通过扫描电镜/能谱、X射线衍射以及金相分析,针对含0.3%Fe(质量分数)的Al Mg Si Cu铝合金,研究了Mn含量对其结晶相的影响。研究表明:合金在铸造过程中形成的结晶相为Al1.9CuMg4.1Si3.3,Al5(FeMn)Si,Al8(FeMn)2Si以及少量的Mg2Si;增大含M...通过扫描电镜/能谱、X射线衍射以及金相分析,针对含0.3%Fe(质量分数)的Al Mg Si Cu铝合金,研究了Mn含量对其结晶相的影响。研究表明:合金在铸造过程中形成的结晶相为Al1.9CuMg4.1Si3.3,Al5(FeMn)Si,Al8(FeMn)2Si以及少量的Mg2Si;增大含Mn量,合金中AlFeMnSi型结晶相数量增多;对合金进行均匀化处理时,Al1.9CuMg4.1Si3.3相完全溶解,发生Al5(FeMn)Si向Al8(FeMn)2Si相的转变;对合金进行轧制及最终热处理后,结晶相碎化且沿轧向呈纤维状分布,但结晶相的类型不变。展开更多
Segregation can seriously damage the mechanical properties of the aluminum alloys.6061 aluminum alloy wheel spokes were prepared by squeeze casting.To investigate the formation mechanism of segregation,the microstruct...Segregation can seriously damage the mechanical properties of the aluminum alloys.6061 aluminum alloy wheel spokes were prepared by squeeze casting.To investigate the formation mechanism of segregation,the microstructure of the alloy was observed using scanning electron microscopy,energy dispersive spectrometry,X-ray diffraction and electron microprobe analysis methods.The Gibbs energy of each phase during solidification was calculated by JMat Pro.Results show that the segregation phases in the R-joint of the wheel spokes are mainly composed of Mg_(2)Si,β-Al Fe Si and Al_(5)Cu_(2)Mg_(8)Si_(6)intermetallics.During the solidification of the 6061 aluminum alloy wheels,Mg_(2)Si andα-Al Fe Si phases precipitate in the mushy zone at first.With the decrease of temperature,α-Al Fe Si transforms intoβ-Al Fe Si,while Al_(5)Cu_(2)Mg_(8)Si_(6)precipitates from the solid-state aluminum alloy after solidification.Segregation at the R-joint of wheel spokes is mainly caused by insufficient cooling,so the cooling during alloy solidification should be enhanced to avoid segregation.展开更多
The Nd_(60)Fe_(20)Al_8Co_(10)B_2 alloy was prepared by suction casting of the molten alloy into a copper mold under argon atmosphere. The micro-structural and magnetic property changes in the Nd_(60)Fe_(20)Al_8Co_(10)...The Nd_(60)Fe_(20)Al_8Co_(10)B_2 alloy was prepared by suction casting of the molten alloy into a copper mold under argon atmosphere. The micro-structural and magnetic property changes in the Nd_(60)Fe_(20)Al_8Co_(10)B_2 alloy during crystallization were investigated by X-ray diffraction (XRD), differential scanning calorimetry (DSC), scanning electron microscope (SEM) and the vibrating sample magnetometer (VSM). The precipitation and Nd-rich and Fe-rich phases have no significant effect on the intrinsic coercitity for Nd_(60)Fe_(20)Al_8Co_(10)B_2 alloy annealed below 723 K. However, the growth of Fe-rich phase decreases the saturate magnetization and remanence of the alloy. The hard magnetic behavior is disappeared when the alloy is fully crystallized.展开更多
文摘通过扫描电镜/能谱、X射线衍射以及金相分析,针对含0.3%Fe(质量分数)的Al Mg Si Cu铝合金,研究了Mn含量对其结晶相的影响。研究表明:合金在铸造过程中形成的结晶相为Al1.9CuMg4.1Si3.3,Al5(FeMn)Si,Al8(FeMn)2Si以及少量的Mg2Si;增大含Mn量,合金中AlFeMnSi型结晶相数量增多;对合金进行均匀化处理时,Al1.9CuMg4.1Si3.3相完全溶解,发生Al5(FeMn)Si向Al8(FeMn)2Si相的转变;对合金进行轧制及最终热处理后,结晶相碎化且沿轧向呈纤维状分布,但结晶相的类型不变。
基金financially supported by the National Natural Science Foundation of China(Grant No.51875365)。
文摘Segregation can seriously damage the mechanical properties of the aluminum alloys.6061 aluminum alloy wheel spokes were prepared by squeeze casting.To investigate the formation mechanism of segregation,the microstructure of the alloy was observed using scanning electron microscopy,energy dispersive spectrometry,X-ray diffraction and electron microprobe analysis methods.The Gibbs energy of each phase during solidification was calculated by JMat Pro.Results show that the segregation phases in the R-joint of the wheel spokes are mainly composed of Mg_(2)Si,β-Al Fe Si and Al_(5)Cu_(2)Mg_(8)Si_(6)intermetallics.During the solidification of the 6061 aluminum alloy wheels,Mg_(2)Si andα-Al Fe Si phases precipitate in the mushy zone at first.With the decrease of temperature,α-Al Fe Si transforms intoβ-Al Fe Si,while Al_(5)Cu_(2)Mg_(8)Si_(6)precipitates from the solid-state aluminum alloy after solidification.Segregation at the R-joint of wheel spokes is mainly caused by insufficient cooling,so the cooling during alloy solidification should be enhanced to avoid segregation.
文摘The Nd_(60)Fe_(20)Al_8Co_(10)B_2 alloy was prepared by suction casting of the molten alloy into a copper mold under argon atmosphere. The micro-structural and magnetic property changes in the Nd_(60)Fe_(20)Al_8Co_(10)B_2 alloy during crystallization were investigated by X-ray diffraction (XRD), differential scanning calorimetry (DSC), scanning electron microscope (SEM) and the vibrating sample magnetometer (VSM). The precipitation and Nd-rich and Fe-rich phases have no significant effect on the intrinsic coercitity for Nd_(60)Fe_(20)Al_8Co_(10)B_2 alloy annealed below 723 K. However, the growth of Fe-rich phase decreases the saturate magnetization and remanence of the alloy. The hard magnetic behavior is disappeared when the alloy is fully crystallized.
