不同热处理工艺轧制态AZ80D镁合金疲劳后的显微组织观察

对不同热处理工艺的轧制态AZ80D镁合金疲劳后试样进行显微组织观察和疲劳断口扫描,分析发现,轧制状态AZ80D镁合金晶粒大小很不均匀。经过固溶处理的AZ80D镁合金,晶粒长大现象非常明显,晶粒大小相对均匀。不同热处理状态的AZ80D镁合金疲劳后,都出现了孪晶变形现象,可为以后提高AZ80D镁合金的疲劳性能提供更多的参考数据。

Microstructure and performance of AZ80D magnesium alloy by purification of chloride flux containing Er

The purification effects of Er addition in chloride flux during smelting on microstructure, tensile properties, and corrosion resistance of as-cast AZ80 D magnesium alloy were carried out. The results show that Er addition in the flux can eliminate the MgO inclusions and improve the tensile properties and corrosion resistance of the alloy. Using chloride flux mixed with 8.0 wt% Er, σb and δ of the as-cast AZ80 D magnesium alloy can be improved from 150 MPa and 2.1 % to the maximum value of 230 MPa and 4.8 %, respectively. Meanwhile, the corrosion rate decreases from 1.10 to 0.12 mg·（cm^2·d）^-1 in 5 wt% NaCl solution. However, with increasing Er content in chloride flux further, φ-（Al7ErMn5） and τ-（Al66.7Mg23.3Er10） phase are formed, and the morphology of γ-（Mg17Al12） phase is modified. The coarse φ-（Al7ErMn5）phase along dendrite boundaries decreases cohesion force between dendrites, which results in the worse of tensile properties.

高功率密度激光重熔镁合金的非均匀性机理研究

采用额定功率为3 kW的Nd:YAG固体激光器,开展镁合金激光重熔试验,通过金相显微镜(TK-C1031EC)、扫描电镜、X射线衍射(XRD)和维氏显微硬度计表征试样的组织、物相和硬度。结果表明:由于激光重熔镁合金存在匙孔现象,试样横截面形貌为短螺栓形;在高能量密度激光重熔下,熔凝过程中的预热作用、熔凝层的热传导等综合影响,使能量累积达到了镁合金熔凝的临界能量,沿激光扫描方向,镁合金的熔深逐渐增加;激光熔凝区域的晶粒细化;在热影响区温度介于α-Mg相及β相时,该区域观察到局部熔化现象,且热影响区Mn-Al相变细小;沿激光扫描方向展现出很好的预热作用,熔池内温度呈增加的趋势,沿扫描方向硬度呈逐渐下降的趋势。