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Studies on the New Constituents of Sal via Miltiorrhiza Bunge
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作者 CEN Ying-zhou (Department of Chemistry, University of Jinan, Guangzhou, 510632)WU Qiu-ming (Center of Analysis, University of Jinan, Guangzhou, 510632) 《Chemical Research in Chinese Universities》 SCIE CAS CSCD 1992年第3期262-266,共5页
Two novel constituents were isolated from the roots of Chinese medicinal herbs, Salvia miltiorrhiza. Their structures were determined by spectroscopic technique. The compounds were named 13,14-dihydroxy-15-methyl-benz... Two novel constituents were isolated from the roots of Chinese medicinal herbs, Salvia miltiorrhiza. Their structures were determined by spectroscopic technique. The compounds were named 13,14-dihydroxy-15-methyl-benzo[2,3-a]-7,7-dimethyl-12-oxa-tricyclo[4,4,21.4,0]dodecane(1) and 16-methyl-tropono[2,3-c]-7,7-dimethyl-12-oxa-tricyclo[4,4,21.4,0]dodecane(2). 展开更多
关键词 Salvria miltiorrhiza 13 14-dihydroxy-15-methyl-benzo [2 3-a]-7 7-dimethyl-12-oxa-tricyclo [4 4 21 4 0] dodecane 16-methyl-tropono [2 3-c]-7 7-dimethyl-12-oxa-tricyclo[4 4.21 4 0] dodecane
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白花蛇舌草中的一个新蒽醌 被引量:12
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作者 于莉 李俊明 +1 位作者 姜珍 郭兴杰 《中国药物化学杂志》 CAS CSCD 2008年第4期298-299,共2页
采用硅胶吸附柱色谱的手段从中药白花蛇舌草中分离得到一个新化合物,根据理化性质和谱学分析的方法确定其结构为2,7-二羟基-3-甲基蒽醌(2,7-dihydroxy-3-methyl anthraquinone)。经Scifinder检索系统检索,确定该化合物是未见文献报道的... 采用硅胶吸附柱色谱的手段从中药白花蛇舌草中分离得到一个新化合物,根据理化性质和谱学分析的方法确定其结构为2,7-二羟基-3-甲基蒽醌(2,7-dihydroxy-3-methyl anthraquinone)。经Scifinder检索系统检索,确定该化合物是未见文献报道的新化合物。 展开更多
关键词 结构鉴定 核磁共振谱 2 7-二羟基-3-甲基蒽醌 白花蛇舌草
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苏木心材中一个新黄酮类化合物 被引量:2
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作者 舒诗会 韩景兰 +1 位作者 杜冠华 秦海林 《中国中药杂志》 CAS CSCD 北大核心 2008年第8期903-905,共3页
目的:从苏木Caesalpinia sappan中寻找新的活性成分。方法:用溶剂萃取及硅胶正相色谱进行活性成分的分离纯化,根据理化性质、光谱数据进行结构鉴定。结果:从苏木95%乙醇提取物中分离得到了9个化合物:3,8-dihydroxy-4,10-dimethoxy-7-oxo... 目的:从苏木Caesalpinia sappan中寻找新的活性成分。方法:用溶剂萃取及硅胶正相色谱进行活性成分的分离纯化,根据理化性质、光谱数据进行结构鉴定。结果:从苏木95%乙醇提取物中分离得到了9个化合物:3,8-dihydroxy-4,10-dimethoxy-7-oxo-[2]benzopyrano[4,3-b][1]benzopyran-7-(5H)-one(1),3-deoxysappanchal-cone(2),sappanchalcone(3),3-deoxysappanone B(4),鼠李素(rhamnetin,5),原苏木素C(protosappanin C,6),3,7-di-hydroxy-chroman-4-one(7),己二酸二甲酯(8),胡萝卜苷(daucosterin,9)。结论:化合物1为新化合物,化合物7,8为首次从该植物中分离得到。药理筛选结果表明,化合物3对多种癌细胞株具有一定的抑制活性。 展开更多
关键词 苏木 黄酮 3 8-dihydroxy-4 benzopyrano[4 benzopyran-7-(5H)-one 细胞毒活性
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A new angelol-type coumarin glucoside from Angelica pubescens 被引量:4
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作者 Xi Fei Ding Xu Feng Yun Fa Dong Xing Zeng Zhao Yu Chen Ming Wang 《Chinese Chemical Letters》 SCIE CAS CSCD 2008年第10期1237-1239,共3页
A new angelol-type coumarin glucoside, 6-[(1R,2R)-1, 2-dihydroxy-3-β-D-glucosyloxy-3-methylbutyl]-7-methoxycoumarin, was isolated from the roots of Angelica pubescens. Its structure was elucidated on the basis of s... A new angelol-type coumarin glucoside, 6-[(1R,2R)-1, 2-dihydroxy-3-β-D-glucosyloxy-3-methylbutyl]-7-methoxycoumarin, was isolated from the roots of Angelica pubescens. Its structure was elucidated on the basis of spectral analysis. 展开更多
关键词 Angelica pubescens UmbeUiferae Coumarin glucoside 6-[(1R 2R)-1 2-dihydroxy-3-β-D-glucosyloxy-3-methylbutyl]-7-methoxy-coumarin
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Indole Alkaloids from the Roots of Ervatamia hainanensis 被引量:4
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作者 Jian Peng HUANG Zi Ming FENG +2 位作者 Chong Fei ZHENG Pei Cheng ZHANG Yang Min MA 《Chinese Chemical Letters》 SCIE CAS CSCD 2006年第6期779-782,共4页
Two new indole alkaloids, named ibogamine-18-carboxylic acid, 3, 4-didehydro-7, 8-dioxo-methyl ester 1, ibogamine-18-carboxylic acid, 16, 17-didehydro-9, 17-dihydro-9-hydroxy (2-oxopropyl)-methyl ester 2, were isola... Two new indole alkaloids, named ibogamine-18-carboxylic acid, 3, 4-didehydro-7, 8-dioxo-methyl ester 1, ibogamine-18-carboxylic acid, 16, 17-didehydro-9, 17-dihydro-9-hydroxy (2-oxopropyl)-methyl ester 2, were isolated from Ervatamia hainanensis. Their structures were elucidated on the basis of spectroscopic methods. 展开更多
关键词 Ervatamia hainanensis indole alkaloid ibogamine-18-carboxylic acid 3 4-didehydro-7 8-dioxo-methyl ester ibogamine- 18-carboxylic acid 16 17-didehydro-9 17-dihydro-9-hydroxy-(2-oxopropyl)-methyl ester.
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A New Chromone Derivative from Stellera chamaejasme L 被引量:6
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作者 Bao Min FENG Yue Hu PEI Hui Ming HUA 《Chinese Chemical Letters》 SCIE CAS CSCD 2002年第8期738-739,共2页
A new chromone derivative, 3-[1- (2, 4, 6-trihydroxyphenyl) 3-di-(4-hydroxyphenyl) 1-propanone-2-yl] 5,7-dihydroxy-8-di(4-hydroxyphenyl)methyl-4H-1-benzopyran-4-one, named as isomohsenone was isolated from the roots o... A new chromone derivative, 3-[1- (2, 4, 6-trihydroxyphenyl) 3-di-(4-hydroxyphenyl) 1-propanone-2-yl] 5,7-dihydroxy-8-di(4-hydroxyphenyl)methyl-4H-1-benzopyran-4-one, named as isomohsenone was isolated from the roots of Stellera chamaejasme L. together with known chamaechromone. Its structure was determined by the analysis of MS and NMR data, especially 2D NMR spectra. 展开更多
关键词 Stellera chamaejasme L. CHROMONE 3-[1- (2 4 6-trihydroxyphenyl) 3-di-(4-hydroxy- phenyl)-1-propanone-2-yl] 5 7-dihydroxy-8-di-(4-hydroxyphenyl) methyl-4H-1- benzopyran-4- one.
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