To search for new and bioactive minor components from traditional Chinese medicines, a new compound, named jujuphenoside (1), was isolated from the seeds of Ziziphusjujuba var. spinosa (Bunge)Hu. The structure of juju...To search for new and bioactive minor components from traditional Chinese medicines, a new compound, named jujuphenoside (1), was isolated from the seeds of Ziziphusjujuba var. spinosa (Bunge)Hu. The structure of jujuphenoside was elucidated by spectral and chemical methods, particularly twodimensional nuclear magnetic resonance analysis. Together with the new compound, 22 known compounds were also isolated and identified from the seeds of Z. jujuba var. spinosa, among which, epiceanothic acid (2) was first obtained from natural resources, whereas compounds 7-16 were first obtained from this plant.展开更多
Using ultradry method and accelerated aging, storage behavior of Ziziphus jujuba var spinosa seeds with MC of 15-80 g/kg was studied. The results showed that seeds with MC of 24-80 g/kg could maintain the stabilizatio...Using ultradry method and accelerated aging, storage behavior of Ziziphus jujuba var spinosa seeds with MC of 15-80 g/kg was studied. The results showed that seeds with MC of 24-80 g/kg could maintain the stabilization in germination percentage, vigor, relative conductivity, and enzyme activities; and during the ageing the seed storability increased with the moisture content decreased to 24 g/kg. Thus, it was feasible for the seeds to be stored under the ultra-dried condition.展开更多
A simple, reproducible and reliable HPLC fingerprint analysis method of Ziziphi Spinosae Semen(ZSS) and Ziziphi Mauritianae Semen(ZMS) was established, and then it was applied to analyze samples collected from differe...A simple, reproducible and reliable HPLC fingerprint analysis method of Ziziphi Spinosae Semen(ZSS) and Ziziphi Mauritianae Semen(ZMS) was established, and then it was applied to analyze samples collected from different locations. A total of 12 common fingerprint peaks were designated in ZSS and ZMS, respectively, and five of which were definitely identified. Of these common peaks, 10 peaks were presented in both ZSS and ZMS, whereas two were characteristic for ZSS and ZMS, respectively. Furthermore, the two characteristic peaks of ZMS were definitely assigned as 6′′′-sinapoylspinosin and frangufoline by HPLC guided purification and structural elucidation. The HPLC fingerprint analysis was proved to be useful in identifying and discriminating ZSS and ZMS, which was beneficial for quality control of ZSS and its products.展开更多
文摘To search for new and bioactive minor components from traditional Chinese medicines, a new compound, named jujuphenoside (1), was isolated from the seeds of Ziziphusjujuba var. spinosa (Bunge)Hu. The structure of jujuphenoside was elucidated by spectral and chemical methods, particularly twodimensional nuclear magnetic resonance analysis. Together with the new compound, 22 known compounds were also isolated and identified from the seeds of Z. jujuba var. spinosa, among which, epiceanothic acid (2) was first obtained from natural resources, whereas compounds 7-16 were first obtained from this plant.
基金foundation projects and is supported by the National Key Project of Scientific and Technical Supporting Programs of China ( No.2006BAD09B06 and 2006BAD03A0308)the "948" Program of the Ministry of Water Resources of China( No. 200207)
文摘Using ultradry method and accelerated aging, storage behavior of Ziziphus jujuba var spinosa seeds with MC of 15-80 g/kg was studied. The results showed that seeds with MC of 24-80 g/kg could maintain the stabilization in germination percentage, vigor, relative conductivity, and enzyme activities; and during the ageing the seed storability increased with the moisture content decreased to 24 g/kg. Thus, it was feasible for the seeds to be stored under the ultra-dried condition.
基金National Project for Standardization of Chinese Material Medica(Grant No.ZYBZH-Y-JIN-34).
文摘A simple, reproducible and reliable HPLC fingerprint analysis method of Ziziphi Spinosae Semen(ZSS) and Ziziphi Mauritianae Semen(ZMS) was established, and then it was applied to analyze samples collected from different locations. A total of 12 common fingerprint peaks were designated in ZSS and ZMS, respectively, and five of which were definitely identified. Of these common peaks, 10 peaks were presented in both ZSS and ZMS, whereas two were characteristic for ZSS and ZMS, respectively. Furthermore, the two characteristic peaks of ZMS were definitely assigned as 6′′′-sinapoylspinosin and frangufoline by HPLC guided purification and structural elucidation. The HPLC fingerprint analysis was proved to be useful in identifying and discriminating ZSS and ZMS, which was beneficial for quality control of ZSS and its products.
