In-situ synthesized ceramic such as TiC,Cr7C3 and Cr5B3 reinforced Ni-based alloy composite coating was fabricated on the surface of mild steel substrate by reactive braze coating processing with colloidal graphite,Cr...In-situ synthesized ceramic such as TiC,Cr7C3 and Cr5B3 reinforced Ni-based alloy composite coating was fabricated on the surface of mild steel substrate by reactive braze coating processing with colloidal graphite,Cr,Ni,ferro-boron,Si and titanium powders as the raw materials at low temperature of 1000℃,and a new kind of coating materials was developed.By means of SEM,EDS,XRD and surface hardness tester,the microstructures,phases,hardness and wear-resistance of the coating were analyzed,respectively.The results revealed that the coating was mainly composed of the ceramic in-situ synthesized reinforcement phases of TiC,Cr7C3 and Cr5B3 and the binder phases in-situ synthesized of Ni31Si12 and(Ni,Fe)solid solution;The ceramic reinforcement phases of TiC,Cr7C3 and Cr5B3 were randomly distributed in the binder phases of Ni31Si12 and(Ni,Fe)solid solution;The coating had about 15vol%pores and can possibly be applied as a self-lubrication coating;The coating and the substrate were integrated together by metallurgical bonding;The coating had a hardness up to 91-94HR15N.展开更多
Brazing is a suitable technology to join different materials such as cemented carbides and steel. Even though this technology has been investigated for many years, insufficient joints can occur easily, as the brazing ...Brazing is a suitable technology to join different materials such as cemented carbides and steel. Even though this technology has been investigated for many years, insufficient joints can occur easily, as the brazing process is very sensitive concerning the handling parameters. Defects such as voids and cracks are hard to detect by commonly used visual inspection methods. Other nondestructive methods such as radiography or ultrasonic testing are usually not economical for the examination of these joints. Studies proved that the electrical resistance has the potential to serve as an effective alternative for the evaluation of brazed joints. In this study, the authors have compared the electrical resistance and the shear strength. For this, cemented carbides were brazed to steel by means of induction heating at an ambient atmosphere. A silver-based filler metal （ BrazeTec 4900 / Ag 449 ） and a flux （ BrazeTec spezial h / FH12） were selected to enable the brazing process. The brazing time and the temperature were varied in order to produce different joint qualities. After brazing, the resistance was measured on each joint with the 4-point probe method to facilitate a high accuracy. The results underline the possibility to use electrical resistance measurements as an effective tool for a quality control of brazed joints.展开更多
A new hardfacing process, reactive braze coating process (RBCC) was studied, and (TiC+Cr_3C_2)/Fe composite coatings were prepared by RBCC using carbon, Cr_3C_2, iron, ferrochromium and titanium powder as the raw mate...A new hardfacing process, reactive braze coating process (RBCC) was studied, and (TiC+Cr_3C_2)/Fe composite coatings were prepared by RBCC using carbon, Cr_3C_2, iron, ferrochromium and titanium powder as the raw materials in vacuum braze furnace. The results show that TiC is in-situ synthesized in the coatings. The methods of introducing Cr_3C_2 have great effects on the distribution of TiC. Adding Cr_3C_2 directly to the raw materials for coatings, fine TiC particles aggregate into discoids parallel to the coating surface, whereas, in-situ synthesizing Cr_3C_2 in coatings, the aggregations of TiC are lumpish. During braze coating, Cr_3C_2 particles directly added dissolve and precipitate to become needle-shaped. The coatings have an even and smooth surface and are combined with their mild steel substrates by a metallurgical bonding.展开更多
基金supported by Yangjiang science and technology project (0202010067)Yangjiang polytechnic for providing financial assistance.
文摘In-situ synthesized ceramic such as TiC,Cr7C3 and Cr5B3 reinforced Ni-based alloy composite coating was fabricated on the surface of mild steel substrate by reactive braze coating processing with colloidal graphite,Cr,Ni,ferro-boron,Si and titanium powders as the raw materials at low temperature of 1000℃,and a new kind of coating materials was developed.By means of SEM,EDS,XRD and surface hardness tester,the microstructures,phases,hardness and wear-resistance of the coating were analyzed,respectively.The results revealed that the coating was mainly composed of the ceramic in-situ synthesized reinforcement phases of TiC,Cr7C3 and Cr5B3 and the binder phases in-situ synthesized of Ni31Si12 and(Ni,Fe)solid solution;The ceramic reinforcement phases of TiC,Cr7C3 and Cr5B3 were randomly distributed in the binder phases of Ni31Si12 and(Ni,Fe)solid solution;The coating had about 15vol%pores and can possibly be applied as a self-lubrication coating;The coating and the substrate were integrated together by metallurgical bonding;The coating had a hardness up to 91-94HR15N.
文摘Brazing is a suitable technology to join different materials such as cemented carbides and steel. Even though this technology has been investigated for many years, insufficient joints can occur easily, as the brazing process is very sensitive concerning the handling parameters. Defects such as voids and cracks are hard to detect by commonly used visual inspection methods. Other nondestructive methods such as radiography or ultrasonic testing are usually not economical for the examination of these joints. Studies proved that the electrical resistance has the potential to serve as an effective alternative for the evaluation of brazed joints. In this study, the authors have compared the electrical resistance and the shear strength. For this, cemented carbides were brazed to steel by means of induction heating at an ambient atmosphere. A silver-based filler metal （ BrazeTec 4900 / Ag 449 ） and a flux （ BrazeTec spezial h / FH12） were selected to enable the brazing process. The brazing time and the temperature were varied in order to produce different joint qualities. After brazing, the resistance was measured on each joint with the 4-point probe method to facilitate a high accuracy. The results underline the possibility to use electrical resistance measurements as an effective tool for a quality control of brazed joints.
文摘A new hardfacing process, reactive braze coating process (RBCC) was studied, and (TiC+Cr_3C_2)/Fe composite coatings were prepared by RBCC using carbon, Cr_3C_2, iron, ferrochromium and titanium powder as the raw materials in vacuum braze furnace. The results show that TiC is in-situ synthesized in the coatings. The methods of introducing Cr_3C_2 have great effects on the distribution of TiC. Adding Cr_3C_2 directly to the raw materials for coatings, fine TiC particles aggregate into discoids parallel to the coating surface, whereas, in-situ synthesizing Cr_3C_2 in coatings, the aggregations of TiC are lumpish. During braze coating, Cr_3C_2 particles directly added dissolve and precipitate to become needle-shaped. The coatings have an even and smooth surface and are combined with their mild steel substrates by a metallurgical bonding.
