount of GDL is0.30%, solidification time is 15min, solidification temperature is 95 ℃.展开更多
The effect of particle size on the recalcitrance of biochar against oxidation has been regarded as one of the most important factors influencing its stability and transportation in soils. Little is known about the pec...The effect of particle size on the recalcitrance of biochar against oxidation has been regarded as one of the most important factors influencing its stability and transportation in soils. Little is known about the peculiar stability of different particle sizes under chemical oxidation conditions. In this study, several sizes of biochar particles derived from beanpod were produced,and their stabilities were tested by using acid dichromate and hydrogen peroxide. We discovered that the 60-100 mesh size of particles produced at 400 and 500 ℃ showed the least carbon loss under the oxidation of both dichromate and hydrogen peroxide. In addition, this particle size also shows great stability at 600 and 700 ℃, but this stability was not observed below 300 °C for all temperature-dependent biochars. Medium-sized particles composed of exclusively heterogeneous components produced a biochar at temperatures over 400 ℃ with comparatively stronger chemical anti-oxidation characteristics. The chemical recalcitrance of biochar should be reevaluated based on particle size before soil application.展开更多
[Objective] The aim was to optimize the appropriate solid state fermentation(SSF)conditions.[Method] The optimization of solid state fermentation using a mixture substrate of bean curd residue and the marc with Bacill...[Objective] The aim was to optimize the appropriate solid state fermentation(SSF)conditions.[Method] The optimization of solid state fermentation using a mixture substrate of bean curd residue and the marc with Bacillus natto was developed.[Result] The best fermentation condition optimized by the test of single factor and the orthogonal design respectively was mixing ratio of bean curd residue to marc 2∶1,substrate pH value 6,fermentation temperature 39 ℃,inoculum volume 10% and fermentation time 48 h.Under this optimized fermentation condition,the content of crude fiber in the substrate decreased from 107.8 mg/g before SSF to 56.2 mg/g after SSF,and the degeneration rate of crude fiber was 47.87%.[Conclusion] The bean curd residue in its palatability was enormously improved by SSF with Bacillus natto strain,which could be expected to be widely used as raw material of health foodstuff.展开更多
Background: Birch pollen sensitization and associated pollen-food syndrome among Chinese allergic patients have not been investigated. Methods: Sera from 203 allergic patients from the northern part of China and col...Background: Birch pollen sensitization and associated pollen-food syndrome among Chinese allergic patients have not been investigated. Methods: Sera from 203 allergic patients from the northern part of China and collected during February to July 2014 were investigated. Specific immunoglobulin E (IgE) against birch pollen extract Bet v and major birch pollen allergen Bet v 1 were measured using the ADVIA Centaur. The presence of major apple allergen Mal d 1 and soy bean allergen Gly m 4 specific IgE was measured by ImmunoCAP 100. Results: Among the 203 sere, 34 sera (16.7%) had specific IgE to Bet v and of these, 28 sere (82.4%) contained Bet v 1-specific IgE. Among the 28 sera with Bet v 1-specific IgE, 27 sera (96.4%) contained Mal d 1-specific IgE and 22 sera (78.6%) contained Gly m 4-specific igE. Of the 34 Bet v-positive sera, 6 sera (17.6%) contained no specific IgE for Bet v 1, Mal d 1, or Gly m 4. Almost all Bet v-positive sera were donated during the birch pollen season. Conclusions: The prevalence of birch allergy among patients visiting health care during pollen season can be as high as 16.7% in Tangshan City. The majority of Chinese birch allergic patients are IgE-sensitized to the major birch pollen allergen Bet v 1 as well as to the major apple allergen Mal d 1 and soy bean allergen Gly m 4. A relatively high number of patients (17.6%) are IgE-sensitized to birch pollen allergen(s) other than Bet v 1. The high prevalence of specific IgE to Mal d 1 and Gly m 4 among Bet v 1-sensitized patients indicates that pollen-food allergy syndrome could be of clinical relevance in China.展开更多
In this research, some of site and silvicultural characteristics of Yew stand in northern forests of Iran was studied. For this purpose, compartment number 16 of district 4 Shir-ghalaye was selected. According to rese...In this research, some of site and silvicultural characteristics of Yew stand in northern forests of Iran was studied. For this purpose, compartment number 16 of district 4 Shir-ghalaye was selected. According to research purposes, stands with an area of 20 ha were chosen in center of the compartment and was separated from map. Due to restricted area of region and according to few number of Yew trees in the stand, the full-callipering method was conducted for measuring quantitative and qualitative characteristics. In the stand diameter at breast height (D.B.H.), height and canopy diameter of all Yew trees were measured. The results showed that the diameter distribution curve and height distribution curve of Yew trees were similar to even-age forests curve. But according to average annual increment, mixture type of Yew trees in stand, diameter distribution of other species and low rate regeneration of Yew, it can be concluded that the studied Yew stand, is an uneven-age stand and because of low rate regeneration in previous years the number of young Yew trees were reduced and even-age forest curve was formed subsequently. The maximum height and diameter of Yew trees were recorded 26.8 m and 112 cm, respectively. Also, the number of trees per hectare and basal area per hectare of Yew trees were calculated 14.55 and 3.23 m2 respectively.展开更多
基金National Natural Science Foundation of China (20432030)
文摘To study the chemical constituents of Hedysarum gmelinii. Methods Theconstituents were separated and purified by different methods of chromatography, and theirstructures were elucidated by DR, MS and NMR. Results Eight compounds were isolated from Hedysarumgmelinii, including three triteipenoids, two flavonoids and two other compounds. Their structureswere identified as squasapogenol (1), soyasapogenol (2), lupeol (3), 3, 9-dihydroxy coumestan (4),3-hydroxy-9-me-thoxy pterocarpan (5), β-sitosterol (6), palmatic acid (7), and hexadecanoic acid 2,3-dihydroxypropyl ester (8). Conclusion All the compounds have been isolated from this plant forthe first time. Compounds 1 — 4 and 8 were obtained from this genus for the first time. The NMRdata of 1 are reported for the first time.
基金supported by the National Key R&D Program of China Grant 2016YFA0601002National Natural Science Foundation of China(Grant Nos.41571130072)(S-L Li)
文摘The nutritive quality in plant organs is related to the different partitioning patterns of nutrient resources among the organs under various environmental conditions.This study examined the relationship between the nutritive quality of pods and seeds in Zanthoxylum and environmental factors, such as temperature and preciptation by using numerous samples collected from Southwest China to the East China of Shandong peninsula. The increasing accumulations of N, P and C in seeds implied that the nutritive quality in seeds was higher at the regions with relative higher mean annual temperature(MAT) and mean annual precipitation(MAP), while that in pods was on the contrary. By contrast, pod nutritive content was relatively high, but seed nutritive content was relatively low at the regions with relative high MAT and MAP. In addition, C:N ratio in pods was significantly and negatively correlated with MAT and MAP, while that in seed was significantly and positively correlated with MAT and MAP. The partitioning patterns of N-compounds between pods and seeds reflected different nitrogen translocations in the plant organs under various climate condition. The N:P ratios were negatively correlated with MAP, implying a higher proportional allocation of P to seeds than that of N in the areas with a relative high MAP. Therefore, the strategies to assess pod nutritional quality should be taken into accountfor nutritive translocation under various environmental conditions.
文摘The effect of low methyl pectin, guar and K-carrageenan at concentrations of 1, 2 and 3% and their combinations at concentrations of 2 and 3% on quality attributes and staling of gluten free bread was studied. Among investigated samples, control (starch) bread with no added
文摘Investigations were conducted to establish effects of fermentation and drying on the fermentation index (FI) and cut test of pulp pre-conditioned Ghanaian cocoa beans using a 4 x 3 full factorial experimental design with the principal factors being pod storage (0, 3, 7 and 10 d) and fermentation time (0, 3 and 6 d) to study the changes occurring during the fermentation process. The study also used a 4 x 3 full factorial design with pod storage (0, 3, 7 and 10 d) and drying time (0, 3 and 7 d) being the principal factors investigated to study the changes occurring during the drying process. FI and cut test of the beans were studied during fermentation as well as the drying process. FI of the beans increased significantly with pod storage and fermentation but decreased slightly during drying. FI of the unfermented beans increased slightly from 0.674 for the unstored pods to 0.763 after 10 days of pod storage. The FI of the fermented beans (six days fermentation) also increased from 1.390 for the unstored pods to 1.424 for pods stored for 10 days. It decreased from 1.389 at the start of drying for the unstored pods to 1.105 for pods stored for 10 days at the end of drying (seven days). FI of all the beans were however, above 1.0 at the end of fermentation and drying for all pod storage treatments. Cut test revealed that storage of pods for 3, 7 and 10 days increased the percentage of brown beans by 66%, 94% and 72%, respectively, by the sixth day of fermentation. Percentage of brown beans decreased to 61%, 76% and 63%, respectively, for pods stored for 3, 7 and 10 d at the end of drying (seven days). Cocoa pods can be stored for up to 10 days, fermented for six days and dried for seven days with the necessary formation of brown pigments characteristics of well fermented and dried cocoa beans.
文摘Using Undaria pinnatifida juice and soya bean as main material, glucono delta lactone (GDL) as coagulant, we produced light green and very nourishing Undaria pinnatifida bean curd. Using the single factor experiment to determine the quantity and concentration of Undaria pinnatifida juice milk, process conditions of coagulation is determined by three factors three levels experiment, the best formulation of Undaria pinnatifida tofu is determined by test of four factors and three levels, process conditions are: the addition of Undaria pinnatifida is 20%, soya-bean milk concentration is1:4.5, the amount of GDL is0.30%, solidification time is 15min, solidification temperature is 95 ℃.
基金Supported by the Provincial Basic Research Program of Hebei Education Department(ZD2015110)the National Special Project on Key Technologies and Demonstration of Wetland Ecological Restoration in the Haihe River Basin(2014ZX07203008)the Fund of the University of Hebei Engineering(Grants 20120169)
文摘The effect of particle size on the recalcitrance of biochar against oxidation has been regarded as one of the most important factors influencing its stability and transportation in soils. Little is known about the peculiar stability of different particle sizes under chemical oxidation conditions. In this study, several sizes of biochar particles derived from beanpod were produced,and their stabilities were tested by using acid dichromate and hydrogen peroxide. We discovered that the 60-100 mesh size of particles produced at 400 and 500 ℃ showed the least carbon loss under the oxidation of both dichromate and hydrogen peroxide. In addition, this particle size also shows great stability at 600 and 700 ℃, but this stability was not observed below 300 °C for all temperature-dependent biochars. Medium-sized particles composed of exclusively heterogeneous components produced a biochar at temperatures over 400 ℃ with comparatively stronger chemical anti-oxidation characteristics. The chemical recalcitrance of biochar should be reevaluated based on particle size before soil application.
文摘[Objective] The aim was to optimize the appropriate solid state fermentation(SSF)conditions.[Method] The optimization of solid state fermentation using a mixture substrate of bean curd residue and the marc with Bacillus natto was developed.[Result] The best fermentation condition optimized by the test of single factor and the orthogonal design respectively was mixing ratio of bean curd residue to marc 2∶1,substrate pH value 6,fermentation temperature 39 ℃,inoculum volume 10% and fermentation time 48 h.Under this optimized fermentation condition,the content of crude fiber in the substrate decreased from 107.8 mg/g before SSF to 56.2 mg/g after SSF,and the degeneration rate of crude fiber was 47.87%.[Conclusion] The bean curd residue in its palatability was enormously improved by SSF with Bacillus natto strain,which could be expected to be widely used as raw material of health foodstuff.
文摘Background: Birch pollen sensitization and associated pollen-food syndrome among Chinese allergic patients have not been investigated. Methods: Sera from 203 allergic patients from the northern part of China and collected during February to July 2014 were investigated. Specific immunoglobulin E (IgE) against birch pollen extract Bet v and major birch pollen allergen Bet v 1 were measured using the ADVIA Centaur. The presence of major apple allergen Mal d 1 and soy bean allergen Gly m 4 specific IgE was measured by ImmunoCAP 100. Results: Among the 203 sere, 34 sera (16.7%) had specific IgE to Bet v and of these, 28 sere (82.4%) contained Bet v 1-specific IgE. Among the 28 sera with Bet v 1-specific IgE, 27 sera (96.4%) contained Mal d 1-specific IgE and 22 sera (78.6%) contained Gly m 4-specific igE. Of the 34 Bet v-positive sera, 6 sera (17.6%) contained no specific IgE for Bet v 1, Mal d 1, or Gly m 4. Almost all Bet v-positive sera were donated during the birch pollen season. Conclusions: The prevalence of birch allergy among patients visiting health care during pollen season can be as high as 16.7% in Tangshan City. The majority of Chinese birch allergic patients are IgE-sensitized to the major birch pollen allergen Bet v 1 as well as to the major apple allergen Mal d 1 and soy bean allergen Gly m 4. A relatively high number of patients (17.6%) are IgE-sensitized to birch pollen allergen(s) other than Bet v 1. The high prevalence of specific IgE to Mal d 1 and Gly m 4 among Bet v 1-sensitized patients indicates that pollen-food allergy syndrome could be of clinical relevance in China.
文摘In this research, some of site and silvicultural characteristics of Yew stand in northern forests of Iran was studied. For this purpose, compartment number 16 of district 4 Shir-ghalaye was selected. According to research purposes, stands with an area of 20 ha were chosen in center of the compartment and was separated from map. Due to restricted area of region and according to few number of Yew trees in the stand, the full-callipering method was conducted for measuring quantitative and qualitative characteristics. In the stand diameter at breast height (D.B.H.), height and canopy diameter of all Yew trees were measured. The results showed that the diameter distribution curve and height distribution curve of Yew trees were similar to even-age forests curve. But according to average annual increment, mixture type of Yew trees in stand, diameter distribution of other species and low rate regeneration of Yew, it can be concluded that the studied Yew stand, is an uneven-age stand and because of low rate regeneration in previous years the number of young Yew trees were reduced and even-age forest curve was formed subsequently. The maximum height and diameter of Yew trees were recorded 26.8 m and 112 cm, respectively. Also, the number of trees per hectare and basal area per hectare of Yew trees were calculated 14.55 and 3.23 m2 respectively.