Phase/grain boundary assisted-3D static globularization mechanism of TC17 alloy based on the microstructure reconstruction and in-situ TEM observation

Lamellar globularization in the dual-phase titanium alloy is the key to improving plasticity and strength.However,the mechanism has not been fully elucidated so far.In this work,the role of phase/grain bound-ary in the static globularization of TC17 alloy was systematically studied by setting differentαphase con-tent before annealing through low-and high-temperature deformation.Isothermal compression causes the parallel distribution and fragmentation of 3Dαplates and few globularαparticles are formed at a strain rate of 1 s^(-1).Post-deformation annealing promotes the static globularization ofαphase while it is affected by initialαphase content.After 730°C deformation,the development ofα/αinterface by absorbing dislocations promotes the formation of globularαgrains based on the nucleation of sepa-ratedαparticles and pre-recoveryαsubgrain during subsequent annealing.Theα/α/βandα/β/βtriple junctions formed due to highαcontent with about 36%volume fraction are favorable for the further nucleation and growth of globularαgrains by reducing interface energy,forming a 3D irregularαplate.Then nucleation and growth of theβphase dominate the microstructure evolution during subsequent an-nealing,resulting in the local dissolution of the plate and formation ofαrods.After 850°C deformation,theαphase tends to nucleate at theβ/β/βtriple junctions and grow into a lamellar shape along the high energyβ/βgrain boundary due to lowαcontent with about 7%volume fraction.Theαnucleation that maintains the Burgers orientation relationship(BOR)with the surroundingβphase grows along the habit plane and thickens slowly,resulting in the formation of a precipitatedαplate with a flat surface and the suppression of static globularization.The comprehensive investigation of lamellar globularization provides guidance for optimizing the 3D microstructure and properties of dual-phase titanium alloy.

A PMMA Passive Micromixer with Three-Dimensional Tortuous Mixing Chamber

In this paper,we design and fabricate a novel three-dimensional passive-micro-mixer by using Polymethyl methacrylate( PMMA). The mixer is fabricated by using ultra-precision engraving machine and bonded by an organic solvent fumigation bonding method. The mixer combines two fluid streams into a mixing chamber integrated with T-shaped pre-mixing and six tortuous shaped mixing elements. We have employed three-dimensional numerical simulations to evaluate the mixing efficiency. The simulation results indicate,under inlet fluid pressure p = 10( Pa), compared to the planar serpentine mixer and tortuous mixer,the concentration fluctuation range at the outlet diagonal reduce to 48% and 71. 6% respectively. And the mixing concentration variances also show that the mixing efficiency has a significant increase. We characterize the device by using visualization microscope,and the results are consistent with the simulation data. The device demonstrates the promising capabilities for micro total analysis system integration.