A novel wet-chemical method for preparation of silver flakes

A novel wet-chemical method for the preparation of silver flakes was studied. The well-defined particles were prepared by directly adding FeSO4 solution into AgNO3 solution containing citric acid at an agitation speed of 150 r/min at room temperature. The products were characterized by scanning electron microscopy （SEM） and X-ray diffraction （XRD）. The results show that particles are irregular thin silver flakes. And the sizes of them range from 2 to 10 μm. It is found that citric acid plays an important role in the formation of sliver flakes. There is an optimum amount of citric acid for the preparation of silver flakes by this method. It is also found that high reduction rate is favorable for the formation of silver flakes.

短周期线性密集台阵揭示宣城地区浅部地壳速度结构及断裂发育特征

宣城市位于东南丘陵与长江中下游平原过渡地带,区内经历多期构造活动,地质构造复杂且断裂十分发育,开展宣城地区浅部速度结构和断裂带探测,不仅有助于深入了解区内地质构造和成矿作用,还可以为区域地震危险性和危害性评价提供重要的参考模型.本文在研究区布设了一条由110套三分量地震仪组成的短周期线性密集台阵,利用采集的一个月的三分量背景噪声数据,采用噪声谱比方法(HVSR)探测研究区场地峰值频率及基岩界面结构;通过垂直分量背景噪声数据重建经验格林函数,采用拓距相移法(ERPS)提取相速度频散曲线并反演线性台阵下方浅部地壳精细横波速度结构.基于HVSR计算的场地峰值频率和基岩界面埋深,刻画了测线下方浅部地表松散沉积层的结构,结果显示研究区内皖南山区基岩埋深较浅,盆地区域基岩埋深较深,地表松散沉积层的厚度最大可至地下80 m,此外还评估了区内地震破坏性和建筑的抗震性,认为研究区内平均振幅放大系数相对较高,局部区域可能会产生明显的地震放大效应,并且皖南山区低矮建筑(1~2层)及宣城—南陵盆地区域的高层建筑(7层及以上)在抗震设防上应当特别注意;依据反演的二维横波速度模型,获得了研究区浅部地壳6 km以深的结构,结果显示宣城—南陵盆地在浅部表现为明显的低速特征,其基底深度可达2 km,并且盆地部分区域呈现相对高速的异常特征,指示在区域多期构造活动中产生的岩浆侵入和逆冲推覆构造作用。此外,区内深部总体表现为高低速异常交替分布的“叠瓦状”构造模式,出现的多处低速异常带推断分别是周王断裂、江南断裂和茅山断裂以及清水河—河湾断裂的构造破碎带,指示了研究区内经历的多期次挤压—拉伸的强烈变形改造.综合上述研究成果,本研究为宣城地区地质构造条件的分析、地震危险性及危害性的评价以及区域找矿勘查等相关工作提供了新的依据.

Error estimates of H^1-Galerkin mixed finite element method for Schrdinger equation

An H^1-Galerkin mixed finite element method is discussed for a class of second order SchrSdinger equation. Optimal error estimates of semidiscrete schemes are derived for problems in one space dimension. At the same time, optimal error estimates are derived for fully discrete schemes. And it is showed that the H1-Galerkin mixed finite element approximations have the same rate of convergence as in the classical mixed finite element methods without requiring the LBB consistency condition.

Clinical role and importance of fluorescence in situ hybridization method in diagnosis of H pylori infection and determination of clarithromycin resistance in H pylori eradication therapy

H pylori is etiologically associated with gastritis, gas-tric and duodenal ulcers, gastric adenocarcinoma and mucosa-associated lymphoid tissue (MALT) lymphoma. Eradicating H pylori may convert rapidly the outcome of related diseases with the use of more accurate diagnostic molecular tests. Indeed some of the tests cannot give the evidence of current infection; H pylori can be detected by noninvasive and invasive methods, the latter requiring an endoscopy. Eradication failure is a big problem in H pylori infection. Recently, clarithromycin resistance in H pylori strains is increasing and eradicati-on therapy of this bacterium is becoming more difficult. Molecular methods have frequently been applied besides phenotypic methods for susceptibility testing to detect clarithromycin resistance due to mutations in the 2143 and 2144 positions of 23S rRNA gene. Fluorescence in situ hybridization (FISH) method on paraffin embedded tissue is a rapid, accurate and cost-effective method for the detection of H pylori infection and to determine clarithromycin resistance within three hours according to the gold standards as a non-culture method. This method can also be applied to fresh biopsy samples and the isolated colonies from a culture of H pylori, detecting both the culturable bacillary forms and the coccoid forms of H pylori, besides the paraffin embedded tissue secti-ons. This technique is helpful for determining the bac-terial density and the results of treatment where clarith-romycin has been widely used in populations to increase the efficacy of the treatment and to clarify the treatment failure in vitro.

3-D numerical modelling of Domino failure of hard rock pillars in Fetr6 Chromite Mine, Iran, and comparison with empirical methods

Fetr6 is an underground mine using the stope-and-pillar mining method. As there was some evidence regarding pillar failure in this mine, improving works such as roof support and replacing existing pillars with concrete pillars (CP) were carried out. During the construction of the second CP, in the space between the remaining pillars, one of the pillars failed leading to the progressive failure of other pillars until 4 000 m 2 of mine had collapsed within a few minutes. In this work, this phenomenon is described by applying both numerical and empirical methods and the respective results are compared. The results of numerical modelling are found to be closer to the actual condition than those of the empirical method. Also, a width-to-height (W/H) ratio less than 1, an inadequate support system and the absence of a detailed program for pillar recovery are shown to be the most important causes of the Domino failure in this mine.

N-doped NaTaO3 synthesized from a hydrothermal method for photocatalytic water splitting under visible light irradiation

NaTaONcatalysts were synthesized by a hydrothermal（H） and a solid-state（S） methods in this study.The H-and S-NaTaONsamples were characterized by X-ray diffraction（XRD）, scanning electron microscopy（SEM）, transmission electron microscopy（TEM）, UV–visible（UV–vis） diffuse reflectance spectroscopy, and photoluminescence（PL） spectroscopy. The XRD patterns of the H-and S-samples showed peaks indexed to the pure phase of perovskite NaTaOand minor peaks assignable to TaNat various synthesis temperatures. Substitution of oxygen by nitrogen ions causes the light absorption of the H-and S-NaTaONsamples to be extended to the 600–650 nm region, thus making the samples visible-light active. The NaTaONsamples exhibited photocatalytic activity for Hand Oevolution from aqueous methanol and silver nitrate solutions under visible-light irradiation. The UV–vis and PL spectra of the Hand S-catalysts revealed the presence of cationic vacancies and reduced metallic species, which acted as recombination centers. These results demonstrated that the preparation method plays a critical role in the formation of defect states, thereby governing the photocatalytic activity of the NaTaONcatalysts.

Mixed H_2/H_∞ State Feedback Attitude Control of Microsatellite Based on Extended LMI Method

For the appearance of the additive perturbation of controller gain when the controller parameter has minute adjustment at the initial running stage of system,to avoid the adverse effects,this paper investigates the mixed H_2/H_∞ state feedback attitude control problem of microsatellite based on extended LMI method.Firstly,the microsatellite attitude control system is established and transformed into corresponding state space form.Then,without the equivalence restriction of the two Lyapunov variables of H_2 and H∞performance,this paper introduces additional variables to design the mixed H_2/H_∞ control method based on LMI which can also reduce the conservatives.Finally,numerical simulations are analyzed to show that the proposed method can make the satellite stable within 20 s whether there is additive perturbation of the controller gain or not.The comparative analysis of the simulation results between extended LMI method and traditional LMI method also demonstrates the effectiveness and feasibility of the proposed method in this paper.

Different Preservation Methods for Long Term Maintenance of <i>Haemophilus influenzae</i>

Haemophilus species are Gram-negative coccobacilli that require factor X and factor V for growth. Beyond this, it is a finicky bacterium to culture, and any modification of culture procedures greatly reduces isolation rates. Poor quality of laboratories in developing countries results in its poor isolation rates. This study was done with the objective of finding out the optimal cultural environment and media so that it could be maintained for a longer period in economical settings like ours which was done using H. influenzae ATCC 49,766. In this study, several culture media were tested as a means to preserve H. influenzae ATCC like TSB + glycerol + sheep blood, BHI broth, BHI broth + glycerol, BHI broth+ glycerol + sheep blood, Chocolate agar slant and satellitism plate. Three sets of respective media were inoculated with 18 - 24 hours growth of H. influenzae. They were incubated at 37?oC 48 hours in a candle extinction jar. The media were checked for growth by subculturing them on chocolate agar plates and identified by biochemical reactions. Each set was maintained at 2 oC - 8?oC, -20?oC and at room temperature and checked for the viability 24 hourly by subculturing them on chocolate agar. Results showed best growth of H. influenza on chocolate agar slants for 15 - 20 days, followed by BHI + glycerol + sheep blood broth and satellitism plate for 4 - 6 days followed by BHI broth for 2 - 4 days. There was no growth in TSB + glycerol + sheep blood broth and BHI + glycerol broth media. Present study showed similar results as done by NS Srikanth et al. 2003 with growth on chocolate agar & satellitism plate for 3 - 5 days but no growth in TSB + Glycerol + Sheep blood broth media. Chocolate agar slant is by far the most long term preserving media for H. influenzae. However, growth on BHI broth with various modifications is also showed a good preservation for 3 - 5 days, so with further experiments we can hope to maintain the organism in these media also.

An H^1-Galerkin Expanded Mixed Element Method for Semi-linear Hyperbolic Wave Equation

An H1-Galerkin expanded mixed finite element method is discussed for a class of second order semi-linear hyperbolic wave equations. By using the mixed formulation, we can get the optimal approximation for three variables: the scalar unknown, its gradient and its flux(coefficient times the gradient), simultaneously. We also prove the existence and uniqueness of semi-discrete solution. Finally, we obtain some numerical results to illustrate the efficiency of the method.

Precipitation Retrieval from Himawari-8 Satellite Infrared Data Based on Dictionary Learning Method and Regular Term Constraint

In this paper,the application of an algorithm for precipitation retrieval based on Himawari-8 (H8) satellite infrared data is studied.Based on GPM precipitation data and H8 Infrared spectrum channel brightness temperature data,corresponding "precipitation field dictionary" and "channel brightness temperature dictionary" are formed.The retrieval of precipitation field based on brightness temperature data is studied through the classification rule of k-nearest neighbor domain (KNN) and regularization constraint.Firstly,the corresponding "dictionary" is constructed according to the training sample database of the matched GPM precipitation data and H8 brightness temperature data.Secondly,according to the fact that precipitation characteristics in small organizations in different storm environments are often repeated,KNN is used to identify the spectral brightness temperature signal of "precipitation" and "non-precipitation" based on "the dictionary".Finally,the precipitation field retrieval is carried out in the precipitation signal "subspace" based on the regular term constraint method.In the process of retrieval,the contribution rate of brightness temperature retrieval of different channels was determined by Bayesian model averaging (BMA) model.The preliminary experimental results based on the "quantitative" evaluation indexes show that the precipitation of H8 retrieval has a good correlation with the GPM truth value,with a small error and similar structure.

Finite cell method compared to h-version finite element method for elasto-plastic problems

The finite cell method （FCM） combines the high-order finite element method （FEM） with the fictitious domain approach for the purpose of simple meshing. In the present study, the FCM is used to the Prandtl-Reuss flow theory of plasticity, and the results are compared with the h-version finite element method （h-FEM）. The numerical results show that the FCM is more efficient compared to the h-FEM for elasto-plastic problems, although the mesh does not conform to the boundary. It is also demonstrated that the FCM performs well for elasto-plastic loading and unloading.

Error Estimates of H^1-Galerkin Mixed Methods for the Viscoelasticity Wave Equation

H1-Galerkin mixed methods are proposed for viscoelasticity wave equation.Depending on the physical quantities of interest,two methods are discussed.The optimal error estimates and the proof of the existence and uniqueness of semidiscrete solutions are derived for problems in one space dimension.And the methods don＇t require the LBB condition.

Research on robust control strategy of single DOF supporting system of MLDSB based on H∞ mixed-sensitivity Method

Because of hydraulic-electromagnetic double supporting forms,the supporting capacity and stiffness of magnetic-liquid double suspension bearing(MLDSB)can be improved sharply and then it is more suitable for medium speed,heavy load and frequent-starting occasions.Due to the multiple uncertainty,such as the coupling,the unmodeled dynamics,the parameter perturbation and the external disturbance perturbation,the robust stability and stiffness of control system of MLDSB are hard to meet the design requirements.Firstly,the structural features and the regulation mechanisms of MLDSB are presented and the radial 4-DOF kinetic equations are established.Secondly,the influence factors of the control system's coupling on unbalanced vibration caused by the deviation of the rotor center of mass are revealed,and then the weighting function of suppressing the unbalanced vibration can be obtained.Finally,H∞ controller of MLDSB is designed with H∞ mixed-sensitivity method,and the control performances of H∞ controller is compared with the state feedback controller.The simulation results show that single degree of freedom(DOF)supporting system of MLDSB with H∞ controller has good robust stability,stiffness and the ability to suppress unbalanced external disturbances.This study can provide the theoretical reference for stabilized suspension and control of MLDSB.

Turbulent-Induced Noise around a Circular Cylinder Using Permeable FW-H Method

Varieties of research on turbulent-induced noise are conducted with combinations of acoustic analogy methods and computational fluid dynamic methods to analyse efficiently and accurately. Application of FW-H acoustic analogy without turbulent noise is the most popular method due to its calculation cost. In this paper, turbulent-induced noise is predicted using RANS turbulence model and permeable FW-H method. For simplicity, noise from 2D cylinder is examined using three different methods: direct method of RANS, FW-H method without turbulent noise and permeable FW-H method which can take into account of turbulent-induced noise. Turbulent noise was well predicted using permeable FW-H method with same computational cost of original FW-H method. Also, ability of permeable FW-H method to predict highly accurate turbulent-induced noise by applying adequate permeable surface is presented. The procedure to predict turbulent- induced noise using permeable FW-H is established and its usability is shown.

Adaptive H-infinity control of synchronous generators with steam valve via Hamiltonian function method

Based on Hamiltonian formulation, this paper proposes a design approach to nonlinear feedback excitation control of synchronous generators with steam valve control, disturbances and unknown parameters. It is shown that the dynamics of the synchronous generators can be expressed as a dissipative Hamiltonian system, based on which an adaptive H-infinity controller is then designed for the systems by using the structure properties of dissipative Hamiltonian systems. Simulations show that the controller obtained in this paper is very effective.

Fault-tolerant decentralized H-infinity control for multi-channel systems using homotopy method

This paper considers a fault-tolerant decentralized H-infinity control problem for multi-channel linear time-invariant systems. The purpose is to design a decentralized H-infinity output feedback controller to.stabilize the given system and achieve a certain H-infinity performance requirement both in the normal situation and in the situation where any one of the local controllers fails. The designed problem is reduced to a feasibility problem of a set of bilinear matrix inequalities （BMIs）. An algorithm is proposed to solve the BMIs. First, the normal situation is considered where all the local controllers are functioning. The local controllers are obtained from a standard centralized H-infinity controller by using a homotopy method imposing a structural constraint progressively. Secondly, the above case is extended to the one where any one of the local controllers fails. We again use a homotopy method where the coefficient matrices of the failed controller are decreased progressively to zero. The efficiency of the proposed algorithm is demonstrated by an example.

An h-adaptive Discontinuous Galerkin Method for Laminar Compressible Navier-Stokes Equations on Curved Mesh

An h-adaptive method is developed for high-order discontinuous Galerkin methods(DGM)to solve the laminar compressible Navier-Stokes(N-S)equations on unstructured mesh.The vorticity is regarded as the indicator of adaptivity.The elements where the vorticity is larger than a pre-defined upper limit are refined,and those where the vorticity is smaller than a pre-defined lower limit are coarsened if they have been refined.A high-order geometric approximation of curved boundaries is adopted to ensure the accuracy.Numerical results indicate that highly accurate numerical results can be obtained with the adaptive method at relatively low expense.

Design of Poiseuille Flow Controllers Using the Method of Inequalities

This paper investigates the use of the method of inequalities （MoI） to design output-feedback compensators for the problem of the control of instabilities in a laminar plane Poiseuille flow. In common with many flows, the dynamics of streamwise vortices in plane Poiseuille flow are very non-normal. Consequently, small perturbations grow rapidly with a large transient that may trigger nonlinearities and lead to turbulence even though such perturbations would, in a linear flow model, eventually decay. Such a system can be described as a conditionally linear system. The sensitivity is measured using the maximum transient energy growth, which is widely used in the fluid dynamics community. The paper considers two approaches. In the first approach, the MoI is used to design low-order proportional and proportional-integral （PI） controllers. In the second one, the MoI is combined with McFarlane and Glover＇s H∞ loop-shaping design procedure in a mixed-optimization approach.

H^1 space-time discontinuous finite element method for convection-diffusion equations

An H1 space-time discontinuous Galerkin （STDG） scheme for convection- diffusion equations in one spatial dimension is constructed and analyzed. This method is formulated by combining the H1 Galerkin method and the space-time discontinuous finite element method that is discontinuous in time and continuous in space. The existence and the uniqueness of the approximate solution are proved. The convergence of the scheme is analyzed by using the techniques in the finite difference and finite element methods. An optimal a-priori error estimate in the L∞ （H1） norm is derived. The numerical exper- iments are presented to verify the theoretical results.

A high-throughput screening method for breeding Aspergillus niger with 12C6+ ion beam-improved cellulase

In this study,a high-throughput screening method was established through the 24-square deep-well microliter plate(MTP) fermentation and micro-plate detection for large-scale screening of the mutants.It was suitable for screening a large number of mutants and improving the breeding efficiency after heavy-ion beam irradiation.Seventeen strains showed higher cellulase activity compared with the initial strain after the screening of plate and MTP fermentation.The filter paper activity and β-glucosidase activity of Aspergillus niger H11201 had increased 38.74 and 63.23%separately compared with A.niger H11 by shaking flask fermentation,and it was genetically stable after being passaged to nine generations.The results indicate that the high-throughput screening method can be used for the quick breeding of A.niger with high cellulase activity.