In order to evaluate the feasibility of steel slag powder as filler,the coating properties of steel slag and limestone aggregate were compared by water boiling test,the micro morphology difierences between steel slag ...In order to evaluate the feasibility of steel slag powder as filler,the coating properties of steel slag and limestone aggregate were compared by water boiling test,the micro morphology difierences between steel slag powder and mineral powder(limestone powder)were compared by scanning electron microscope(SEM),and the high-temperature rheological properties of asphalt mortar with difierent ratio of filler quality to asphalt quality(F/A)and difierent substitution rates of mineral powder(S/F)were studied by dynamic shear rheological test.The results show that the surface microstructure of steel slag powder is more abundant than that of mineral powder,and the adhesion of steel slag to asphalt is better than that of limestone.At the same temperature,the lower the ratio of S/F is,the greater the rutting factor and complex modulus will be.In addition,the complex modulus and rutting factor of the asphalt mortar increase with the increase of F/A,and the filler type and F/A have a negligible efiect on the phase angle.展开更多
This study aims to investigate the efiect of the mesoscopic characteristics of mineral powder fillers on the rutting resistance of asphalt mortar.Extraction and sieving tests were used to obtain the buton rock asphalt...This study aims to investigate the efiect of the mesoscopic characteristics of mineral powder fillers on the rutting resistance of asphalt mortar.Extraction and sieving tests were used to obtain the buton rock asphalt(BRA)ash with particle size smaller than 0.075 mm,which is consistent with that of the conventional mineral powder.The mesoscopic characteristics of BRA ash and conventional mineral powder were measured by SEM image analysis and the osmotic free pressure water method.Mesoscopic structure models of structural and free asphalts in mortar were obtained.The 70#matrix asphalt was used to prepare two kinds of asphalt mortar with BRA ash and conventional mineral powders fillers.The rutting factor of the two asphalt mortars was tested by dynamic shear test(DSR).Test results show that the ash extracted from BRA has a similar mesoscopic classification with the conventional mineral powder.Still,its fractal dimensions are larger,indicating the particles in BRA ash have more complex shapes and rougher surfaces,which is beneficial for forming structural asphalt and subsequently increasing the rutting factor(G*/sinδ),i e,improving the rutting resistance of the asphalt mortar.展开更多
To understand the effects offiller-asphalt ratio on different properties of lignin and polyesterfiber reinforced shape memory polyurethane(SMPU)/styrene butadiene styrene(SBS)composite modified asphalt mortar(PSAM),as we...To understand the effects offiller-asphalt ratio on different properties of lignin and polyesterfiber reinforced shape memory polyurethane(SMPU)/styrene butadiene styrene(SBS)composite modified asphalt mortar(PSAM),as well as to reveal the reinforcing and toughening mechanisms of lignin and polyesterfibers on PSAM,SMPU,SBS and mineral powder werefirst utilized to prepare PSAM.Then the conventional,rheological and anti-cracking properties of ligninfiber reinforced PSAM(LFAM)and polyesterfiber reinforced PSAM(PFAM)at dif-ferentfiller-asphalt ratios were characterized.Test results indicate that the shear strength,deformation resistance and viscosity are increased after adding 0.8wt%ligninfiber or polyesterfiber and increasing thefiller-asphalt ratio from 0.8 to 1.2.The optimalfiller-asphalt ratio of 1.0 is proposed after comprehensive performance assessments of PSAM.Polyesterfiber shows a better reinforcing effect than ligninfiber,but its improvement in the thermal stability of PSAM is not significant at high temperatures.Additionally,the complex modulus,storage modulus,loss modulus and rutting resistance factor of PSAM are improved after adding ligninfiber and polyesterfiber,as well as show an increasing trend as thefiller-asphalt ratio is raised,but the phase angle is gradually decreased.Further,the increase of elastic components in PSAM effectively enhances the anti-deformation ability of PSAM at high temperatures,and polyesterfiber more obviously improves the high-temperature deformation resistance of PSAM than ligninfiber.Finally,the anti-cracking performance of PFAM and LFAM at low temperatures is reduced by 74.2%and 46.7%,respectively,as thefiller-asphalt ratio is raised from 0.8 to 1.2.The low-temperature anti-cracking performance of LFAM is lower than that of PFAM at the samefiller-asphalt ratio,even lower than that of PSA.Compared with ligninfiber,the anti-cracking performance and deformation resistance of PSAM at low temperature is more greatly enhanced by polyester fiber.展开更多
In this paper we investigate the reinforcement mechanism of high viscosity rubber/SBS modified asphalt mortar mixed with fiber (mineral, lignin or carbon fiber) and deoiled asphalt (DOA). The softening point, pene...In this paper we investigate the reinforcement mechanism of high viscosity rubber/SBS modified asphalt mortar mixed with fiber (mineral, lignin or carbon fiber) and deoiled asphalt (DOA). The softening point, penetration and viscosity tests were conducted to characterize the engineering properties of asphalt-fiber mortar. The microstructure of fiber was observed using scanning electron microscopy (SEM), and the results indicated that fiber can effectively improve the toughness of asphalt matrix through forming a spatial network structure, and then adhesion and stabilization of asphalt binder. The cone penetration test was designed to study the rheological property of fiber modified asphalt. The results indicated that the reinforcement effect increased with fibers and DOA fraction increasing to a certain threshold, and the optimal fiber content was dependent on the fiber type and its length. Fiber content and filler-asphalt ratio had significant effects on the softening point, penetration, viscosity and cone penetration of asphalt mortar.展开更多
The compressive strength developing process and the microstructure of cement-asphalt mortar (CA mortar) were investigated.The fluidity of CA mortar has a great influence on its strength.The optimum value of spread d...The compressive strength developing process and the microstructure of cement-asphalt mortar (CA mortar) were investigated.The fluidity of CA mortar has a great influence on its strength.The optimum value of spread diameter of slump flow test is in the range of 300 to 400 mm.The compressive strength of CA mortar keeps a relatively high growth rate in 56 days and grows slowly afterwards.The residual water of hydration in CA mortar freezes under minus environmental temperature which can lead to a significant reduction of the strength of CA mortar.Increasing A/C retards asphalt emulsion splitting and thus prolongs the setting process of CA mortar.The hydration products of cement form the major structural framework of hardened CA mortar and asphalt is a weak phase in the framework but improves the viscoelastic behavior of CA mortar.Therefore,asphalt emulsion should be used as much as possible on the condition that essential performance criterions of CA mortar are satisfied.展开更多
Physical properties of different fibers (mineral, cellulose, or carbon fiber) and their stabilizing and reinforcing effects on asphalt mortar performance were studied. Scanning electron microscopy was used to study ...Physical properties of different fibers (mineral, cellulose, or carbon fiber) and their stabilizing and reinforcing effects on asphalt mortar performance were studied. Scanning electron microscopy was used to study the effect of fiber's microstructure on asphalt mortar's performance. Laboratory tests of mesh-basket draindown and oven heating were designed and performed to evaluate the fibers' asphalt absorption and thermostability. A cone penetration test was used to study the flow resistance of fiber-modified asphalt mortar. Results showed that fiber can form a three-dimensional network structure in asphalt, and this network can be retained at high temperature. This network of fibers favors the formation of a thick coating of mastic without asphalt draining down. Cellulose fiber possessed a greater effect on asphalt absorption and sta- bilization than did the other fibers (mineral and carbon fiber). A dynamic shear rheometer was used to evaluate their rheological properties and rut resistance. Results indicated that fiber can effectively improve the rut and flow resistance of asphalt mortar. However, the bending beam rheometer results demonstrated that the addition of fiber had negative effects on the creep stiffness and creep rate of asphalt mortar.展开更多
When the filler-bitumen ratio of asphalt mortar changes, its adhesion and viscoelasticity will also change, as well as its performance at the high and low temperatures, fatigue durability, and ductility. Thus, the app...When the filler-bitumen ratio of asphalt mortar changes, its adhesion and viscoelasticity will also change, as well as its performance at the high and low temperatures, fatigue durability, and ductility. Thus, the appropriate fillerbitumen ratio directly affects the asphalt mortar's performance. This paper tested the physical indexes of the No. 70 matrix asphalt mortar modified by additive Sasobit (SB) and Sasowam (SW) through dynamic shear rheometer and bending beam rheometer under different temperature conditions, and comprehensively analyzed the high-temperature anti-rutting and fatigue performance, low-temperature crack resistance performance, and ductility of asphalt mortar. The results show that ore powder not only can increase the antirutting factor but also can increase the aging resistance of asphalt. SB has better performances than SW at high temperatures. As for the filler-bitumen ratio of asphalt mortar with additive SB, the recommended value is between 0.8 and 1.2, and the value may be a little larger for that with SW.展开更多
Chemical admixtures are of paramount importance to the performance of modern cement based composites. In this paper, we performed a series of tests to investigate the effects of chemical admixtures on the cement aspha...Chemical admixtures are of paramount importance to the performance of modern cement based composites. In this paper, we performed a series of tests to investigate the effects of chemical admixtures on the cement asphalt mortar(CA mortar), i e, compressive strength, frost resistance, permeability, fatigue resistance, pore structure and microstructure. In particular, two types of chemical admixtures were tested, i e, defoamer(tributyl phosphate(TBP)) and polycarboxylate superplasticizer(PS). The results indicate that the addition of TBP and PS eliminates big bubbles and promotes small non-connected pores forming in matrix. Besides, an optimum dosage of TBP and PS may be determined with respect to the frost resistance, permeability and fatigue resistance of CA mortar. Further elaborative discussions are presented as well as experimental evidences from mercury intrusion porosimetry, scanning electron microscopy and energy dispersive spectroscopy.展开更多
To research the possibility of steel-making dust as a kind of mineral filler in asphalt mixture, two steel-making dusts and one ordinary mineral filler were adopted. The specific density, specific surface area, finene...To research the possibility of steel-making dust as a kind of mineral filler in asphalt mixture, two steel-making dusts and one ordinary mineral filler were adopted. The specific density, specific surface area, fineness modulus and mineralogy component of the dusts were tested. Scanning electron microscopy(SEM) was carried out to research the microstructure of the dusts; dynamic shear rheological(DSR) test and time sweep test were used to research the high temperature and fatigue performance of asphalt mortars containing steel-making dust. The experimental results indicate that, compared with ordinary mineral filler, steel-making dusts have more active ingredients, difference surface characteristics and micro-structure. Furthermore, the high temperature and fatigue performance of steel-making dusts corresponding asphalt mortars are superior to those of reference group. Therefore, the steel-making dust would be an alternative to the ordinary mineral filler to improve the performance of asphalt mortars and reduce the harm of the dusts to the environment at the same time.展开更多
To research the dynamic mechanical properties and road performances of flame retardant asphalt mortars and mixtures, four different asphalt mortars/mixtures were prepared: a reference group and three asphalt mortars/m...To research the dynamic mechanical properties and road performances of flame retardant asphalt mortars and mixtures, four different asphalt mortars/mixtures were prepared: a reference group and three asphalt mortars/mixtures containing composite flame retardant materials(M-FRs) of different proportions. Temperature sweep, frequency sweep, repeated creep test, force ductility test and bending beam rheological test were carried out to research the dynamic mechanical properties of asphalt mortars containing M-FRs; wheeltracking test, low-temperature bending test and freeze-thaw split test were used to study the road performances of asphalt mixtures containing M-FRs. The results show that high-temperature performances of the three flame retardant asphalt mortars improve greatly, while low-temperature cracking resistances decline. Both hightemperature performances and water stabilities of asphalt mixtures containing M-FRs are quite good and exceed the specification requirements. However, their low-temperature performances decline in different degrees. In summary, besides their good flame retardancy, the flame retardant asphalt mortars and mixtures also exhibit acceptable road performance.展开更多
Asphalt materials will be ignited and release significant toxic fumes within tunnel fires. Thus, combustion character- istics of asphalt materials used in road tunnel should be studied in order to limit such an advers...Asphalt materials will be ignited and release significant toxic fumes within tunnel fires. Thus, combustion character- istics of asphalt materials used in road tunnel should be studied in order to limit such an adverse effect. In the present work we study the influence of limestone fillers on combustion characteristics of asphalt mortar by thermogravimetric and kinetic analysis. It is shown that the combustion of asphalt mortar is not just a linear superposition of asphalt and limestone. The limestone will increase the ignition point and the activation energy of the primary volatile release, and will catalyze the char formation from the primary volatile release. Kinetic analysis shows that the primary volatile release stage of asphalt mortar combustion can be explained by a three-dimensional diffusion model, the secondary volatile release and char combustion stage can be explained by a model under the assumption of random nucleation and nuclei growth, whereas the limestone decomposition stage appears to follow the one-dimensional phase boundary model.展开更多
基金Funded by National Natural Science Foundation of China(No.52278446)。
文摘In order to evaluate the feasibility of steel slag powder as filler,the coating properties of steel slag and limestone aggregate were compared by water boiling test,the micro morphology difierences between steel slag powder and mineral powder(limestone powder)were compared by scanning electron microscope(SEM),and the high-temperature rheological properties of asphalt mortar with difierent ratio of filler quality to asphalt quality(F/A)and difierent substitution rates of mineral powder(S/F)were studied by dynamic shear rheological test.The results show that the surface microstructure of steel slag powder is more abundant than that of mineral powder,and the adhesion of steel slag to asphalt is better than that of limestone.At the same temperature,the lower the ratio of S/F is,the greater the rutting factor and complex modulus will be.In addition,the complex modulus and rutting factor of the asphalt mortar increase with the increase of F/A,and the filler type and F/A have a negligible efiect on the phase angle.
基金Funded by the National Natural Science Foundation of China(No.51978088)。
文摘This study aims to investigate the efiect of the mesoscopic characteristics of mineral powder fillers on the rutting resistance of asphalt mortar.Extraction and sieving tests were used to obtain the buton rock asphalt(BRA)ash with particle size smaller than 0.075 mm,which is consistent with that of the conventional mineral powder.The mesoscopic characteristics of BRA ash and conventional mineral powder were measured by SEM image analysis and the osmotic free pressure water method.Mesoscopic structure models of structural and free asphalts in mortar were obtained.The 70#matrix asphalt was used to prepare two kinds of asphalt mortar with BRA ash and conventional mineral powders fillers.The rutting factor of the two asphalt mortars was tested by dynamic shear test(DSR).Test results show that the ash extracted from BRA has a similar mesoscopic classification with the conventional mineral powder.Still,its fractal dimensions are larger,indicating the particles in BRA ash have more complex shapes and rougher surfaces,which is beneficial for forming structural asphalt and subsequently increasing the rutting factor(G*/sinδ),i e,improving the rutting resistance of the asphalt mortar.
基金This work was supported by National Natural Science Foundation of China(No.52208440)Natural Science Foundation of Jiangsu Province(BK20210618)+1 种基金the Natural Science Foundation of the Jiangsu Higher Education Institutions of China(21KJB580003)National Undergraduate Training Program for Innovation and Entrepreneurship(2021NFUSPITP0638).
文摘To understand the effects offiller-asphalt ratio on different properties of lignin and polyesterfiber reinforced shape memory polyurethane(SMPU)/styrene butadiene styrene(SBS)composite modified asphalt mortar(PSAM),as well as to reveal the reinforcing and toughening mechanisms of lignin and polyesterfibers on PSAM,SMPU,SBS and mineral powder werefirst utilized to prepare PSAM.Then the conventional,rheological and anti-cracking properties of ligninfiber reinforced PSAM(LFAM)and polyesterfiber reinforced PSAM(PFAM)at dif-ferentfiller-asphalt ratios were characterized.Test results indicate that the shear strength,deformation resistance and viscosity are increased after adding 0.8wt%ligninfiber or polyesterfiber and increasing thefiller-asphalt ratio from 0.8 to 1.2.The optimalfiller-asphalt ratio of 1.0 is proposed after comprehensive performance assessments of PSAM.Polyesterfiber shows a better reinforcing effect than ligninfiber,but its improvement in the thermal stability of PSAM is not significant at high temperatures.Additionally,the complex modulus,storage modulus,loss modulus and rutting resistance factor of PSAM are improved after adding ligninfiber and polyesterfiber,as well as show an increasing trend as thefiller-asphalt ratio is raised,but the phase angle is gradually decreased.Further,the increase of elastic components in PSAM effectively enhances the anti-deformation ability of PSAM at high temperatures,and polyesterfiber more obviously improves the high-temperature deformation resistance of PSAM than ligninfiber.Finally,the anti-cracking performance of PFAM and LFAM at low temperatures is reduced by 74.2%and 46.7%,respectively,as thefiller-asphalt ratio is raised from 0.8 to 1.2.The low-temperature anti-cracking performance of LFAM is lower than that of PFAM at the samefiller-asphalt ratio,even lower than that of PSA.Compared with ligninfiber,the anti-cracking performance and deformation resistance of PSAM at low temperature is more greatly enhanced by polyester fiber.
基金supported by the National Natural Science Foundation of China (51008307)the Fundamental Research Funds for the Central Universities (09CX04039A)the Graduate Student Innovation Project of China University of Petroleum (East China) (12CX06055A)
文摘In this paper we investigate the reinforcement mechanism of high viscosity rubber/SBS modified asphalt mortar mixed with fiber (mineral, lignin or carbon fiber) and deoiled asphalt (DOA). The softening point, penetration and viscosity tests were conducted to characterize the engineering properties of asphalt-fiber mortar. The microstructure of fiber was observed using scanning electron microscopy (SEM), and the results indicated that fiber can effectively improve the toughness of asphalt matrix through forming a spatial network structure, and then adhesion and stabilization of asphalt binder. The cone penetration test was designed to study the rheological property of fiber modified asphalt. The results indicated that the reinforcement effect increased with fibers and DOA fraction increasing to a certain threshold, and the optimal fiber content was dependent on the fiber type and its length. Fiber content and filler-asphalt ratio had significant effects on the softening point, penetration, viscosity and cone penetration of asphalt mortar.
基金Funded by National Natural Science Foundation of China (No.50802050)the Key Research and Development Program of Chinese Ministry of Railway (No.2008G031-18-6)
文摘The compressive strength developing process and the microstructure of cement-asphalt mortar (CA mortar) were investigated.The fluidity of CA mortar has a great influence on its strength.The optimum value of spread diameter of slump flow test is in the range of 300 to 400 mm.The compressive strength of CA mortar keeps a relatively high growth rate in 56 days and grows slowly afterwards.The residual water of hydration in CA mortar freezes under minus environmental temperature which can lead to a significant reduction of the strength of CA mortar.Increasing A/C retards asphalt emulsion splitting and thus prolongs the setting process of CA mortar.The hydration products of cement form the major structural framework of hardened CA mortar and asphalt is a weak phase in the framework but improves the viscoelastic behavior of CA mortar.Therefore,asphalt emulsion should be used as much as possible on the condition that essential performance criterions of CA mortar are satisfied.
基金supported by the National Natural Science Foundation of China (51008307)the Fundamental Research Funds for the Central Universities (09CX04039A)the Graduate Student Innovation Project of China University of Petroleum (East China) (12CX06055A)
文摘Physical properties of different fibers (mineral, cellulose, or carbon fiber) and their stabilizing and reinforcing effects on asphalt mortar performance were studied. Scanning electron microscopy was used to study the effect of fiber's microstructure on asphalt mortar's performance. Laboratory tests of mesh-basket draindown and oven heating were designed and performed to evaluate the fibers' asphalt absorption and thermostability. A cone penetration test was used to study the flow resistance of fiber-modified asphalt mortar. Results showed that fiber can form a three-dimensional network structure in asphalt, and this network can be retained at high temperature. This network of fibers favors the formation of a thick coating of mastic without asphalt draining down. Cellulose fiber possessed a greater effect on asphalt absorption and sta- bilization than did the other fibers (mineral and carbon fiber). A dynamic shear rheometer was used to evaluate their rheological properties and rut resistance. Results indicated that fiber can effectively improve the rut and flow resistance of asphalt mortar. However, the bending beam rheometer results demonstrated that the addition of fiber had negative effects on the creep stiffness and creep rate of asphalt mortar.
文摘When the filler-bitumen ratio of asphalt mortar changes, its adhesion and viscoelasticity will also change, as well as its performance at the high and low temperatures, fatigue durability, and ductility. Thus, the appropriate fillerbitumen ratio directly affects the asphalt mortar's performance. This paper tested the physical indexes of the No. 70 matrix asphalt mortar modified by additive Sasobit (SB) and Sasowam (SW) through dynamic shear rheometer and bending beam rheometer under different temperature conditions, and comprehensively analyzed the high-temperature anti-rutting and fatigue performance, low-temperature crack resistance performance, and ductility of asphalt mortar. The results show that ore powder not only can increase the antirutting factor but also can increase the aging resistance of asphalt. SB has better performances than SW at high temperatures. As for the filler-bitumen ratio of asphalt mortar with additive SB, the recommended value is between 0.8 and 1.2, and the value may be a little larger for that with SW.
基金Funded by the National Natural Science Foundation of China(Nos.U1134206,51178230)the Technological Development Projects of China Railway Engineering Corporation(No.Z2013-038-3)
文摘Chemical admixtures are of paramount importance to the performance of modern cement based composites. In this paper, we performed a series of tests to investigate the effects of chemical admixtures on the cement asphalt mortar(CA mortar), i e, compressive strength, frost resistance, permeability, fatigue resistance, pore structure and microstructure. In particular, two types of chemical admixtures were tested, i e, defoamer(tributyl phosphate(TBP)) and polycarboxylate superplasticizer(PS). The results indicate that the addition of TBP and PS eliminates big bubbles and promotes small non-connected pores forming in matrix. Besides, an optimum dosage of TBP and PS may be determined with respect to the frost resistance, permeability and fatigue resistance of CA mortar. Further elaborative discussions are presented as well as experimental evidences from mercury intrusion porosimetry, scanning electron microscopy and energy dispersive spectroscopy.
基金Funded by the National Natural Science Foundation of China(51778482)
文摘To research the possibility of steel-making dust as a kind of mineral filler in asphalt mixture, two steel-making dusts and one ordinary mineral filler were adopted. The specific density, specific surface area, fineness modulus and mineralogy component of the dusts were tested. Scanning electron microscopy(SEM) was carried out to research the microstructure of the dusts; dynamic shear rheological(DSR) test and time sweep test were used to research the high temperature and fatigue performance of asphalt mortars containing steel-making dust. The experimental results indicate that, compared with ordinary mineral filler, steel-making dusts have more active ingredients, difference surface characteristics and micro-structure. Furthermore, the high temperature and fatigue performance of steel-making dusts corresponding asphalt mortars are superior to those of reference group. Therefore, the steel-making dust would be an alternative to the ordinary mineral filler to improve the performance of asphalt mortars and reduce the harm of the dusts to the environment at the same time.
基金Funded by the National Key Technology R&D Program for the 12th Five-Year Plan(No.2011BAE27B04)
文摘To research the dynamic mechanical properties and road performances of flame retardant asphalt mortars and mixtures, four different asphalt mortars/mixtures were prepared: a reference group and three asphalt mortars/mixtures containing composite flame retardant materials(M-FRs) of different proportions. Temperature sweep, frequency sweep, repeated creep test, force ductility test and bending beam rheological test were carried out to research the dynamic mechanical properties of asphalt mortars containing M-FRs; wheeltracking test, low-temperature bending test and freeze-thaw split test were used to study the road performances of asphalt mixtures containing M-FRs. The results show that high-temperature performances of the three flame retardant asphalt mortars improve greatly, while low-temperature cracking resistances decline. Both hightemperature performances and water stabilities of asphalt mixtures containing M-FRs are quite good and exceed the specification requirements. However, their low-temperature performances decline in different degrees. In summary, besides their good flame retardancy, the flame retardant asphalt mortars and mixtures also exhibit acceptable road performance.
基金supported by the Natural Science Foundation of Zhejiang Province,China(Grant No.LY14E080014)the National Natural Science Foundation ofChina(Grant Nos.61154002 and 51078331)
文摘Asphalt materials will be ignited and release significant toxic fumes within tunnel fires. Thus, combustion character- istics of asphalt materials used in road tunnel should be studied in order to limit such an adverse effect. In the present work we study the influence of limestone fillers on combustion characteristics of asphalt mortar by thermogravimetric and kinetic analysis. It is shown that the combustion of asphalt mortar is not just a linear superposition of asphalt and limestone. The limestone will increase the ignition point and the activation energy of the primary volatile release, and will catalyze the char formation from the primary volatile release. Kinetic analysis shows that the primary volatile release stage of asphalt mortar combustion can be explained by a three-dimensional diffusion model, the secondary volatile release and char combustion stage can be explained by a model under the assumption of random nucleation and nuclei growth, whereas the limestone decomposition stage appears to follow the one-dimensional phase boundary model.