The main agronomic traits,economic traits,appearance quality,main chemical components,gas composition and physical parameters of 10 flue cured tobacco varieties were investigated in the experiment.And the field natura...The main agronomic traits,economic traits,appearance quality,main chemical components,gas composition and physical parameters of 10 flue cured tobacco varieties were investigated in the experiment.And the field natural incidence of the main diseases was investigated.The results showed that main agronomic characters of the 10 varieties were in line with the breeding objectives,among which 5 varieties have good economic characters;5 varieties have good appearance quality;6 varieties have coordinated chemical composition and high potassium content;9 varieties have good smoke components and physical indicators.展开更多
The low temperature coal tar(CT)is taken as the raw material,and the extraction and column chromatography are used for detailed and accurate characterization in this paper.The n-heptane soluble fraction(CT-HS)and inso...The low temperature coal tar(CT)is taken as the raw material,and the extraction and column chromatography are used for detailed and accurate characterization in this paper.The n-heptane soluble fraction(CT-HS)and insoluble fraction(CT-HI)were obtained by n-heptane Soxhlet extraction.The extraction rate of CT-HS reached 92.79%(mass),which indicated that there are few heavy compounds in it.Further,different solvents(methylbenzene,benzene,ethyl acetate,methylbenzene-ethanol)were used to elute CT-HS by chromatographic column to obtain five fractions(saturates,aromatics,heteroatoms,phenolics and resins,named CT-SA,CT-AR,CT-HE,CT-PH,CT-RE,respectively).The yields of CTSA,CT-AR,CT-HE,CT-PH,CT-RE are 42.12%,10.43%,2.19%,9.50%and 6.63%(mass),respectively.Gas chromatography-mass spectrometry analysis of eluting components show that alkanes are the main components in CT,followed by polycyclic aromatics,and the corresponding fractions are CT-SA and CT-AR,respectively.The relative content of aliphatics in CT-SA is 76.93%,and the relative content of aromatics in CT-AR is 75.05%.This separation technology effectively separates and enriches different components in CT,and the activation energy required for the pyrolysis process of a single eluting fraction is lower than that of CT,which is expected to provide an important reference for the separation,analysis and conversion of complex oil products such as coal-oil co-processing products,coal tar and other complex heavy carbon oil products.展开更多
The composition of low temperature pyrolysis coal tar has an effect on its further processing and reasomble utlization In this paper, the compeition or coal tars produced from both low temperature pyroysis in a fluidi...The composition of low temperature pyrolysis coal tar has an effect on its further processing and reasomble utlization In this paper, the compeition or coal tars produced from both low temperature pyroysis in a fluidized bed aud flash pyrolysis with solid heat carrier have been investigated by the methch of fractional seperation and Gas Chromatography-Mass Spectrometry (GC-MS)- It is observed that the degree of coalification maceral and secondary reaction temperature (freeboard temperature in a fluidized bed) have some iufluence on the composition of coal tars- The main compoundes are phenol cresols,xylenols, naphthalene, alkylnaphthalenes, antbraceue, phenanthrene,acenaphthylene, fluoren, indene and so展开更多
文摘The main agronomic traits,economic traits,appearance quality,main chemical components,gas composition and physical parameters of 10 flue cured tobacco varieties were investigated in the experiment.And the field natural incidence of the main diseases was investigated.The results showed that main agronomic characters of the 10 varieties were in line with the breeding objectives,among which 5 varieties have good economic characters;5 varieties have good appearance quality;6 varieties have coordinated chemical composition and high potassium content;9 varieties have good smoke components and physical indicators.
基金financed by the project supported by the National Natural Science Foundation of China(22078266,21908180,22178289,22278338)the Key Research and Development Program of Shaanxi(2020ZDLGY11-02,2021GY-136)the Special Fund for High-level Scholars of China(XJ21B10)。
文摘The low temperature coal tar(CT)is taken as the raw material,and the extraction and column chromatography are used for detailed and accurate characterization in this paper.The n-heptane soluble fraction(CT-HS)and insoluble fraction(CT-HI)were obtained by n-heptane Soxhlet extraction.The extraction rate of CT-HS reached 92.79%(mass),which indicated that there are few heavy compounds in it.Further,different solvents(methylbenzene,benzene,ethyl acetate,methylbenzene-ethanol)were used to elute CT-HS by chromatographic column to obtain five fractions(saturates,aromatics,heteroatoms,phenolics and resins,named CT-SA,CT-AR,CT-HE,CT-PH,CT-RE,respectively).The yields of CTSA,CT-AR,CT-HE,CT-PH,CT-RE are 42.12%,10.43%,2.19%,9.50%and 6.63%(mass),respectively.Gas chromatography-mass spectrometry analysis of eluting components show that alkanes are the main components in CT,followed by polycyclic aromatics,and the corresponding fractions are CT-SA and CT-AR,respectively.The relative content of aliphatics in CT-SA is 76.93%,and the relative content of aromatics in CT-AR is 75.05%.This separation technology effectively separates and enriches different components in CT,and the activation energy required for the pyrolysis process of a single eluting fraction is lower than that of CT,which is expected to provide an important reference for the separation,analysis and conversion of complex oil products such as coal-oil co-processing products,coal tar and other complex heavy carbon oil products.
文摘The composition of low temperature pyrolysis coal tar has an effect on its further processing and reasomble utlization In this paper, the compeition or coal tars produced from both low temperature pyroysis in a fluidized bed aud flash pyrolysis with solid heat carrier have been investigated by the methch of fractional seperation and Gas Chromatography-Mass Spectrometry (GC-MS)- It is observed that the degree of coalification maceral and secondary reaction temperature (freeboard temperature in a fluidized bed) have some iufluence on the composition of coal tars- The main compoundes are phenol cresols,xylenols, naphthalene, alkylnaphthalenes, antbraceue, phenanthrene,acenaphthylene, fluoren, indene and so
