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Synthesis and Crystal Structure of 3-Nitrophthalic Acid·3-methyl-4-nitropyridine N-Oxide Adducts
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作者 WANG Yi FENG Wei XUE Lin ZHENG Ji-Min 《Chinese Journal of Structural Chemistry》 SCIE CAS CSCD 北大核心 2006年第8期923-926,共4页
The title compound, a 1:1 molecular adduct of 3-nitrophthalic acid and 3-methyl- 4-nitropyridine N-oxide (PPOM), has been synthesized and characterized by X-ray single-crystal structure analysis. It crystallizes in... The title compound, a 1:1 molecular adduct of 3-nitrophthalic acid and 3-methyl- 4-nitropyridine N-oxide (PPOM), has been synthesized and characterized by X-ray single-crystal structure analysis. It crystallizes in triclinic, space group PI with α = 7.6076(15), b = 7.8180(16), c = 14.546(3)A, α= 93.90(3), β = 97.21(3), γ= 114.43(3)°, C14H1N3O9, Mr = 365.26, Z = 2, V = 774.6(3) A^3, Dc = 1.566 g/m^3,μ(MoKa) = 0.134 mm^-1, F(000) = 376, R = 0.0538 and wR = 0. 1460 for 885 observed reflections (1 〉 2σ(I)). The protons of the carbonylic acids in the molecule are not transferred and the O-H…O and C-H…O hydrogen bonds form zigzag chains in the molecule. 展开更多
关键词 crystal structure SYNTHESIS 3-methyl-4-nitropyridine n-oxide ADDUCT
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