For a detector in a capacitanee fuze working in an electrostatic field, the bomblength (effective length of the conductor part) is an important factor affecting the sensitivityof detection. For the two different kinds...For a detector in a capacitanee fuze working in an electrostatic field, the bomblength (effective length of the conductor part) is an important factor affecting the sensitivityof detection. For the two different kinds of detecting circuit models in general use (the frequency-sensitive and the amplitude-coupling ), mechanism of the effect of bomblength on the sensitvity of detection is analyzed. Through the analysis a conclusion in fullagreement with experimental results has been drawn, that is. the longer the bomb length,the higher the sensitivity, on the condition that the sizes and the sites of the detecting electrodes and bomb diameter remain unchanged.展开更多
Based on the study of the characteristics of the cloud, firstly the interference mechanism of the capacitance proximity fuze passing through the cloud has been studied. Analysis shows that the medium property of the c...Based on the study of the characteristics of the cloud, firstly the interference mechanism of the capacitance proximity fuze passing through the cloud has been studied. Analysis shows that the medium property of the cloud only, has little effect on the capacitance proximity fuze. Secondly, the adherence interference of the cloud to capacitance proximity fuze has been studied for the first time in this paper. Then finite element analysis (FEA) method has been used to simulate the adherence interference of the cloud. Simulation result shows that the cloud adherence effect interferes the output of the capacitance fuze greatly. At last, experiments have been made for the study of the cloud interference.展开更多
By employing an electrical micro-titration system, in which a capacitively coupled contactless conductivity detector(C^4D) was used to monitor the reaction process in real time, herein a novel method for determining...By employing an electrical micro-titration system, in which a capacitively coupled contactless conductivity detector(C^4D) was used to monitor the reaction process in real time, herein a novel method for determining ciprofloxacin hydrochloride(CIPHCl) was developed for the first time. Mode 1: Standard CIPHCl solutions at different concentrations were loaded into reaction cells, respectively, and were titrated with standard Ag^+. Upon the titration, the formation of a precipitate alters the number of ions in the solution, raising the change of conductivity, which was monitored by a special C-4 D to construct a titration curve. The endpoint of the titration was located from the peak of the curve. Between the elapsed time and the initial concentration of titrand, a linear relationship was established over the range of2.0–8.0 mmol/L. Mode 2: Standard Fe^3+ took the place of Ag^+, and was used as titrant to recognize ciprofloxacin contributed to the formation of complexation, which also resulting a change of solution conductivity. Under optimized conditions, a working range of 1.0–5.0 mmol/L CIPHCl was found. Because the reaction solutions were isolated from the working electrodes, this pioneer work shows significant simplicity and cost-effectiveness, by eliminating the requirements for detector exchange/renewal between different measurements, and by involving no auxiliary chemicals. Both of the two approaches were applied successfully to determine CIPHCl in tablet samples. And the results were in good agreement with those obtained by reference method.展开更多
文摘For a detector in a capacitanee fuze working in an electrostatic field, the bomblength (effective length of the conductor part) is an important factor affecting the sensitivityof detection. For the two different kinds of detecting circuit models in general use (the frequency-sensitive and the amplitude-coupling ), mechanism of the effect of bomblength on the sensitvity of detection is analyzed. Through the analysis a conclusion in fullagreement with experimental results has been drawn, that is. the longer the bomb length,the higher the sensitivity, on the condition that the sizes and the sites of the detecting electrodes and bomb diameter remain unchanged.
文摘Based on the study of the characteristics of the cloud, firstly the interference mechanism of the capacitance proximity fuze passing through the cloud has been studied. Analysis shows that the medium property of the cloud only, has little effect on the capacitance proximity fuze. Secondly, the adherence interference of the cloud to capacitance proximity fuze has been studied for the first time in this paper. Then finite element analysis (FEA) method has been used to simulate the adherence interference of the cloud. Simulation result shows that the cloud adherence effect interferes the output of the capacitance fuze greatly. At last, experiments have been made for the study of the cloud interference.
基金financial support from Key R&D of Shandong Province (No. 2016GSF120008)Qingdao National Laboratory for Marine Science and Technology (No. 2015ASKJ02-05)
文摘By employing an electrical micro-titration system, in which a capacitively coupled contactless conductivity detector(C^4D) was used to monitor the reaction process in real time, herein a novel method for determining ciprofloxacin hydrochloride(CIPHCl) was developed for the first time. Mode 1: Standard CIPHCl solutions at different concentrations were loaded into reaction cells, respectively, and were titrated with standard Ag^+. Upon the titration, the formation of a precipitate alters the number of ions in the solution, raising the change of conductivity, which was monitored by a special C-4 D to construct a titration curve. The endpoint of the titration was located from the peak of the curve. Between the elapsed time and the initial concentration of titrand, a linear relationship was established over the range of2.0–8.0 mmol/L. Mode 2: Standard Fe^3+ took the place of Ag^+, and was used as titrant to recognize ciprofloxacin contributed to the formation of complexation, which also resulting a change of solution conductivity. Under optimized conditions, a working range of 1.0–5.0 mmol/L CIPHCl was found. Because the reaction solutions were isolated from the working electrodes, this pioneer work shows significant simplicity and cost-effectiveness, by eliminating the requirements for detector exchange/renewal between different measurements, and by involving no auxiliary chemicals. Both of the two approaches were applied successfully to determine CIPHCl in tablet samples. And the results were in good agreement with those obtained by reference method.