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Improved calibration method for displacement transformation coefficient in optical and visual measurements
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作者 Haopeng Li Zurong Qiu 《Nanotechnology and Precision Engineering》 CAS CSCD 2023年第1期12-25,共14页
Optical and visual measurement technology is used widely in fields that involve geometric measurements,and among such technology are laser and vision-based displacement measuring modules(LVDMMs).The displacement trans... Optical and visual measurement technology is used widely in fields that involve geometric measurements,and among such technology are laser and vision-based displacement measuring modules(LVDMMs).The displacement transformation coefficient(DTC)of an LVDMM changes with the coordinates in the camera image coordinate system during the displacement measuring process,and these changes affect the displacement measurement accuracy of LVDMMs in the full field of view(FFOV).To give LVDMMs higher accuracy in the FFOV and make them adaptable to widely varying measurement demands,a new calibration method is proposed to improve the displacement measurement accuracy of LVDMMs in the FFOV.First,an image coordinate system,a pixel measurement coordinate system,and a displacement measurement coordinate system are established on the laser receiving screen of the LVDMM.In addition,marker spots in the FFOV are selected,and the DTCs at the marker spots are obtained from calibration experiments.Also,a fitting method based on locally weighted scatterplot smoothing(LOWESS)is selected,and with this fitting method the distribution functions of the DTCs in the FFOV are obtained based on the DTCs at the marker spots.Finally,the calibrated distribution functions of the DTCs are applied to the LVDMM,and experiments conducted to verify the displacement measurement accuracies are reported.The results show that the FFOV measurement accuracies for horizontal and vertical displacements are better than±15μm and±19μm,respectively,and that for oblique displacement is better than±24μm.Compared with the traditional calibration method,the displacement measurement error in the FFOV is now 90%smaller.This research on an improved calibration method has certain significance for improving the measurement accuracy of LVDMMs in the FFOV,and it provides a new method and idea for other vision-based fields in which camera parameters must be calibrated. 展开更多
关键词 Displacement transformation coefficient(DTC) Laser and vision-based displacement measuring module(LVDMM) Displacement measurement Locally weighted scatterplot smoothing(LOWESS) calibration method
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Practical calibration method for instantaneous polarization radar systems utilizing a metal sphere 被引量:2
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作者 杨凝 赵国强 +1 位作者 孙厚军 吕昕 《Journal of Beijing Institute of Technology》 EI CAS 2014年第2期248-253,共6页
A practical calibration method is proposed for instantaneous polarization radar systems.The method only needs one measurement by using a metal sphere.The distortions of system and the actual polarization scattering ma... A practical calibration method is proposed for instantaneous polarization radar systems.The method only needs one measurement by using a metal sphere.The distortions of system and the actual polarization scattering matrix(PSM)of target can be obtained.First,an instantaneous polarization radar system is presented.The system can obtain PSM by a single pulse echo.The dual-polarization antenna can transmit and receive two orthogonal polarization waves.The multilayer micro-strip patch antenna is adopted for this kind of radar system.Second,based on the multi-port network theory,the operation and system errors of instantaneous polarization radar system are analyzed.By making assumption on the cross-talk factors of antenna,distortion matrices of R and Tare derived.Finally,the calibration method based on instantaneous polarization measurement is introduced.Simulation results show the performance of this calibration method.The values of calibrated PSM are in agreement with the actual ones after calibration. 展开更多
关键词 polarization scattering matrix(PSM) instantaneous polarization radar system distortion ma-trix calibration method
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Study on the Drift Calibration Method and Device for the Tin Oxide pH Electrode
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作者 Chu-Neng Tsai Jung-Chuan Chou +1 位作者 Tai-Ping Sun Shen-Kan Hsiung 《稀有金属材料与工程》 SCIE EI CAS CSCD 北大核心 2006年第A03期210-212,共3页
Drift phenomenon has been known as the drawback of sensors and causes inaccuracy on the long-term measurement. In general,there are two methods to reduce the drift problem.One is to tune the parameters of the fabricat... Drift phenomenon has been known as the drawback of sensors and causes inaccuracy on the long-term measurement. In general,there are two methods to reduce the drift problem.One is to tune the parameters of the fabrication process to improve the properties of the front-ended device.Another is to compensate the drift phenomenon by adding extra drift compensation circuit or software in the back-ended readout circuit.In this study,a drift calibration method for the potentiometric sensor was presented and the drift calibration method was performed by using the circuit.According to experimental results,the drift phenomenon of the SnO_2 pH electrode was reduced by the drift calibration device. 展开更多
关键词 drift phenomenon long-term measurement drift calibration method drift calibration device SnO2 pH electrode
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Optimised Calibration Method for Six-Port Junction
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作者 熊祥正 廖成 肖华清 《Journal of Southwest Jiaotong University(English Edition)》 2008年第4期392-397,共6页
A dual-tone technique is used to produce multi-samples in optimising calibration of six-port junction. More accurate results are achieved by using the least-square method and excluding those samples which may cause bi... A dual-tone technique is used to produce multi-samples in optimising calibration of six-port junction. More accurate results are achieved by using the least-square method and excluding those samples which may cause bigger errors. A 0.80 -1.10 GHz microwave integrated circuit (MIC) six-port reflectometer is constructed. Nine test samples are used in the measurement. With Engen's calibration procedure, the difference between the HP8510 and the six-port reflectrometer is in the order of 0.20 dB/1.5° for most cases, above 0.50 dB/5.0° at boundary frequency. With the optimised method, the difference is less than 0. 10 dB/1.0° for most cases, and the biggest error is 0.42 dB/2.1° for boundary frequencies. 展开更多
关键词 Six-port junction calibration method Dual-tone technique
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A universal calibration method for eliminating topographydependent current in conductive AFM and its application in nanoscale imaging
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作者 Chunlin Hao Hao Xu +7 位作者 Shiquan Lin Yaju Zhang Jinmiao He Bei Liu Yuanzheng Zhang Banghao Wu Guozhen Shen Haiwu Zheng 《Nano Research》 SCIE EI CSCD 2024年第7期6509-6517,共9页
The topography and electrical properties are two crucial characteristics that determine the roles and functionalities of materials.Conductive atomic force microscopy(CAFM)is widely recognized for its ability to indepe... The topography and electrical properties are two crucial characteristics that determine the roles and functionalities of materials.Conductive atomic force microscopy(CAFM)is widely recognized for its ability to independently measure the topography and conductivity.The increasing trend towards miniaturization in electrical devices and sensors has encouraged an urgent demand for enhancing the accuracy of CAFM characterization.However,when performing CAFM tests on Bi_(0.5)Na_(0.5)TiO_(3)bulk ceramic,it is interesting to observe significant currents related to the topography.Why do insulators exhibit“conductivity”in CAFM testing?Herein,we thoroughly investigated the topography-dependent current during CAFM testing for the first time.Based on the linear dependence between the current and the first derivative of topography,the calibration method has been proposed to eliminate the topographic crosstalk.This method is evaluated on Bi_(0.5)Na_(0.5)TiO_(3)bulk ceramic,one-dimensional(1D)ZnO nanowire,twodimensional(2D)NbOI_(2)flake,and biological lotus leaf.The corresponding results of negligible topography-interference current affirm the feasibility and universality of this calibration method.This work effectively addresses the challenge of topographic crosstalk in CAFM characterization,thereby preventing the erroneous estimation of the conductivity of any unknown sample. 展开更多
关键词 conductive atomic force microscopy topographic crosstalk current error calibration method
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Calibration of Soil Electromagnetic Conductivity in Inverted Salinity Profiles with an Integration Method 被引量:9
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作者 YAO Rong-Jian YANG Jin-Song LIU Guang-Ming 《Pedosphere》 SCIE CAS CSCD 2007年第2期246-256,共11页
Various calibration methods have been propounded to determine profiles of apparent bulk soil electrical conductivity (ECa) and soil electrical conductivity of a saturated soil paste extract (ECe) or a 1:5 soil water e... Various calibration methods have been propounded to determine profiles of apparent bulk soil electrical conductivity (ECa) and soil electrical conductivity of a saturated soil paste extract (ECe) or a 1:5 soil water extract (EC1:5) using an electromagnetic induction instrument (EM38). The modeled coefficients, one of the successful and classical methods hitherto, were chosen to calibrate the EM38 measurements of the inverted salinity profiles of characteristic coastal saline soils at selected sites of Xincao Farm, Jiangsu Province, China. However, this method required three parameters for each depth layer. An integration approach, based on an exponential decay profile model, was proposed and the model was fitted to all the calibration sites. The obtained model can then be used to predict EC1:5 at a certain depth from electromagnetic measurements made using the EM38 device positioned in horizontal and vertical positions at the soil surface. This exponential decay model predicted the EC1:5 well according to the results of a one-way analysis of variance, and the further comparison indicated that the modeled coefficients appeared to be slightly superior to, but not statistically different from, this exponential decay model. Nevertheless, this exponential decay model was more significant and practical because it depended on less empirical parameters and could be used to perform point predictions of EC1:5 continuously with depth. 展开更多
关键词 coastal saline soils electromagnetic conductivity exponential decay model integration calibration method inverted salinity profiles
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Calibration method to improve the accuracy of THz imaging and spectroscopy in reflection geometry 被引量:5
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作者 Shuting Fan Edward P.J.Parrott +1 位作者 Benjamin S.Y.Ung Emma Pickwell-MacPherson 《Photonics Research》 SCIE EI 2016年第3期29-35,共7页
We introduce a novel method to accurately extract the optical parameters in terahertz reflection imaging. Our method builds on standard self-referencing methods using the reflected signal from the bottom of the imagin... We introduce a novel method to accurately extract the optical parameters in terahertz reflection imaging. Our method builds on standard self-referencing methods using the reflected signal from the bottom of the imaging window material to further compensate for time-dependent system fluctuations and position-dependent variation in the window thickness. Our proposed method not only improves the accuracy, but also simplifies the imaging procedure and reduces measurement times. 展开更多
关键词 calibration method to improve the accuracy of THz imaging and spectroscopy in reflection geometry THZ
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A calibration method for optical trap force by use of electrokinetic phenomena
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作者 喻有理 张镇西 张孝林 《Chinese Optics Letters》 SCIE EI CAS CSCD 2006年第9期529-531,共3页
An experimental method for calibration of optical trap force upon cells by use of electrokinetic phenomena is demonstrated. An electronkinetic sample chamber system (ESCS) is designed instead of a common sample cham... An experimental method for calibration of optical trap force upon cells by use of electrokinetic phenomena is demonstrated. An electronkinetic sample chamber system (ESCS) is designed instead of a common sample chamber and a costly automatism stage, thus the experimental setup is simpler and cheaper. Experiments indicate that the range of the trap force measured by this method is piconewton and sub-piconewton, which makes it fit for study on non-damage interaction between light and biological particles with optical tweezers especially. Since this method is relevant to particle electric charge, by applying an alternating electric field, the new method may overcome the problem of correcting drag force and allow us to measure simultaneously optical trap stiffness and particle electric charge. 展开更多
关键词 OTF A calibration method for optical trap force by use of electrokinetic phenomena
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Resolving double-sided inverse heat conduction problem using calibration integral equation method
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作者 CHEN Hong-chu 《Journal of Central South University》 SCIE EI CAS CSCD 2019年第8期2100-2108,共9页
In this paper, a novel calibration integral equation is derived for resolving double-sided, two-probe inverse heat conduction problem of surface heat flux estimation. In contrast to the conventional inverse heat condu... In this paper, a novel calibration integral equation is derived for resolving double-sided, two-probe inverse heat conduction problem of surface heat flux estimation. In contrast to the conventional inverse heat conduction techniques, this calibration approach does not require explicit input of the probe locations, thermophysical properties of the host material and temperature sensor parameters related to thermal contact resistance, sensor capacitance and conductive lead losses. All those parameters and properties are inherently contained in the calibration framework in terms of Volterra integral equation of the first kind. The Laplace transform technique is applied and the frequency domain manipulations of the heat equation are performed for deriving the calibration integral equation. Due to the ill-posed nature, regularization is required for the inverse heat conduction problem, a future-time method or singular value decomposition (SVD) can be used for stabilizing the ill-posed Volterra integral equation of the first kind. 展开更多
关键词 inverse heat conduction problem surface heat flux estimation calibration integral equation method
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A methodology for laser tool setters calibration and its precise mathematical model
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作者 Tao FANG Zixi FANG +1 位作者 Ze Zhong CHEN Zhiyong CHANG 《Chinese Journal of Aeronautics》 SCIE EI CAS CSCD 2024年第7期564-581,共18页
On-machine tool setting is a pivotal approach in achieving intelligent manufacturing,and laser tool setters have become a crucial component of smart machine tools.Laser tool setters play a crucial role in precisely me... On-machine tool setting is a pivotal approach in achieving intelligent manufacturing,and laser tool setters have become a crucial component of smart machine tools.Laser tool setters play a crucial role in precisely measuring the dimensions of cutting tools during the part machining process,focusing on tool length and diameter.As a measuring instrument,the positions of the laser axis of the laser tool setter need to be accurately calibrated before use.However,in actual calibration scenarios,traditional calibration methods face challenges due to installation errors in the tool setter and geometric errors in the measuring rod.To address this issue,this study proposes a novel calibration method.Initially,the calibration mechanism of the laser beam axis is established.Based on the accurate mathematical model of the laser beam and the measuring rod,and using the polygon clipping algorithm,the mathematical mechanism of the laser tool setter’s work is established.Then,a novel method is introduced to calculate the compensation distance between the laser beam reference point and the rod bottom center point at each moment during calibration.Furthermore,by utilizing the kinematic chain of the tool setter calibration system,a new calibration method is developed to accurately calibrate the position of the laser beam axis in the machine tool coordinate system.Finally,the accuracy of the calibration method is verified through simulation experiments and calibration tests.This method improves the calibration accuracy of the tool setter,and the mathematical model of the laser tool setter can be extended to the measurement of tools,thereby improving the precision of tool measurements.This research significantly improves the efficient production performance of smart machine tools. 展开更多
关键词 On-machine tool setting Smart machine tools Mathematical model calibration method Laser tool sette
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System for Measuring Elevator Guide Rail Quality and Its Calibration
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作者 李醒飞 HU S Jack +1 位作者 张国雄 郭敬滨 《Transactions of Tianjin University》 EI CAS 2006年第2期84-91,共8页
A system for measuring the quality parameters of elevator guide rails is developed. The quality parameters the system can measure include straightness, flatness, squareness, width and height of the rail. The system co... A system for measuring the quality parameters of elevator guide rails is developed. The quality parameters the system can measure include straightness, flatness, squareness, width and height of the rail. The system consists of six parts:main guideway, auxiliary guideway, reference rail, saddle, control casing and measured rail. The guide rail to be measured is mounted on a bed. The straightness errors of surfaces are checked by five linear displacement sensors mounted on the saddle. The deviation of readings from the sensor, which is in contact with top guiding surface, gives the straightness error of the surface and height of the rail. The other four sensors are used to measure side guiding surfaces respectively and give other parameters including flatness on the surfaces, squareness, width and height of the rail. A novel calibration method is also developed to calibrate the straightness motion error of the system in horizontal and vertical directions. The deflection deformation of the measured rail is fitted by using a fourth-order polynomial. Experimental results show that the uncertainty of the system on the side surfaces after compensating the straightness motion error is less than 0. 01 mm, and the uncertainty of the system on the top surface after compensating the straightness motion error and the deflection deformation of the rail is less than 0. 03 mm. 展开更多
关键词 error compensation elevator rail calibration method
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Study on Calibration of L-band Radar by a Drone
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作者 Yi ZHANG Xiaolei CHEN 《Meteorological and Environmental Research》 CAS 2021年第3期32-33,37,共3页
A new calibration method of L-band radar accuracy using a rotary-wing drone equipped with"GPS"satellite positioning system was proposed.The L-band radar calibration system scheme based on this method was des... A new calibration method of L-band radar accuracy using a rotary-wing drone equipped with"GPS"satellite positioning system was proposed.The L-band radar calibration system scheme based on this method was designed.The theoretical basis required for system realization was studied,and the system calibration method was given.The calibration results referred to the domestic new generation weather radar antenna beam pointing calibration technical indicator(≤0.3°),and its accuracy met relevant business requirement.It show that this method can easily and quickly complete the radar system calibration.Compared with the traditional radar calibration method,it is more convenient,less affected by surrounding environment,and has low requirements on the weather. 展开更多
关键词 Radar calibration Rotary-wing drone "GPS"positioning system calibration method
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Relative flux calibration for the Guoshoujing Telescope (LAMOST) 被引量:5
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作者 Yi-Han Song A-Li Luo +7 位作者 Georges Comte Zhong-Rui Bai Jian-Nan Zhang Wei Du Hao-Tong Zhang Jian-Jun Chen Fang Zuo Yong-Heng Zhao 《Research in Astronomy and Astrophysics》 SCIE CAS CSCD 2012年第4期453-464,共12页
This paper presents a relative flux calibration method for the Guoshoujing Telescope (LAMOST), which may be applied to connect a blue spectrum to a red spectrum to build the whole spectrum across the total wavelengt... This paper presents a relative flux calibration method for the Guoshoujing Telescope (LAMOST), which may be applied to connect a blue spectrum to a red spectrum to build the whole spectrum across the total wavelength range (3700 ~ 9000 A). In each spectrograph, we estimate the effective temperatures of selected stars using a grid of spectral line indices in the blue spectral range and a comparison with stellar atmosphere models. For each spectrograph, stars of types A and F are selected as pseudo-standard stars, and the theoretical spectra are used to calibrate both the blue (3700 ~ 5900 A) and red spectrograph arms (5700 ~ 9000 A). Then the spectral response function for these pseudo-standard stars could be used to correct the raw spectra provided by the other fibers of the spectrograph, after a fiber efficiency function has been derived from twilight flat-field exposures. A key problem in this method is the fitting of a pseudo stellar continuum, so we also give a detailed description of this step. The method is tested by comparing a small sample of LAMOST spectra calibrated in this way on stars also observed by the Sloan Digital Sky Survey. The result shows that the T eff estimation and relative flux calibration method are adequate. 展开更多
关键词 techniques: spectroscopic calibration methods:data analysis
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Calibration of Discrete Element Heat Transfer Parameters by Central Composite Design 被引量:1
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作者 Zongquan DENG Jinsheng CUI +1 位作者 Xuyan HOU Shengyuan JIANG 《Chinese Journal of Mechanical Engineering》 SCIE EI CAS CSCD 2017年第2期419-427,共9页
The efficiency and precision of parameter calibration in discrete element method (DEM) are not satisfactory, and parameter calibration for granular heat transfer is rarely involved. Accordingly, parameter calibratio... The efficiency and precision of parameter calibration in discrete element method (DEM) are not satisfactory, and parameter calibration for granular heat transfer is rarely involved. Accordingly, parameter calibration for granular heat transfer with the DEM is studied. The heat transfer in granular assemblies is simulated with DEM, and the effective thermal conductivity (ETC) of these granular assemblies is measured with the transient method in simulations. The measurement testbed is designed to test the ETC of the granular assemblies under normal pressure and a vacuum based on the steady method. Central composite design (CCD) is used to simulate the impact of the DEM parameters on the ETC of granular assemblies, and the heat transfer parameters are calibrated and compared with experimental data. The results show that, within the scope of the considered parameters, the ETC of the granular assemblies increases with an increasing particle thermal conductivity and decreases with an increasing particle shear modulus and particle diameter. The particle thermal conductivity has the greatest impact on the ETC of granular assemblies followed by the particle shear modulus and then the particle diameter. The calibration results show good agreement with the experimental results. The error is less than 4%, which is within a reasonable range for the scope of the CCD parameters. The proposed research provides high efficiency and high accuracy parameter calibration for granular heat transfer in DEM. 展开更多
关键词 Granular assembly · Parameter calibration · Effective thermal conductivity (ETC) · Discrete element method (DEM) · Central composite design (CCD) · Vacuum
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A method to determine the bonded-particle model parameters for simulation of ores
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作者 Shuwei Wu Guoqiang Wang +4 位作者 Longfei Fan Wei Guan Jianbo Guo Zhengbin Liu Yukuan Wang 《Particuology》 SCIE EI CAS CSCD 2024年第3期24-38,共15页
The bonded-particle model(BPM)is commonly used in the numerical analysis of ore samples.To improve the accuracy of simulating the mechanical process of ore process of ore crushing in a crusher,the parameters of the BP... The bonded-particle model(BPM)is commonly used in the numerical analysis of ore samples.To improve the accuracy of simulating the mechanical process of ore process of ore crushing in a crusher,the parameters of the BPM for the ore must be calibrated.In this study,a calibration method was proposed for the scientific determination of the parameters of the BPM for ore undergoing uniaxial compression.First,physical tests and simulations were conducted to determine the mechanical response(uniaxial compressive strength and macroscopic stiffness)of ore during uniaxial compression.Then,the sensitivity of the mechanical response to the values of microscopic parameters was tested using a Plackett-Burman design.Next,the microscopic parameters with the greatest impact on the response were identified,and the range of parameters that met the target response was determined using a steepest ascent design;Second,a second-order model of the mechanical response was established using the sensitive parameters by combining a Box-Behnken design with response surface methodology to obtain the optimal BPM parameters.Simulation tests showed that the normal stiffness per unit area,critical shear stress,and bonded disk radius had significant effects on the uniaxial compressive strength(UCS)and macroscopic stiffness(MS).To verify the validity of the proposed calibration method,laboratory tests were conducted.The consistency of the simulation results with experimental results indicated that response surface methodology with the Plackett-Burman design,steepest ascent design,and Box-Behnken design can be an effective method for calibrating the BPM of ores. 展开更多
关键词 Bonded-particle model Discrete element method calibration method Design of experiment Uniaxial compression test
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Theoretical Research and Experimental Validation of Elastic Dynamic Load Spectra on Bogie Frame of High-speed Train 被引量:13
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作者 ZHU Ning SUN Shouguang +1 位作者 LI Qiang ZOU Hua 《Chinese Journal of Mechanical Engineering》 SCIE EI CAS CSCD 2016年第3期498-506,共9页
When a train runs at high speeds, the external exciting frequencies approach the natural frequencies of bogie critical components, thereby inducing strong elastic vibrations. The present international reliability test... When a train runs at high speeds, the external exciting frequencies approach the natural frequencies of bogie critical components, thereby inducing strong elastic vibrations. The present international reliability test evaluation standard and design criteria of bogie frames are all based on the quasi-static deformation hypothesis. Structural fatigue damage generated by structural elastic vibrations has not yet been included. In this paper, theoretical research and experimental validation are done on elastic dynamic load spectra on bogie frame of high-speed train. The construction of the load series that correspond to elastic dynamic deformation modes is studied. The simplified form of the load series is obtained. A theory of simplified dynamic load–time histories is then deduced. Measured data from the Beijing–Shanghai Dedicated Passenger Line are introduced to derive the simplified dynamic load–time histories. The simplified dynamic discrete load spectra of bogie frame are established. Based on the damage consistency criterion and a genetic algorithm, damage consistency calibration of the simplified dynamic load spectra is finally performed. The computed result proves that the simplified load series is reasonable. The calibrated damage that corresponds to the elastic dynamic discrete load spectra can cover the actual damage at the operating conditions. The calibrated damage satisfies the safety requirement of damage consistency criterion for bogie frame. This research is helpful for investigating the standardized load spectra of bogie frame of high-speed train. 展开更多
关键词 elastic dynamic load spectra finite element method modal deformation calibration bogie frame high-speed train
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Method for in situ calibration of multiple feedback interferometers 被引量:1
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作者 谈宜东 曾召利 +2 位作者 张书练 张鹏 陈浩 《Chinese Optics Letters》 SCIE EI CAS CSCD 2013年第10期90-92,共3页
A method is presented for in situ resolution calibration of multiple feedback interferometers(MFIs) using two lasers with di?erent feedback levels simultaneously. The laser with weak optical feedback level generates h... A method is presented for in situ resolution calibration of multiple feedback interferometers(MFIs) using two lasers with di?erent feedback levels simultaneously. The laser with weak optical feedback level generates half-wavelength optical fringes, whereas the laser with strong multiple feedback level generates optical nanofringes. By using this method, the number of displaced optical nano-fringes can be easily counted, and the resolution of the MFIs can be accurately determined. The integrated MFIs can be used to measure displacements and calibrate other displacement sensors. 展开更多
关键词 method for in situ calibration of multiple feedback interferometers
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Quantitative Analysis of Fe Content in Iron Ore via External Calibration in Conjunction with Internal Standardization Method Coupled with LIBS 被引量:2
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作者 SHENG Liwen ZHANG Tianlong +2 位作者 WANG Kang TANG Hongsheng LI Hua 《Chemical Research in Chinese Universities》 SCIE CAS CSCD 2015年第1期107-111,共5页
The external calibration in conjunction with internal standardization(ECIS) coupled with laser-induced breakdown spectroscopic(LIBS) technique was proposed to perform the quantitative analysis of Fe content in iro... The external calibration in conjunction with internal standardization(ECIS) coupled with laser-induced breakdown spectroscopic(LIBS) technique was proposed to perform the quantitative analysis of Fe content in iron ore The plasma temperature and the electron number density were calculated to prove that the plasma was under local thermodynamic equilibrium(LTE) conditions and to ensure that the integral intensities of Fe I lines were reasonable. In addition, the result of the quantitative analysis shows a content of (20.26±0.59)% by mass of Fe in the iron ore. It was determined by four calibration curves, drawn for four emission lines of Fe I(373.48, 373.71,404.58 and 438.35 nm) normalized by Mn I line, base on the ECIS method which can eliminate the influence of matrix effect and improve the accuracy of quantitative analysis, compared with the standard addition method. Both the results of these two analytical methods were compared with that listed in the Standard Substance Certificate. The percentage content of Fe in the same sample of iron ore by the ECIS method was (20.17±0.08)% by mass, which shows a good performance to analyze the Fe content of iron ore in combination with LIBS. 展开更多
关键词 Laser-induced breakdown spectroscopy(LIBS) External calibration in conjunction with internal standardization(ECIS) method Chemical analysis Iron ore
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Method study and uncertainty analysis of calibration coefficients validation based on the Inner Mongolia test site 被引量:1
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作者 GAO HaiLiang GU XingFa +3 位作者 YU Tao GONG Hui LI JiaGuo LI XiaoYing 《Science China Earth Sciences》 SCIE EI CAS 2013年第9期1540-1547,共8页
Calibration coefficients validation is the foundation for ascertaining the sensor performance and carrying out the quantitative application.Based on the analysis of the differences between the calibration and validati... Calibration coefficients validation is the foundation for ascertaining the sensor performance and carrying out the quantitative application.Based on the analysis of the differences between the calibration and validation,two calibration coefficients validation methods were introduced in this paper.Taking the HJ-1A satellite CCD1 camera as an example,the uncertainties of calibration coefficients validation were analyzed.The calibration coefficients validation errors were simulated based on the measured data at an Inner Mongolia test site.The result showed that in the large view angle,the ground directional reflectance variation and the atmospheric path variation were the main error sources in calibration coefficients validation.The ground directional reflectance correction and atmospheric observation angle normalization should be carried out to improve the validation accuracy of calibration coefficients. 展开更多
关键词 method study and uncertainty analysis of calibration coefficients validation based on the Inner Mongolia test site
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New method for calibration of sun photometers
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作者 H.H.Asadov I.G.Chobanzadeh 《Chinese Optics Letters》 SCIE EI CAS CSCD 2009年第9期760-763,共4页
A new method for calibration of sun photometers based on Bouguer-Beer law is proposed. The developed basic equation of calibration makes it possible to formulate the derivative methods of calibration on the basis of p... A new method for calibration of sun photometers based on Bouguer-Beer law is proposed. The developed basic equation of calibration makes it possible to formulate the derivative methods of calibration on the basis of photometric measurements upon optical air masses, the ratio of which is an integer number. 展开更多
关键词 New method for calibration of sun photometers 双入
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