Fatigue crack propagation rate,da/dN,and threshold stress intensity range,ΔK_(th),of steel 20CrMnMo containing low carbon martensite or low carbon martensite/bainite(LCM/B) duplex structure,obtained by oil quenching ...Fatigue crack propagation rate,da/dN,and threshold stress intensity range,ΔK_(th),of steel 20CrMnMo containing low carbon martensite or low carbon martensite/bainite(LCM/B) duplex structure,obtained by oil quenching and austempered at 360℃,have been measured using specimens under four-point bending.Observation was also made of the crack path and fracture morphology with relation to microstructure.The formation of LCM/B duplex structure,which caused by 20% lower bainite after short-time isothermal treatment,may re- markably increase ΔK_(th)and considerably decrease da/dN.The effect of microstructure on da/dN and ΔK_(th)was discussed with the emphasis on the crack propagation path.展开更多
Determination was carried out of fatigue crack propagation rate of steel 65Cr5Mo3W2VSiTi (LM2)with various bainite contents and M/B duplex structure tempered at various tempera- tures.The threshold value of fatigue fo...Determination was carried out of fatigue crack propagation rate of steel 65Cr5Mo3W2VSiTi (LM2)with various bainite contents and M/B duplex structure tempered at various tempera- tures.The threshold value of fatigue for each processing was estimated by experimental data. The mechanism for fatigue crack propagation of M/B duplex structure in steel LM2 seems to be non-continuous.The calculated fatigue crack micro-propagation rates are found to agree with the experimental data.展开更多
The microstructural evolutions of the cold rolled Fe-0.1C-5Mn steel during intercritical annealing were ex- amined using combined advanced techniques. It was demonstrated that intercritical annealing results in an ult...The microstructural evolutions of the cold rolled Fe-0.1C-5Mn steel during intercritical annealing were ex- amined using combined advanced techniques. It was demonstrated that intercritical annealing results in an ultrafine granular ferrite and austenite duplex structure in cold rolled 0.1C-5Mn steel. The strong partitioning of manganese and carbon elements from ferrite to austenite was found during intercritical annealing by scanning transmission elec- tron microscopy (STEM) and X-ray diffraction (XRD). Strong effects of boundary characters on the austenite for- mation were indicated by austenite fast nucleation and growth in the high angle boundaries but sluggish nucleation and growth in the low angle boundaries. The ultrafine grained duplex structure in 0.1C-5Mn was resulted from the the sluggish Mn-diffusion and the extra high Gibbs free energy of ferrite phase. Based on the analysis of the micro- structure evolution, it was pointed out that the intercritical annealing of the medium Mn steels could be applied to fabricate an ultrafine duplex grained microstructure, which would be a promising approach to develop the 3rd genera- tion austomobile steels with excellent combination of strength and ductility.展开更多
Duplex nanoporous Cu was successfully fabricated by dealloying a dual-phase Mg-Cu precursor alloy consisting of intermetallic Mg2Cu and MgCu2.The duplex nanoporous Cu with embedded nanoporous struts exhibited highly e...Duplex nanoporous Cu was successfully fabricated by dealloying a dual-phase Mg-Cu precursor alloy consisting of intermetallic Mg2Cu and MgCu2.The duplex nanoporous Cu with embedded nanoporous struts exhibited highly enhanced strength compared to the typical monolithic nanoporous Cu under both compressive and flexural test conditions at room temperature;the duplex np-Cu sample exhibited a 12 times higher compressive strength and a 40 times greater flexural strength than the monolithic np-Cu sample.Factors responsible for the strength enhancement in the duplex nanoporous Cu are discussed.展开更多
Lying at the junction of the Dabashan, Longmenshan and Qinling mountains, the Micangshan Orogenic Belt coupled with a basin is a duplex structure and back-thrust triangular belt with little horizontal displacement, sm...Lying at the junction of the Dabashan, Longmenshan and Qinling mountains, the Micangshan Orogenic Belt coupled with a basin is a duplex structure and back-thrust triangular belt with little horizontal displacement, small thrust faults and continuous sedimentary cover. On the basis of 3D seismic data, and through sedimentary and structural research, the Micangshan foreland can be divided into five subbelts, which from north to south are: basement thrust, frontal thrust, foreland depression-back-thrust triangle, foreland fold belt or anticline belt, and the Tongjiang Depression. Along the direction of strike from west to east, the arcuate structural belt of Micangshan can be divided into west, middle and east segments. During the collision between the Qinling and Yangtze plates, the Micangshan Orogenic Belt was subjected to the interaction of three rigid terranes: Bikou, Foping, and Fenghuangshan (a.k.a. Ziyang) terranes. The collision processes of rigid terranes controlled the structural development of the Micangshan foreland, which are: (a) the former collision between the Micangshan-Hannan and Bikou terranes forming the earlier rudiments of the structure; and (b) the later collision forming the main body of the structural belt. The formation processes of the Micangshan Orogenic Belt can be divided into four stages: (1) in the early stage of the Indosinian movement, the Micangshan-Hannan Rigid Terrane was jointed to the Qinling Plate by the clockwise subduction of the Yangtze Plate toward the Qinling Plate; (2) since the late Triassic, the earlier rudiments of the Tongnanba and Jiulongshan anticlines and corresponding syncline were formed by compression from different directions of the Bikou, Foping and Micangshan-Hannan terranes; (3) in the early stage of the Himalayan movement, the Micangshan-Hannan Terrane formed the Micangshan Nappe torwards the foreland basin and the compression stresses were mainly concentrated along both its flanks, whereas the Micangshan-Hannan Terrane wedged into the Qinling Orogenic Belt with force; (4) in the late stage of the Himalayan movement, the main collision of the Qinling Plate made the old basement rocks of the terrane uplift quickly, to form the Micangshan Orogenic Belt. The Micangshan foreland arcuate structure was formed due to the non-homogeneity of terrane movement.展开更多
In this study, the effect of temperatures and cooling rates of heat treatment on the microstructure of a powder metallurgy (PM) Ti-46Al-2Cr-2Nb-(B,W) (at.%) alloy was studied. Depending on the cooling rate and tempera...In this study, the effect of temperatures and cooling rates of heat treatment on the microstructure of a powder metallurgy (PM) Ti-46Al-2Cr-2Nb-(B,W) (at.%) alloy was studied. Depending on the cooling rate and temperature, the different structures were obtained from the initial near-γ (NG) microstructures by heat treatment in the α+γ field. The results show that the microstructures of samples after furnace cooling (FC) consist primarily of equiaxed γ and α 2 grains, with a few grains containing lamellae. Duplex microstructures consist mainly of γ grains and lamellar colonies were obtained in the quenching into another furnace at 900°C (QFC) samples. However, further increasing of the cooling rate to air cooling (AC) induces the transformation of α→α_2 and results in a microstructure with equiaxed γ and α_2 grains, and no lamellar colonies are found.展开更多
To evaluate the residual stress in TiAl based alloys by X ray diffraction, X ray elastic constants (REC) of a γ TiAl alloy were determined. From these results, the stress state of a given phase in a duplex TiAl based...To evaluate the residual stress in TiAl based alloys by X ray diffraction, X ray elastic constants (REC) of a γ TiAl alloy were determined. From these results, the stress state of a given phase in a duplex TiAl based alloy under a uniaxial tensile loading has been characterized by X ray diffraction. The results show that the X ray elastic constants and the microscopic stresses of the given phase are different from the apparent elastic constants and the macroscopic stresses of the alloy. The reason of the different distribution of the alloy was also discussed. [展开更多
Microstructure evolution during ART-annealing (austenite reverted transformation annealing) of 0.2C-5Mn steel processed by austenitation at different temperatures was examined by SEM, TEM and XRD. It was demonstrate...Microstructure evolution during ART-annealing (austenite reverted transformation annealing) of 0.2C-5Mn steel processed by austenitation at different temperatures was examined by SEM, TEM and XRD. It was demonstrated that the initial mi- crostructures resulted from austenization at different temperatures strongly affect the microstructure evolution during followed ART-annealing, even the ultrafine grained ferrite/austenite duplex structure with about 30% austenite could be obtained af- ter long time ART-annealing in all cases. Austenization in the intercritical region (between Ad and At3) gave a duplex structure after quenching, which was nearly not affected by followed annealing process. However, high temperature austenization (above A^3) resulted in a full martensite structure after quenching, which gradually transformed into a ferrite/austenite duplex structure during the following anneal- ing process. Based on the analysis of austenite fraction and carbon concentrate, it was found that not only carbon partitioning but also manganese paxtitioning in the austenite affected the stability of austenite and even dominated the development of lamellar ferrite and austenite duplex structure during intercritical annealing with different times. At last an austenite lath nucleation and thickening model was pro- posed to describe the microstructure evolution of medium mangenese steel during ART-annealing.展开更多
文摘Fatigue crack propagation rate,da/dN,and threshold stress intensity range,ΔK_(th),of steel 20CrMnMo containing low carbon martensite or low carbon martensite/bainite(LCM/B) duplex structure,obtained by oil quenching and austempered at 360℃,have been measured using specimens under four-point bending.Observation was also made of the crack path and fracture morphology with relation to microstructure.The formation of LCM/B duplex structure,which caused by 20% lower bainite after short-time isothermal treatment,may re- markably increase ΔK_(th)and considerably decrease da/dN.The effect of microstructure on da/dN and ΔK_(th)was discussed with the emphasis on the crack propagation path.
文摘Determination was carried out of fatigue crack propagation rate of steel 65Cr5Mo3W2VSiTi (LM2)with various bainite contents and M/B duplex structure tempered at various tempera- tures.The threshold value of fatigue for each processing was estimated by experimental data. The mechanism for fatigue crack propagation of M/B duplex structure in steel LM2 seems to be non-continuous.The calculated fatigue crack micro-propagation rates are found to agree with the experimental data.
基金Item Sponsored by National Natural Science Foundation of China(51371057)National Basic Research Program of China(2010CB630803)
文摘The microstructural evolutions of the cold rolled Fe-0.1C-5Mn steel during intercritical annealing were ex- amined using combined advanced techniques. It was demonstrated that intercritical annealing results in an ultrafine granular ferrite and austenite duplex structure in cold rolled 0.1C-5Mn steel. The strong partitioning of manganese and carbon elements from ferrite to austenite was found during intercritical annealing by scanning transmission elec- tron microscopy (STEM) and X-ray diffraction (XRD). Strong effects of boundary characters on the austenite for- mation were indicated by austenite fast nucleation and growth in the high angle boundaries but sluggish nucleation and growth in the low angle boundaries. The ultrafine grained duplex structure in 0.1C-5Mn was resulted from the the sluggish Mn-diffusion and the extra high Gibbs free energy of ferrite phase. Based on the analysis of the micro- structure evolution, it was pointed out that the intercritical annealing of the medium Mn steels could be applied to fabricate an ultrafine duplex grained microstructure, which would be a promising approach to develop the 3rd genera- tion austomobile steels with excellent combination of strength and ductility.
基金the National Research Foundation of Korea(NRF)grant funded by the Korea government(MSIT)(No.2019R1A2C1003905).
文摘Duplex nanoporous Cu was successfully fabricated by dealloying a dual-phase Mg-Cu precursor alloy consisting of intermetallic Mg2Cu and MgCu2.The duplex nanoporous Cu with embedded nanoporous struts exhibited highly enhanced strength compared to the typical monolithic nanoporous Cu under both compressive and flexural test conditions at room temperature;the duplex np-Cu sample exhibited a 12 times higher compressive strength and a 40 times greater flexural strength than the monolithic np-Cu sample.Factors responsible for the strength enhancement in the duplex nanoporous Cu are discussed.
基金These research results are part of a key project carried out in 2005-2007 and financially supported by the Natural Science Foundation of China (No.40472110).
文摘Lying at the junction of the Dabashan, Longmenshan and Qinling mountains, the Micangshan Orogenic Belt coupled with a basin is a duplex structure and back-thrust triangular belt with little horizontal displacement, small thrust faults and continuous sedimentary cover. On the basis of 3D seismic data, and through sedimentary and structural research, the Micangshan foreland can be divided into five subbelts, which from north to south are: basement thrust, frontal thrust, foreland depression-back-thrust triangle, foreland fold belt or anticline belt, and the Tongjiang Depression. Along the direction of strike from west to east, the arcuate structural belt of Micangshan can be divided into west, middle and east segments. During the collision between the Qinling and Yangtze plates, the Micangshan Orogenic Belt was subjected to the interaction of three rigid terranes: Bikou, Foping, and Fenghuangshan (a.k.a. Ziyang) terranes. The collision processes of rigid terranes controlled the structural development of the Micangshan foreland, which are: (a) the former collision between the Micangshan-Hannan and Bikou terranes forming the earlier rudiments of the structure; and (b) the later collision forming the main body of the structural belt. The formation processes of the Micangshan Orogenic Belt can be divided into four stages: (1) in the early stage of the Indosinian movement, the Micangshan-Hannan Rigid Terrane was jointed to the Qinling Plate by the clockwise subduction of the Yangtze Plate toward the Qinling Plate; (2) since the late Triassic, the earlier rudiments of the Tongnanba and Jiulongshan anticlines and corresponding syncline were formed by compression from different directions of the Bikou, Foping and Micangshan-Hannan terranes; (3) in the early stage of the Himalayan movement, the Micangshan-Hannan Terrane formed the Micangshan Nappe torwards the foreland basin and the compression stresses were mainly concentrated along both its flanks, whereas the Micangshan-Hannan Terrane wedged into the Qinling Orogenic Belt with force; (4) in the late stage of the Himalayan movement, the main collision of the Qinling Plate made the old basement rocks of the terrane uplift quickly, to form the Micangshan Orogenic Belt. The Micangshan foreland arcuate structure was formed due to the non-homogeneity of terrane movement.
基金supported by the National Natural Science Foundation of China (No. 51101003)
文摘In this study, the effect of temperatures and cooling rates of heat treatment on the microstructure of a powder metallurgy (PM) Ti-46Al-2Cr-2Nb-(B,W) (at.%) alloy was studied. Depending on the cooling rate and temperature, the different structures were obtained from the initial near-γ (NG) microstructures by heat treatment in the α+γ field. The results show that the microstructures of samples after furnace cooling (FC) consist primarily of equiaxed γ and α 2 grains, with a few grains containing lamellae. Duplex microstructures consist mainly of γ grains and lamellar colonies were obtained in the quenching into another furnace at 900°C (QFC) samples. However, further increasing of the cooling rate to air cooling (AC) induces the transformation of α→α_2 and results in a microstructure with equiaxed γ and α_2 grains, and no lamellar colonies are found.
文摘To evaluate the residual stress in TiAl based alloys by X ray diffraction, X ray elastic constants (REC) of a γ TiAl alloy were determined. From these results, the stress state of a given phase in a duplex TiAl based alloy under a uniaxial tensile loading has been characterized by X ray diffraction. The results show that the X ray elastic constants and the microscopic stresses of the given phase are different from the apparent elastic constants and the macroscopic stresses of the alloy. The reason of the different distribution of the alloy was also discussed. [
基金supported by National Basic Research Program of China(No.G2010CB630803) National High Technical Research and Development Programme of China (Nos.2009AA03Z519 and 2009AA033401)
文摘Microstructure evolution during ART-annealing (austenite reverted transformation annealing) of 0.2C-5Mn steel processed by austenitation at different temperatures was examined by SEM, TEM and XRD. It was demonstrated that the initial mi- crostructures resulted from austenization at different temperatures strongly affect the microstructure evolution during followed ART-annealing, even the ultrafine grained ferrite/austenite duplex structure with about 30% austenite could be obtained af- ter long time ART-annealing in all cases. Austenization in the intercritical region (between Ad and At3) gave a duplex structure after quenching, which was nearly not affected by followed annealing process. However, high temperature austenization (above A^3) resulted in a full martensite structure after quenching, which gradually transformed into a ferrite/austenite duplex structure during the following anneal- ing process. Based on the analysis of austenite fraction and carbon concentrate, it was found that not only carbon partitioning but also manganese paxtitioning in the austenite affected the stability of austenite and even dominated the development of lamellar ferrite and austenite duplex structure during intercritical annealing with different times. At last an austenite lath nucleation and thickening model was pro- posed to describe the microstructure evolution of medium mangenese steel during ART-annealing.