期刊文献+
共找到4,437篇文章
< 1 2 222 >
每页显示 20 50 100
A New Algorithm of Rain Type Classification for GPM Dual-Frequency Precipitation Radar in Summer Tibetan Plateau
1
作者 Yunfei FU Liu YANG +4 位作者 Zhenhao WU Peng ZHANG Songyan GU Lin CHEN Sun NAN 《Advances in Atmospheric Sciences》 SCIE CAS CSCD 2024年第11期2093-2111,共19页
In this study, a new rain type classification algorithm for the Dual-Frequency Precipitation Radar(DPR) suitable over the Tibetan Plateau(TP) was proposed by analyzing Global Precipitation Measurement(GPM) DPR Level-2... In this study, a new rain type classification algorithm for the Dual-Frequency Precipitation Radar(DPR) suitable over the Tibetan Plateau(TP) was proposed by analyzing Global Precipitation Measurement(GPM) DPR Level-2 data in summer from 2014 to 2020. It was found that the DPR rain type classification algorithm(simply called DPR algorithm) has mis-identification problems in two aspects in summer TP. In the new algorithm of rain type classification in summer TP,four rain types are classified by using new thresholds, such as the maximum reflectivity factor, the difference between the maximum reflectivity factor and the background maximum reflectivity factor, and the echo top height. In the threshold of the maximum reflectivity factors, 30 d BZ and 18 d BZ are both thresholds to separate strong convective precipitation, weak convective precipitation and weak precipitation. The results illustrate obvious differences of radar reflectivity factor and vertical velocity among the three rain types in summer TP, such as the reflectivity factor of most strong convective precipitation distributes from 15 d BZ to near 35 d BZ from 4 km to 13 km, and increases almost linearly with the decrease in height. For most weak convective precipitation, the reflectivity factor distributes from 15 d BZ to 28 d BZ with the height from 4 km to 9 km. For weak precipitation, the reflectivity factor mainly distributes in range of 15–25 d BZ with height within 4–10 km. It is also shows that weak precipitation is the dominant rain type in summer TP, accounting for 40%–80%,followed by weak convective precipitation(25%–40%), and strong convective precipitation has the least proportion(less than 30%). 展开更多
关键词 satellite precipitation radar rain type classification method Tibetan Plateau strong convective precipitation
下载PDF
A deep learning–based U-Net model for ENSO-related precipitation responses to sea surface temperature anomalies over the tropical Pacific 被引量:1
2
作者 Yuchao Zhu Rong-Hua Zhang 《Atmospheric and Oceanic Science Letters》 CSCD 2023年第4期57-64,共8页
SST–降水反馈过程在热带太平洋ENSO演变过程中起着重要作用,能否真实地在数值模式中表征SST–降水年际异常之间的关系及相关反馈过程,对于准确模拟和预测ENSO至关重要.例如,在一些模拟ENSO的混合型耦合模式中,通常采用大气统计模型(如... SST–降水反馈过程在热带太平洋ENSO演变过程中起着重要作用,能否真实地在数值模式中表征SST–降水年际异常之间的关系及相关反馈过程,对于准确模拟和预测ENSO至关重要.例如,在一些模拟ENSO的混合型耦合模式中,通常采用大气统计模型(如经验正交函数;EOF)来表征降水(海气界面淡水通量的一个重要分量)对SST年际异常的线性响应.然而在当前的耦合模式中,真实观测到的降水–SST统计关系还不能被很好地再现出来,从而引起ENSO模拟误差和不确定性.在本研究中,使用基于深度学习的U-Net模型来构建热带太平洋降水异常场对SST年际异常的非线性响应模型.研究发现:U-Net模型的性能优于传统的基于EOF方法的模型.特别是在热带西太平洋海区,U-Net模型估算的降水误差远小于EOF模型的模拟.此外,当SST和降水异常的趋势信息作为输入变量也被同时引入以进一步约束模式训练时,U-Net模型的性能可以进一步提高,如能使热带辐合带区域的误差显著降低. 展开更多
关键词 U-Net模型 EOF方法 SST-降水年际异常关系 CMIP6模拟
下载PDF
Analysis of Cold Air and Precipitation in Central and Eastern China, 2-5 October, 2022
3
作者 Ming Shi 《Journal of Geoscience and Environment Protection》 2023年第7期205-212,共8页
This paper used potential height field data published by the China National Climate Center and the US NCEP reanalysis data. A study was conducted on a strong cold wave weather process in central and eastern China from... This paper used potential height field data published by the China National Climate Center and the US NCEP reanalysis data. A study was conducted on a strong cold wave weather process in central and eastern China from October 2 to 5, 2022. The results show that this weather process is a cold air weather process of “horizontal trough to vertical” type from the east of Novaya Zemlya Island. Cold air passes through Russia and Mongolia south, controlling northern China. The precipitation process is caused by the combination of high-altitude trough, ground front, warm and humid air flow, and precipitation weather formed by the influence of warm and humid air due to the 700 hPa shear line. The northern Sichuan Basin and the middle and lower reaches of the Yellow River in China can precipitate almost 50 mm. Water vapor is transported from the South China Sea to central and eastern China by the southwest warm and humid air flow along the west side of the West Pacific Subtropical High. Water vapor is concentrated over the precipitation area through horizontal convergence and is the most important source of water vapor causing precipitation. 展开更多
关键词 METEOROLOGICAL method precipitation Cold Wave Cold Air
下载PDF
Improved continuous precipitation kinetics and tensile properties of extruded AZ80 alloy through {10-12} twin formation
4
作者 Hyun Ji Kim Sumi Jo Sung Hyuk Park 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2023年第9期3323-3337,共15页
This study investigates the effect of{10-12}deformation twins on the continuous precipitation behavior of an extruded Mg-8.0Al-0.5Zn-0.2Mn(AZ80)alloy during aging.The extruded AZ80 alloy is compressed along the transv... This study investigates the effect of{10-12}deformation twins on the continuous precipitation behavior of an extruded Mg-8.0Al-0.5Zn-0.2Mn(AZ80)alloy during aging.The extruded AZ80 alloy is compressed along the transverse direction to introduce{10-12}twins,followed by an aging treatment at 300℃.The extruded material exhibits a twin-free microstructure with low internal strain energy,whereas the pre-twinned material possesses abundant{10-12}twins and has high internal strain energy.The aging results reveal that the peak-aging time of the pre-twinned material(1 h)is one-eighth of that of the extruded material(8 h).Although Mg_(17)Al_(12)continuous precipitates(CPs)are observed in both the peak-aged materials,these CPs are much smaller and more densely distributed in the pre-twinned material despite the significantly shorter aging time.The CPs size in the peak-aged materials increases in the following order:twinned region in the pre-twinned material(0.47μm)<residual matrix region in the pre-twinned material(1.71μm)<matrix region in the extruded material(2.55μm).Moreover,the CPs number density in the twinned region of the pre-twinned material is approximately 11 times higher than that in the matrix region of the extruded material.The peak-aged pre-twinned material exhibits significantly higher tensile strength and ductility than the peak-aged extruded material.These results demonstrate that the formation of{10-12}twins in the extruded AZ80 alloy substantially accelerates the static precipitation of CPs during aging at 300℃and improves the tensile properties of the peak-aged material. 展开更多
关键词 AZ80 alloy {10-12}twin AGING Continuous precipitation Tensile properties
下载PDF
Synthesis and Characterization of Y-Doped Mesoporous CeO_2 Using A Chemical Precipitation Method 被引量:5
5
作者 宋晓岚 江楠 +2 位作者 李宇焜 徐大余 邱冠周 《Journal of Rare Earths》 SCIE EI CAS CSCD 2007年第4期428-433,共6页
Using cetyltrimethylammonium bromide (CTAB) as the template agent, cerium nitrate as the cerium resource, yttrium nitrate as the yttrium resource, and ammonium carbonate as the precipitating agent, mesoporous CeO2 p... Using cetyltrimethylammonium bromide (CTAB) as the template agent, cerium nitrate as the cerium resource, yttrium nitrate as the yttrium resource, and ammonium carbonate as the precipitating agent, mesoporous CeO2 powders doped with different yttrium contents were successfully synthesized using a chemical precipitation method, under an alkalescent condition. Properties of the obtained samples were characterized and analyzed with X-ray diffraction (XRD), energy dispersive analysis of X-rays (EDAX), transmission electron microscopy (TEM), infrared (IR) absorbance, and the BET method. For the prepared samples with 20% (molar ratio) Y-doped content, a BET specific surface area of 106. 6 m^2 · g^- 1, with an average pore size of3~27 nm were obtained. XRD patterns showed that the doped samples were with a cubic fluorite structure. TEM micrographs revealed that the doped samples showed a spherical morphology with a diameter ranging from 20 to 30 nm and a round pore shape. IR results indicated that the Ce-O-Ce vibration intensity decreased as the Y-doped content increased. N2 adsorption-desorption isotherms showed that the samples possessed typical mesopore characteristics. The average pore size of the samples decreased alter mesoporous CeO2 was doped with yttrium, and the average pore size decreased largely as the Y-doped content increased. 展开更多
关键词 mesoporous ceria Y-doped chemical precipitation method SYNTHESIS characterization rare earths
下载PDF
Influence of different solution methods on microstructure, precipitation behavior and mechanical properties of Al-Mg-Si alloy 被引量:8
6
作者 Guan-jun GAO Chen HE +3 位作者 Yong LI Jia-dong LI Zhao-dong WANG R. D. K. MISRA 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2018年第5期839-847,共9页
The effects of different solution methods on microstructure, mechanical properties and precipitation behavior of Al-Mg-Si alloy were investigated by scanning electron microscope, transmission electron microscope, tens... The effects of different solution methods on microstructure, mechanical properties and precipitation behavior of Al-Mg-Si alloy were investigated by scanning electron microscope, transmission electron microscope, tensile test, and differential scanning calorimetry. The results revealed that the recrystallized grains of the alloy after the solution treatment with hot air became smaller and more uniform, compared with solution treatment with electrical resistance. The texture of the alloy after two solution treatment methods was different. More rotated cube components were formed through solution treatment with electrical resistance, which was better for improving the drawability of the alloy. The strength of the alloy under the solution treatment with hot air was higher before stamping, because of the small uniform grains and many clusters in the matrix. The alloy solution treated with hot air also possessed good bake hardenability, because the transformation occurred on more clusters in the matrix. 展开更多
关键词 Al-Mg-Si alloy solution method recrystallization grain TEXTURE mechanical property precipitation activation energy
下载PDF
Precipitation Retrieval from Himawari-8 Satellite Infrared Data Based on Dictionary Learning Method and Regular Term Constraint 被引量:2
7
作者 Wang Gen Ding Conghui Liu Huilan 《Meteorological and Environmental Research》 CAS 2019年第3期61-65,68,共6页
In this paper,the application of an algorithm for precipitation retrieval based on Himawari-8 (H8) satellite infrared data is studied.Based on GPM precipitation data and H8 Infrared spectrum channel brightness tempera... In this paper,the application of an algorithm for precipitation retrieval based on Himawari-8 (H8) satellite infrared data is studied.Based on GPM precipitation data and H8 Infrared spectrum channel brightness temperature data,corresponding "precipitation field dictionary" and "channel brightness temperature dictionary" are formed.The retrieval of precipitation field based on brightness temperature data is studied through the classification rule of k-nearest neighbor domain (KNN) and regularization constraint.Firstly,the corresponding "dictionary" is constructed according to the training sample database of the matched GPM precipitation data and H8 brightness temperature data.Secondly,according to the fact that precipitation characteristics in small organizations in different storm environments are often repeated,KNN is used to identify the spectral brightness temperature signal of "precipitation" and "non-precipitation" based on "the dictionary".Finally,the precipitation field retrieval is carried out in the precipitation signal "subspace" based on the regular term constraint method.In the process of retrieval,the contribution rate of brightness temperature retrieval of different channels was determined by Bayesian model averaging (BMA) model.The preliminary experimental results based on the "quantitative" evaluation indexes show that the precipitation of H8 retrieval has a good correlation with the GPM truth value,with a small error and similar structure. 展开更多
关键词 Himawari-8(H8) RETRIEVAL of precipitation k-nearest NEIGHBOR (KNN) REGULAR TERM constraints DICTIONARY method Bayesian model average (BMA)
下载PDF
Improvement of 6–15 Day Precipitation Forecasts Using a Time-Lagged Ensemble Method 被引量:4
8
作者 JIE Weihua WU Tongwen +2 位作者 WANG Jun LI Weijing LIU Xiangwen 《Advances in Atmospheric Sciences》 SCIE CAS CSCD 2014年第2期293-304,共12页
A time-lagged ensemble method is used to improve 6-15 day precipitation forecasts from the Beijing Climate Center Atmospheric General Circulation Model,version 2.0.1.The approach averages the deterministic predictions... A time-lagged ensemble method is used to improve 6-15 day precipitation forecasts from the Beijing Climate Center Atmospheric General Circulation Model,version 2.0.1.The approach averages the deterministic predictions of precipitation from the most recent model run and from earlier runs,all at the same forecast valid time.This lagged average forecast (LAF) method assigns equal weight to each ensemble member and produces a forecast by taking the ensemble mean.Our analyses of the Equitable Threat Score,the Hanssen and Kuipers Score,and the frequency bias indicate that the LAF using five members at time-lagged intervals of 6 h improves 6-15 day forecasts of precipitation frequency above 1 mm d-1 and 5 mm d-1 in many regions of China,and is more effective than the LAF method with selection of the time-lagged interval of 12 or 24 h between ensemble members.In particular,significant improvements are seen over regions where the frequencies of rainfall days are higher than about 40%-50% in the summer season; these regions include northeastern and central to southern China,and the southeastem Tibetan Plateau. 展开更多
关键词 time-lagged ensemble system lagged average forecast 6-15 day forecasts precipitation
下载PDF
Enhanced Photocatalytic Properties of Pure and Cr-Modified ZnS Powders Synthesized by Precipitation Method 被引量:1
9
作者 Bedour A. Mahammed Luma M. Ahmed 《Journal of Geoscience and Environment Protection》 2017年第10期101-111,共11页
Zinc sulfide photocatalysts doped with chromium (1:1)% were synthesized via precipitation technique. Their characteristics were studied by X-ray diffraction (XRD), AFM and Florescence spectrometer. The photocatalytic ... Zinc sulfide photocatalysts doped with chromium (1:1)% were synthesized via precipitation technique. Their characteristics were studied by X-ray diffraction (XRD), AFM and Florescence spectrometer. The photocatalytic reaction was applied under light intensity equal to 1.45 × 10-7 Einstein mol-1 to investigate the kinetics and thermodynamic parameters for photo-decolorization of reactive black 5 dye in collide solution of bare and Cr-doped ZnS. The mean crystal size and particle size for bare ZnS are more than those values for prepared Cr loaded ZnS. 展开更多
关键词 Cr-Loaded ZNS NANOPOWDERS Reactive Black 5 DYE AZO DYE precipitation method
下载PDF
Fluorescence and preparation of Sr_2(P_2O_7 ):Ce,Tb phosphate by co-precipitation method 被引量:8
10
作者 Cheng-Guo Ma Wei Zheng +1 位作者 Li-Guo Jin Li-Min Dong 《Rare Metals》 SCIE EI CAS CSCD 2013年第4期420-424,共5页
The micron-sized Sr2(P2OT):Ce,Tb green phosphors were prepared by being annealed at different temperatures with its precursors synthesized by co-pre-cipitates of (NH4)2HPO4 at ambient temperature. The phase struc... The micron-sized Sr2(P2OT):Ce,Tb green phosphors were prepared by being annealed at different temperatures with its precursors synthesized by co-pre-cipitates of (NH4)2HPO4 at ambient temperature. The phase structure, grain size, surface morphology, and luminescent properties of phosphors were investigated by X-ray diffraction, scanning electron microscope, trans-mission electron microscope, and fluorescence spectrum. The results show that the product of precursor annealed at 1,100 ℃ is Sr2(P2O7):Ce,Tb, which belongs to ortho-rhombic phase. The powder is spherical and the size dis-tribution is in micron grade. The sample with the molar ratio of Sr/Tb/Ce of 100.0:0.4:0.6 shows the best fluores-cence effect annealed at 1,100 ℃ for 3 h. The phosphors produce green fluorescence by being excitated with ultra-violet radiation of 254 nm wavelength, and the main emission peak is at 547 nm. The Sr2(P2O7):Ce,Tb phos-phors synthesized by co-precipitation method of precursors at ambient temperature is a kind of efficient green-emitting phosphors. 展开更多
关键词 PHOSPHORS Co-precipitation method Rareearth phosphate PHOSPHORESCENCE
下载PDF
Synthesis of γ-Al_2O_3 nanoparticles by chemical precipitation method 被引量:1
11
作者 宋晓岚 曲鹏 +2 位作者 杨海平 何希 邱冠周 《Journal of Central South University of Technology》 EI 2005年第5期536-541,共6页
Highly pure active γ-Al2O3 nanoparticles were synthesized from aluminum nitrate and ammonium carbonate with a little surfactant by chemical precipitation method. The factors affecting the synthesis process were studi... Highly pure active γ-Al2O3 nanoparticles were synthesized from aluminum nitrate and ammonium carbonate with a little surfactant by chemical precipitation method. The factors affecting the synthesis process were studied. The properties of γ-Al2O3 nanoparticles were characterized by DTA, XRD, BET, TEM, laser granularity analysis and impurity content analysis. The results show that the amorphous precursor AI(OH)3 sols are produced by using 0.1 mol/L Al(NO3)3·9H2O and 0.16 mol/L (NH4)2CO3·H2O reaction solutions, according to the volume ratio 1.33, adding 0.024%(volume fraction) surfactant PEG600, and reacting at 40℃, 1000 r/min stirring rate for 15min. Then, after stabilizing for 24 h, the precursors were extracted and filtrated by vacuum, washed thoroughly with deionized water and dehydrated ethanol, dried in vacuum at 80℃ for 8h, final calcined at 800℃ for 1h in the air, and high purity active γ-Al2O3 nanoparticles can be prepared with cubic in crystal system, OH^7-FD3M in space group, about 9 nm in crystal grain size, about 20 nm in particle size and uniform size distribution, 131.35 m^2/g in BET specific surface area, 7 - 11 nm in pore diameter, and not lower than 99.93% in purity. 展开更多
关键词 chemical precipitation method γ-Al2O3 nanoparticles characterization of properties
下载PDF
Effects of synthesis conditions on the structural and electrochemical properties of layered LiNi_(1/3)Co_(1/3)Mn_(1/3)O_2 cathode material via oxalate co-precipitation method 被引量:6
12
作者 TIAN Hua YE Naiqing +1 位作者 LIU Dan LI Wenqun 《Rare Metals》 SCIE EI CAS CSCD 2008年第6期575-579,共5页
The uniform layered LiNi1/3Co1/3Mn1/3O2 cathode material for lithium ion batteries was prepared by using (Ni1/3Co1/3Mn1/3)C2O4 as precursor synthesized via oxalate co-precipitation method in air. The effects of calc... The uniform layered LiNi1/3Co1/3Mn1/3O2 cathode material for lithium ion batteries was prepared by using (Ni1/3Co1/3Mn1/3)C2O4 as precursor synthesized via oxalate co-precipitation method in air. The effects of calcination temperature and time on the structure and electrochemical properties of the LiNi1/3Co1/3Mn1/3O2 were systemically studied. XRD results revealed that the optimal calcination conditions to prepare the layered LiNi1/3Co1/3Mn1/302 were 950℃ for 15 h. Electrochemical measurement showed that the sample prepared under the such conditions has the highest initial discharge capacity of 160.8 mAh/g and the smallest irreversible capacity loss of 13.5% as well as stable cycling performance at a constant current density of 30 mA/g between 2.5 and 4.3 V versus Li at room temperature. 展开更多
关键词 lithium ion batteries oxalate co-precipitation method cathode materials electrochemical performance
下载PDF
Preparation and Characterization of Y_3Sc_2Ga_3O_(12) Nano-Polycrystalline Powders by Co-Precipitation Method 被引量:1
13
作者 苏静 张庆礼 +3 位作者 邵淑芳 谷长江 万松明 殷绍唐 《Journal of Rare Earths》 SCIE EI CAS CSCD 2007年第3期302-305,共4页
In order to grow high-quality gallium garnet crystals,polycrystalline materials were used as starting materials.YSGG precursor was synthesized by co-precipitation method using aqueous ammonia as a precipitator,and the... In order to grow high-quality gallium garnet crystals,polycrystalline materials were used as starting materials.YSGG precursor was synthesized by co-precipitation method using aqueous ammonia as a precipitator,and the precursor was then sintered at different temperatures.The results showed that the feasible pH range was 8.3~9.84 in the process of co-precipitation reaction.The YSGG precursor and the powders sintered at different temperatures were characterized by IR,XRD and TEM methods.It was found that the precursor transformed to pure YSGG polycrystalline phase at 800 ℃.YSGG nano-polycrystalline powders sintered at 800~1000 ℃ were well dispersed and the sizes of the YSGG grains were about 40~100 nm. 展开更多
关键词 co-precipitation method YSGG nano-polycrystalline powder rare earths
下载PDF
Preparation and Magnetic Properties of Mn-Zn Ferrites by the Co-precipitation Method 被引量:1
14
作者 李雪 张俊喜 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2009年第6期875-878,共4页
Mn-Zn ferrites (Mn1-xZnxFe2O4) with different compositions were prepared by the coprecipitation method, and the influences of such synthesis conditions as pH value, composition and volume ratio (R) of the mixed so... Mn-Zn ferrites (Mn1-xZnxFe2O4) with different compositions were prepared by the coprecipitation method, and the influences of such synthesis conditions as pH value, composition and volume ratio (R) of the mixed solution and NH4HCO3 solution on their microstructures and magnetic properties were discussed. The samples were characterized by X-ray diffraction (XRD) and magnetization measurement instrument. Lattice parameters and average crystalline size of the synthesized materials were calculated from the corresponding XRD patterns with the related software Jade.5. For samples of different pH values, only one phase was found when pH values were 7.0, 8.0 and 9.0. The sample with pH value of 7.0 exhibited the highest saturation magnetic induction, the lowest coercive force, and crystallized best. For samples of different R values with pH value of 7.0, only one phase was observed in all samples, and the sample with R value of 2.3 exhibited the highest saturation magnetic induction and the lowest coercive force. The composition has mainly afected the magnetic properties, and the saturation magnetic induction increases with the increase of the content of Zn (x), but decreases when x is beyond 0.6. The trend of coercive force is on the contrary. However, no magnetism is exhibited when the x value is up to 0.8. 展开更多
关键词 co-precipitation method MICROSTRUCTURE magnetic property Mn-Zn ferrite
下载PDF
Synthesis of LaPO_4:Ce,Terbium by Co-Precipitation Method 被引量:1
15
作者 龙志奇 任乐 +4 位作者 朱兆武 崔大力 赵娜 李明来 黄小卫 《Journal of Rare Earths》 SCIE EI CAS CSCD 2006年第z2期137-140,共4页
The synthesis of precursor of green phosphors, LaPO4: Ce, Tb, by means of co-precipitation with cocurrent flow feed was studied. The effects of the reaction temperature, the kind and concentration of the acid in the b... The synthesis of precursor of green phosphors, LaPO4: Ce, Tb, by means of co-precipitation with cocurrent flow feed was studied. The effects of the reaction temperature, the kind and concentration of the acid in the bottom water, and the charging rate on the physical properties, such as particle size, were investigated. It is found that the particle size of the powder is controllable by adjusting acidity in bottom water and charging rate. The powder with diameter size of 3 to 5μm was obtained. Its XRD and SEM were analyzed. XRD patterns of the as-prepared green phosphor powders display the typical peaks of CePO4. SEM shows that the morphology of powders is ball-shaped. 展开更多
关键词 LaPO4:Ce Tb PRECURSOR green phosphors co-precipitation method rare earths
下载PDF
Yttrium-Doped SnO_2 Prepared by Co-Precipitation Method for Lithium-Ion Battery Anodes 被引量:1
16
作者 李超 毕磊 +4 位作者 方少明 徐甲强 吴诗德 谢冰 陈荣峰 《Journal of Rare Earths》 SCIE EI CAS CSCD 2007年第S1期508-511,共4页
SnO2 doped with Y were prepared by co-precipitation method and tested in lithium-ion cells. The structure and morphology of the materials were characterized by X-ray diffraction (XRD) and transmission electron microsc... SnO2 doped with Y were prepared by co-precipitation method and tested in lithium-ion cells. The structure and morphology of the materials were characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). XRD patterns presented that the all the as-prepared materials had tetragonal rutile structure but a second phase (Y2O3) was observed when Y content reached 4%. TEM micrograph indicated that Y doped SnO2 had a small particle size ranging from 20 to 25 nm. The electrochemical properties for an anode active material in lithium-ion batteries were investigated at room temperature, including the observed capacity involved in the first-discharge and the reversible capacity values during subsequent charge-discharge cycles. The as-prepared Y-doped SnO2 exhibited promising electrochemical properties as anodes for lithium-ion batteries. 展开更多
关键词 Y-doped SnO_2 co-precipitation method anode material lithium-ion battery rare earths
下载PDF
Synthesis of M1-3xAl2O4:Eu2+x/Dy3+ 2x(M^2+= Sr^2+, Ca^2+ and Ba^2+) phosphors with long-lasting phosphorescence properties via co-precipitation method 被引量:1
17
作者 Jinkai Li Bin Liu +2 位作者 Qi Chen Yizhong Lu Zongming Liu 《Chemical Reports》 2019年第2期112-117,共6页
The long afterglow fluorescent material of M1-3xAl2O4:Eu2+ x/Dy3+2x(M2+= Sr2+, Ca2+ and Ba2+) phosphors are successfully synthesized by calcining precursor obtained via co-precipitation method at 1300oC for 4 h with r... The long afterglow fluorescent material of M1-3xAl2O4:Eu2+ x/Dy3+2x(M2+= Sr2+, Ca2+ and Ba2+) phosphors are successfully synthesized by calcining precursor obtained via co-precipitation method at 1300oC for 4 h with reducing atmosphere (20% H2 and 80% N2). The phase evolution, morphology and afterglow fluorescent properties are systematically studied by the various instruments of XRD, FE-SEM, PLE/PL spectroscopy and fluorescence decay analysis. The PL spectra shows that the Sr1-3xAl2O4:Eu2+x/Dy3+ 2x phosphors display vivid green emission at s519 nm (4f65d1!4f7 transition of Eu2+) with monitoring of the maximum excitation wavelength at s334 nm (8S7=2!6IJ transition of Eu2+), among which the optimal concentration of Eu2+ and Dy3+ is 15 at.% and 30 at.%, respectively. The color coordinates and temperature of Sr1-3xAl2O4:Eu2+ x/Dy3+ 2x phosphors are approximately at (s0.27, s0.57) and s6700 K, respectively. On the above basis, the M0:55Al2O4:Eu2+ 0:15/Dy3+ 0:3 (M2+= Ca2+ and Ba2+) phosphors is obtained by the same method. The PL spectra of these phosphors shows the strongest blue emission at s440 nm and cyan emission at s499 nm under s334 nm wavelength excitation, respectively, which are blue shifted comparing to Sr1??3xAl2O4:Eu2+ x/Dy3+ 2x phosphors. The color coordinates and temperatures of M0:55Al2O4:Eu2+ 0:15/Dy3+ 0:3 (M2+= Ca2+ and Ba2+) phosphors are approximately at (s0.18, s0.09), s2000 K and (s0.18, s0.42), s11600 K, respectively. In this work, long afterglow materials of green, blue and cyan aluminates phosphors with excellent properties have been prepared, in order to obtain wide application in the field of night automatic lighting and display. 展开更多
关键词 long AFTERGLOW material CO-precipitation method M1-3xAl2O4:Eu2+ x/Dy3+ 2x(M2+= Sr2+ Ca2+ and Ba2+) PHOSPHORS luminescent property
下载PDF
Phase-field study on competition precipitation process of Ni-Al-V alloy 被引量:5
18
作者 卢艳丽 卢广明 +1 位作者 贾德伟 陈铮 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2015年第2期544-551,共8页
With microscopic phase-field kinetic model, atomic-scale computer simulation program for the precipitation sequence and microstructure evolution of the ordered intermetallic compound γ' and θ in ternary Ni75AlxV25-... With microscopic phase-field kinetic model, atomic-scale computer simulation program for the precipitation sequence and microstructure evolution of the ordered intermetallic compound γ' and θ in ternary Ni75AlxV25-x alloy were studied. The simulation results show that Al concentration has important effects on the precipitation sequence. When Al concentration in Ni75AlxV25-x alloy is low, 0(Ni3V) ordered phase will be firstly precipitated, followed by γ'(Ni3Al) ordered phase. With Al concentration increasing, θ and γ' ordered phases are simultaneously precipitated. With A1 concentration further increasing, γ' ordered phase is firstly precipitated, followed by θ ordered phase. There is a competition relationship between θ and γ' ordered phases during growth and coarsening process. No matter which first precipitates, θ ordered phase always occupies advantage in the competition process of coarsening, thus, the microstructure with preferred orientation is formed. 展开更多
关键词 Ni-Al-V alloy microstructure evolution precipitation process phase-field method
下载PDF
Green Emitting Phosphor M_3(PO_4)_2∶Ce, Tb (M=Mg, Ca, Sr, Ba) Prepared by Co-Precipitation Method
19
作者 董丽敏 张耀明 +2 位作者 韩志东 吴泽 张显友 《Journal of Rare Earths》 SCIE EI CAS CSCD 2007年第S1期290-293,共4页
The M3-3x(PO4)2∶2xCe, xTb(M=Mg, Ca, Sr, Ba) phosphors were prepared by coprecipitation in this paper. Their phase structures, morphologies and luminescent properties were investigated by X-ray diffractometer, field e... The M3-3x(PO4)2∶2xCe, xTb(M=Mg, Ca, Sr, Ba) phosphors were prepared by coprecipitation in this paper. Their phase structures, morphologies and luminescent properties were investigated by X-ray diffractometer, field emission scanning electron microscopy and fluorospectrophotometer. The results indicate that the Ce3+ and Tb3+ enteres the host lattice because the XRD patterns of alkaline earth phosphate show no impurity phase, the SEM shows the spherical particles with an average size about 1 μm. The emission and excitation spectra are similar to rare earth phosphate. Concentration quenching of the Sr3(PO4)2∶Ce, Tb emission intensity was not observed even when the Tb3+ increases to 0.05, while the maximum emission intensity appears when x=0.04 in M3-3x(PO4)2∶2xCe, xTb(M=Ca, Ba) emission spectrum. 展开更多
关键词 alkali earth phosphate green phosphor co-precipitation method LUMINESCENT rare earths
下载PDF
Structural and Optical Properties of Mg<SUB>1-x</SUB>Zn<SUB>x</SUB>Fe<SUB>2</SUB>O<SUB>4</SUB>Nano-Ferrites Synthesized Using Co-Precipitation Method
20
作者 Abdalrawf I. Ahmed Mohamed A. Siddig +2 位作者 Abdulmajid A. Mirghni Mohamed I. Omer Abdelrahman A. Elbadawi 《Advances in Nanoparticles》 2015年第2期45-52,共8页
In this work, the Mg1-x Znx Fe2 O4 Nanoferrites (where x = 0.0, 0.2, 0.4, 0.6 and 0.8) was synthesized using co-precipitation method. The investigation of structural and optical properties was carried out for the synt... In this work, the Mg1-x Znx Fe2 O4 Nanoferrites (where x = 0.0, 0.2, 0.4, 0.6 and 0.8) was synthesized using co-precipitation method. The investigation of structural and optical properties was carried out for the synthesized samples using X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR) and Ultraviolet visible spectrophotometer (UV-Vis). XRD revealed that the structure of these nanoparticles is spinel with space group Fd3m and crystallite size lies in the range 21.0 - 42.8 nm. Lattice parameter was found to increases with Zn concentration and this may be due to the larger ionic radius of the Zn2+?ion. FTIR spectroscopy confirmed the formation of spinel ferrite and showed the characteristics absorption bands around 612, 1146, 1404, 1649 and 3245 cm-1. The energy band gap was calculated for samples with different ratio and was found to be 4.77, 4.82, 4.86, 4.87 and 4.95 eV. The substitution was resulted in slight increased in the lattice constant and that sequentially may lead to the slightly decreased in the energy gap. 展开更多
关键词 CO-precipitation method Ferrite Nanoparticles SPINEL Structure XRD
下载PDF
上一页 1 2 222 下一页 到第
使用帮助 返回顶部