A rapid method to determine glutamic acid (Glu) in cerebrospinal fluid (CSF) by capillaryelectrophoresis with high frequency conductivity detection (contactless conductivity detection) wasdescribed. The CSF sample was...A rapid method to determine glutamic acid (Glu) in cerebrospinal fluid (CSF) by capillaryelectrophoresis with high frequency conductivity detection (contactless conductivity detection) wasdescribed. The CSF sample was pretreated with silver cation resin to remove high concentration ofCl- ions in CSF. The separation was achieved in the buffer solution of 10 mmol/L Tris and 8mmol/L boric acid at the separation voltage of 20.0 kV. Glu showed linear response in the range of5.0×10-6 to 6.0×10-3 mol/L, the limit of detection was 1.0×10-6 mol/L. The method was used foranalysis Glu in CSF satisfactorily with a recovery of 97.8-98.8%.展开更多
In order to obtain accurate real-time soil moisture data and the spatial distribution of soil moisture,the soil moisture measurement methods based on high-frequency capacitance edge field effect were analyzed,the stru...In order to obtain accurate real-time soil moisture data and the spatial distribution of soil moisture,the soil moisture measurement methods based on high-frequency capacitance edge field effect were analyzed,the structure of probe was studied,and a multi-channel soil moisture sensor was designed.Moreover,with the established two-dimensional trace planar capacitance probe model and the method of the finite element analysis,relationship between the structure of sensor probe and electric field intensity was studied and capacitance of the probe trace amount planar capacitance model was analyzed,the most optimal structure of sensor probe was determined.Design parameters of the probe which can achieve optimal sensitivity and detection range are:outer diameter 40 mm and inner diameter 38.4 mm for the probe copper ring electrode,axial length 20 mm and axial spacing 10 mm.The sensor is suitable for measuring the moisture of different type of soil.Moreover,the features of the profile soil moisture sensor were experimentally explored.The measurement accuracy reached±1.31%with better stability and consistency.Sensor probes can be assembled according to the measurement depth and used to measure soil moisture of different crop root zone.展开更多
基金This project was supported by the Guangdong Provincial Foundation of Natural Science(021808)
文摘A rapid method to determine glutamic acid (Glu) in cerebrospinal fluid (CSF) by capillaryelectrophoresis with high frequency conductivity detection (contactless conductivity detection) wasdescribed. The CSF sample was pretreated with silver cation resin to remove high concentration ofCl- ions in CSF. The separation was achieved in the buffer solution of 10 mmol/L Tris and 8mmol/L boric acid at the separation voltage of 20.0 kV. Glu showed linear response in the range of5.0×10-6 to 6.0×10-3 mol/L, the limit of detection was 1.0×10-6 mol/L. The method was used foranalysis Glu in CSF satisfactorily with a recovery of 97.8-98.8%.
基金We thank Beijing Natural Science Foundation(6142011)for supporting this research.
文摘In order to obtain accurate real-time soil moisture data and the spatial distribution of soil moisture,the soil moisture measurement methods based on high-frequency capacitance edge field effect were analyzed,the structure of probe was studied,and a multi-channel soil moisture sensor was designed.Moreover,with the established two-dimensional trace planar capacitance probe model and the method of the finite element analysis,relationship between the structure of sensor probe and electric field intensity was studied and capacitance of the probe trace amount planar capacitance model was analyzed,the most optimal structure of sensor probe was determined.Design parameters of the probe which can achieve optimal sensitivity and detection range are:outer diameter 40 mm and inner diameter 38.4 mm for the probe copper ring electrode,axial length 20 mm and axial spacing 10 mm.The sensor is suitable for measuring the moisture of different type of soil.Moreover,the features of the profile soil moisture sensor were experimentally explored.The measurement accuracy reached±1.31%with better stability and consistency.Sensor probes can be assembled according to the measurement depth and used to measure soil moisture of different crop root zone.
