Simplified quantitative analysis method and its application in the insitu synthesized copper-based azide chips

Copper-based azide(Cu(N_(3))2 or CuN_(3),CA)chips synthesized by in-situ azide reaction and utilized in miniaturized explosive systems has become a hot research topic in recent years.However,the advantages of in-situ synthesis method,including small size and low dosage,bring about difficulties in quantitative analysis and differences in ignition capabilities of CA chips.The aim of present work is to develop a simplified quantitative analysis method for accurate and safe analysis of components in CA chips to evaluate and investigate the corresponding ignition ability.In this work,Cu(N_(3))2 and CuN_(3)components in CA chips were separated through dissolution and distillation by utilizing the difference in solubility and corresponding content was obtained by measuring N_(3)-concentration through spectrophotometry.The spectrophotometry method was optimized by studying influencing factors and the recovery rate of different separation methods was studied,ensuring the accuracy and reproducibility of test results.The optimized method is linear in range from 1.0-25.0 mg/L,with a correlation coefficient R^(2)=0.9998,which meets the requirements of CA chips with a milligram-level content test.Compared with the existing ICP method,component analysis results of CA chips obtained by spectrophotometry are closer to real component content in samples and have satisfactory accuracy.Moreover,as its application in miniaturized explosive systems,the ignition ability of CA chips with different component contents for direct ink writing CL-20 and the corresponding mechanism was studied.This study provided a basis and idea for the design and performance evaluation of CA chips in miniaturized explosive systems.

Numerical Simulation Study of Oil-Water Emulsion Separation in an Ultrasonic Field:Effect of Coupling between Acoustic and Flow Field Parameters

In this study,the separation and coalescence of oil-in-water emulsions are explored in an ultrasonic field using the lattice Boltzmann method.By simulating the propagation of ultrasonic waves,this study focuses on examining the effects of acoustic wave frequency,the ratio of oil to water components,and the aspect ratio of the boundary on the emulsification and separation processes of oil-water mixtures.The following conclusions are drawn.①Frequency affects the speed of oil droplet separation,leading to an increase in droplet size over time.Larger droplets are found near the source,while smaller droplets are distributed throughout the wave web.②As the boundary aspect ratio increases,the emulsification efficiency of the droplets weakens,and the system takes longer to stabilize.③Emulsions with a higher component of oil can better resist acoustic waves.④At the same acoustic frequency,longer wavelength ultrasonic fields promote the formation of uniformly distributed,smaller oil droplets,which is beneficial to the storage of emulsions.These numerical simulation results offer insights for optimizing conditions for oil-in-water separation and serve as a numerical reference for the study of oil-in-water emulsion separation in ultrasonic environments.

A new method for separating complex touching equiaxed and lamellar alpha phases in microstructure of titanium alloy

A new method for separating complex touching equiaxed and lamellar alpha phases in the optical micrograph of titanium alloy was proposed for quantitative characterization. This new method involves three steps. First, concave points of the microstructural feature are identified with a threshold of the concaveness of the comer points which are extracted from the binarized image. Secondly, concave points pairs are selected from the concave points group established by means of marker circle or distance. Third, whether a candidate separation line which connects two concave points within a pair can be accepted or not is determined by the proposed four rules. The obtained results show that this method is effective on separating complex touching microstructural features.

On the feasibility of variable separation method based on Hamiltonian system for plane magnetoelectroelastic solids

The eigenvalue problem of an infinite-dimensional Hamiltonian operator appearing in the isotropic plane magnetoelectroelastic solids is studied. First, all the eigenvalues and their eigenfunctions in a rectangular domain are solved directly. Then the completeness of the eigenfunction system is proved, which offers a theoretic guarantee of the feasibility of variable separation method based on a Hamiltonian system for isotropic plane magnetoelectroelastic solids. Finally, the general solution for the equation in the rectangular domain is obtained by using the symplectic Fourier expansion method.

Solving mKdV-sinh-Gordon equation by a modified variable separated ordinary differential equation method

By introducing a more general auxiliary ordinary differential equation （ODE）, a modified variable separated ODE method is developed for solving the mKdV-sinh-Gordon equation. As a result, many explicit and exact solutions including some new formal solutions are successfully picked up for the mKdV-sinh-Gordon equation by this approach.

Extended Group Foliation Method and Functional Separation of Variables to Nonlinear Wave Equations

Generalized functional separation of variables to nonlinear evolution equations is studied in terms of the extended group foliation method, which is based on the Lie point symmetry method. The approach is applied to nonlinear wave equations with variable speed and external force. A complete classification for the wave equation which admits functional separable solutions is presented. Some known results can be recovered by this approach.

Functional Separable Solutions to Nonlinear Diffusion Equations by Group Foliation Method

We consider the functional separation of variables to the nonlinear diffusion equation with source and convection term： ut = （A（x）D（u）ux）x ＋ B（x）Q（u）, Ax ≠ 0. The functional separation of variables to this equation is studied by using the group foliation method. A classification is carried out for the equations which admit the function separable solutions. As a consequence, some solutions to the resulting equations are obtained.

Neutron-gamma discrimination method based on blind source separation and machine learning

The discrimination of neutrons from gamma rays in a mixed radiation field is crucial in neutron detection tasks.Several approaches have been proposed to enhance the performance and accuracy of neutron-gamma discrimination.However,their performances are often associated with certain factors,such as experimental requirements and resulting mixed signals.The main purpose of this study is to achieve fast and accurate neutron-gamma discrimination without a priori information on the signal to be analyzed,as well as the experimental setup.Here,a novel method is proposed based on two concepts.The first method exploits the power of nonnegative tensor factorization(NTF)as a blind source separation method to extract the original components from the mixture signals recorded at the output of the stilbene scintillator detector.The second one is based on the principles of support vector machine(SVM)to identify and discriminate these components.In addition to these two main methods,we adopted the Mexican-hat function as a continuous wavelet transform to characterize the components extracted using the NTF model.The resulting scalograms are processed as colored images,which are segmented into two distinct classes using the Otsu thresholding method to extract the features of interest of the neutrons and gamma-ray components from the background noise.We subsequently used principal component analysis to select the most significant of these features wich are used in the training and testing datasets for SVM.Bias-variance analysis is used to optimize the SVM model by finding the optimal level of model complexity with the highest possible generalization performance.In this framework,the obtained results have verified a suitable bias–variance trade-off value.We achieved an operational SVM prediction model for neutron-gamma classification with a high true-positive rate.The accuracy and performance of the SVM based on the NTF was evaluated and validated by comparing it to the charge comparison method via figure of merit.The results indicate that the proposed approach has a superior discrimination quality(figure of merit of 2.20).

Preparation of Microcapsules with Liquid Droplet Coalescence Method Followed by Phase Separation

Novel preparation method of microencapsules was developed on the basis of the liquid coalescence method followed by phase separation. Oil droplets of limonene dissolving expanded polystyrene as a shell material were forced to collide and coalesce with the Isopar oil droplets of core material in the continuous wates phase. When two kinds of oil droplets are collided and coalesced with each other, expanded polystyrene dissolved in the limonene oil may be phase-separated in the oil droplets newly formed to form the microcapsule shell, because the Isopar oil was a poor solvent for expanded polystyrene but a good solvent for the limonene oil. In the experiment, the diameter (or number) of limonene oil droplets dissolving expanded polystyrene was mainly changed, because the coalescence frequency between the droplets is strongly dependent on the number of droplets. Favorable core shell types of microcapsules with the shell thickness from 1.0 to 5.0 μm were able to be prepared under all the experimental conditions adopted here.

A Privilege Separation Method for Security Commercial Transactions

Privilege user is needed to manage the commercial transactions, but a super-administrator may have monopolize power and cause serious security problem. Relied on trusted computing technology, a privilege separation method is proposed to satisfy the security management requirement for information systems. It authorizes the system privilege to three different managers, and none of it can be interfered by others. Process algebra Communication Sequential Processes is used to model the three powers mechanism, and safety effect is analyzed and compared.

Solving (2+1)-dimensional sine-Poisson equation by a modified variable separated ordinary differential equation method

By introducing a more general auxiliary ordinary differential equation （ODE）, a modified variable separated ordinary differential equation method is presented for solving the （2 ＋ 1）-dimensional sine-Poisson equation. As a result, many explicit and exact solutions of the （2 ＋ 1）-dimensional sine-Poisson equation are derived in a simple manner by this technique.

A SPECIAL METHOD OF FOURIER SERIES WHICH IS EQUAL TO THE METHOD OF SEPARATION OF VARIABLES ON BOUNDARY VALUE PROBLEM

By the separation of singularity, a special Fourier series solution of the boundary value problem for plane is obtained, which can satisfy all boundary conditions and converges rapidly. II is proved that the solution is equal to the result of separation of variables. As a result, the non-linear characteristic equations resulting from the method of separation of variables are transformed into polynomial equations that can provide a foundation for approximate computation and asymptotic analysis.

P-and S-wavefield simulations using both the firstand second-order separated wave equations through a high-order staggered grid finite-difference method

In seismic exploration, it is common practice to separate the P-wavefield from the S-wavefield by the elastic wavefield decomposition technique, for imaging purposes. However, it is sometimes difficult to achieve this, especially when the velocity field is complex. A useful approach in multi-component analysis and modeling is to directly solve the elastic wave equations for the pure P- or S-wavefields, referred as the separate elastic wave equa- tions. In this study, we compare two kinds of such wave equations： the first-order （velocity-stress） and the second- order （displacement-stress） separate elastic wave equa- tions, with the first-order （velocity-stress） and the second- order （displacement-stress） full （or mixed） elastic wave equations using a high-order staggered grid finite-differ- ence method. Comparisons are given of wavefield snap- shots, common-source gather seismic sections, and individual synthetic seismogram. The simulation tests show that equivalent results can be obtained, regardless of whether the first-order or second-order separate elastic wave equations are used for obtaining the pure P- or S-wavefield. The stacked pure P- and S-wavefields are equal to the mixed wave fields calculated using the corre- sponding first-order or second-order full elastic wave equations. These mixed equations are computationallyslightly less expensive than solving the separate equations. The attraction of the separate equations is that they achieve separated P- and S-wavefields which can be used to test the efficacy of wave decomposition procedures in multi-com- ponent processing. The second-order separate elastic wave equations are a good choice because they offer information on the pure P-wave or S-wave displacements.

Some discussions about method for solving the variable separating nonlinear models

Through analysing the exact solution of some nonlinear models, the role of the variable separating method in solving nonlinear equations is discussed. We find that rich solution structures of some special fields of these equations come from the nonzero seed solution. However, these nonzero seed solutions is likely to result in the divergent phenomena for the other field component of the same equation. The convergence and the signification of all field components should be discussed when someone solves the nonlinear equation using the variable separating method.

Application of Multi－objective Optimization Method to Extracton Separtion Process

A multi-objective decision procedure was proposed to select the optimal precase parameters of extractionseporating zirconium and hafnium from sulphuric acid solution with Alamine-336 as an extractant in this pa-per.Adaptive Random Search(ARS) algorithm was adopted for optimizing calculation. The results obtainedshow that the multi-objective decision method is much better than sangle-objecive decision method.

Separation Method in the Problem of a Beam-Plasma Interaction in a Cylindrical Warm Plasma Waveguide

The stabilization effect of a strong HF electric field on beam-plasma instability in a cylindrical warm plasma waveguide is discussed. A mathematical technique “separation method” applied to the two-fluid plasma model to separate the equations, which describe the system, into two parts, temporal and space parts. Plasma electrons are considered to have a thermal velocity. It is shown that a HF electric field has no essential influence on dispersion characteristics of unstable surface waves excited in a warm plasma waveguide by a low-density electron beam. The region of instability only slightly narrowing and the growth rate decreases by a small parameter and this result has been reduced compared to cold plasma. Also, it is found that the plasma electrons have not affected the solution of the space part of the problem.

A Novel Method for Separation of Tungsten and Molybdenum

Research on the separation of tungstenand molybdenum is of importance as it is a ba-sic problem in the metallurgy and industry oftungsten.Traditional methods for the separa-tion include precipitation with sulfides andsolvent extraction.There are,however,certaindisadvantages for these methods.A novelmethod was developed based on another

Fault Diagnosis and Separation for a Distributed Rotary-laser Scanning System

The wMPS is a laser-based measurement system used for large scale metrology.However,it is susceptible to external factors such as vibrations,which can lead to unreliable measurements.This paper presents a fault diagnosis and separation method which can counter this problem.To begin with,the paper uses simple models to explain the fault diagnosis and separation methods.These methods are then mathematically derived using statistical analysis and the principles of the wMPS.A comprehensive solution for fault diagnosis and separation is proposed,considering the characteristics of the wMPS.The effectiveness of this solution is verified through experimental observations.It can be concluded that this approach can detect and separate false observations,thereby enhancing the reliability of the wMPS.

A New Algorithm of Roundness Error Separation Technique of Three-point Method

Through the analysis of roundness error separation technique of three-point method and based on the invariability and periodicity of the geometrical characteristic of measured round contour, a new matrix algorithm, which can be used to solve directly the roundness of the measured round contour without Fourier transform, is presented. On the basis of the research and analysis of the rotation error movement which is separated by using the three-point method, a mathematical equation is derived, which can be used to separate the eccentric motion of least square center of measured round contour and the pure rotation motion error of spindle in rotation motion. The correctness of this method is validated by means of simulation.

二氧化碳膜分离材料及其性能研究进展

碳捕集、利用与封存技术是能源行业绿色发展的重要途径。与化学吸收法、变压吸附法和低温蒸馏法等传统工艺相比,膜分离法具有低能耗、高效率、小型化、环境友好、易与其他技术集成等优势。目前,膜材料的选择、改性以及对膜结构的重构是提高膜材料分离性能的关键。该文总结对比了有机聚合物膜、无机膜及混合基质膜的研究进展,并对其分离机理、材料及性能进行了介绍,重点综述了材料的改性研究及用于制备混合基质膜的填充材料,展望了CO_(2)分离膜材料性能改进的研究方向及膜分离技术所面临的挑战。