The acute toxic effects of ammonium sulphate to fresh-water catfish, Heteropneustes fossilis (H.fossilis) have been studied by determining LC50 values with 95% confidence limits, by the graphic method, the logistic me...The acute toxic effects of ammonium sulphate to fresh-water catfish, Heteropneustes fossilis (H.fossilis) have been studied by determining LC50 values with 95% confidence limits, by the graphic method, the logistic method, the Spearman and Karber method and the trimmed Spearman-Karber method. The trimmed Spearman-Karber method was found the most ideal for ammonium salt toxicity test. The flaws in the trimmed Spearman-Karber method are also discussed.展开更多
The present paper is addressed to the finite element method combined with dynamic photoelastic analysis of propagating cracks, that is, on the basis of [1] by Chien Wei-zang, finite elements which incorporate the prop...The present paper is addressed to the finite element method combined with dynamic photoelastic analysis of propagating cracks, that is, on the basis of [1] by Chien Wei-zang, finite elements which incorporate the propagating crack-tip singularity intrinsic to two-dimensional elasticity are employed. THe relation between crack opening length and time step obtained from dynamic photoelaslie analysis is used as a definite condition for solving the dynamic equations and simulating the crack propagations as well As an example, the impact response of dynamie-bending-test specimen is investigated and the dynamic stress-intensity factor obtained from the mentioned finite element analysis and dynamic photoelasticity is in reasonable agreement with each other.展开更多
Coal seam gas content is frequently measured in quantity during underground coal mining operation and coalbed methane(CBM)exploration as a significant basic parameter.Due to the calculation error of lost gas and resid...Coal seam gas content is frequently measured in quantity during underground coal mining operation and coalbed methane(CBM)exploration as a significant basic parameter.Due to the calculation error of lost gas and residual gas in the direct method,the efficiency and accuracy of the current methods are not inadequate to the large area multi-point measurement of coal seam gas content.This paper firstly deduces a simplified theoretical dynamic model for calculating lost gas based on gas dynamic diffusion theory.Secondly,the effects of various factors on gas dynamic diffusion from coal particle are experimentally studied.And sampling procedure of representative coal particle is improved.Thirdly,a new estimation method of residual gas content based on excess adsorption and competitive adsorption theory is proposed.The results showed that the maximum error of calculating the losing gas content by using the new simplified model is only 4%.Considering the influence of particle size on gas diffusion law,the particle size of the collected coal sample is below 0.25 mm,which improves the measurement speed and reflects the safety representativeness of the sample.The determination time of gas content reduced from 36 to 3 h/piece.Moreover,the absolute error is 0.15–0.50 m^3/t,and the relative error is within 5%.A new engineering method for determining the coal seam gas content is developed according to the above research.展开更多
GB/T 13245-91 1 Theme and Scope This standard specifies the method abstract, reagents, apparatus, specimen, analyzing procedure, result calculation and permissible tolerance used for determination of the total carbon ...GB/T 13245-91 1 Theme and Scope This standard specifies the method abstract, reagents, apparatus, specimen, analyzing procedure, result calculation and permissible tolerance used for determination of the total carbon with combustion gravimetric method.展开更多
Degradation rate of feed proteins in rumen is a basic indicator of new intestinal protein system of ruminants. In this paper, determination methods of degradation rate in tureen including in-vivo method, nylon bag met...Degradation rate of feed proteins in rumen is a basic indicator of new intestinal protein system of ruminants. In this paper, determination methods of degradation rate in tureen including in-vivo method, nylon bag method and artificial rumen method are compared in order to provide a reference for animal nutrition.展开更多
The time-dependent Jones Wilkins-Lee equation products for aluminized explosives. To obtain the of state (JWL-EOS) is applied to describe detonation state time-dependent JWL-EOS parameters, cylinder tests and underw...The time-dependent Jones Wilkins-Lee equation products for aluminized explosives. To obtain the of state (JWL-EOS) is applied to describe detonation state time-dependent JWL-EOS parameters, cylinder tests and underwater explosion experiments are performed. According to the result of the wall radial velocity in cylinder tests and the shock wave pressures in underwater explosion experiments, the time-dependent JWL-EOS parameters are determined by iterating these variables in AUTODYN hydroeode simulations until the experimental values are reproduced. In addition, to verify the reliability of the derived JWL-EOS parameters, the aluminized explosive experiment is conducted in concrete. The shock wave pressures in the affected concrete bodies are measured by using manganin pressure sensors, and the rod velocity is obtained by using a high-speed camera. Simultaneously, the shock wave pressure and the rod velocity are calculated by using the derived time-dependent JWL equation of state. The calculated results are in good agreement with the experimental data.展开更多
Sudan Red are the chemosynthesis dyes of series of azo, which are mainly used as coloring additives in ma- nufacturing of some products, such as the wax, the oil-dyes, the petrol, and etc. In the process of food produ...Sudan Red are the chemosynthesis dyes of series of azo, which are mainly used as coloring additives in ma- nufacturing of some products, such as the wax, the oil-dyes, the petrol, and etc. In the process of food production, Sudan Dyes are banned to be used as food dyes in our country.展开更多
Background: Grain legumes represent a valuable energy source in pig diets due to their high starch content. The present study was conducted to determine the content and apparent ileal digestibility(AID) of starch i...Background: Grain legumes represent a valuable energy source in pig diets due to their high starch content. The present study was conducted to determine the content and apparent ileal digestibility(AID) of starch in different grain legume cultivars for pigs by means of both a polarimetric and enzymatic method for starch determination.Methods: Three experiments were conducted with six barrows each which were fitted with ileal T-cannulas. In total, 18 diets including six different cultivars of faba beans(Vicia faba L.) and peas(Pisum sativum L.), five different cultivars of lupins(Lupinus luteus L., Lupinus angustifolius L.), and one diet with a soybean meal(SBM) were fed.Results: The starch content of faba beans and peas was greater(P < 0.05) when determined polarimetrically than enzymatically(438 vs. 345 g/kg dry matter(DM) in faba beans and 509 vs. 390 g/kg DM in peas, respectively).Considerable lower starch contents were obtained in lupins and SBM, with 82 and 48 g/kg DM(analyzed polarimetrically) and <1.1 and 3 g/kg DM(analyzed enzymatically), respectively. Mean values for contents of neutral detergent fiber(NDF) and acid detergent fiber(ADF) in grain legumes ranged from 111 and 79 g/kg DM in peas to248 and 207 g/kg DM in lupins, respectively. Contents of condensed tannins in the colored flowered faba bean cultivars ranged from 2.1 to 7.4 g/kg DM. The AID of starch was greater(P < 0.05) in pea than in faba bean cultivars,and using the polarimetric starch determination method resulted in greater(P < 0.05) digestibility values than using enzymatic starch analysis(84 vs. 80% in faba beans and 86 vs. 83% in peas). Moreover, AID of starch differed(P < 0.05)within pea cultivars and starch digestibility in faba beans decreased linearly(P < 0.05) as the content of condensed tannins increased. However, there was no relationship between contents of NDF and ADF and AID of starch in pea and faba bean cultivars.Conclusion: Both contents and AID of starch in grain legumes can vary as influenced by the analytical method used for starch determination. Generally, starch digestibility is greater when measured by polarimetric rather than enzymatic methods.展开更多
A single three point bend specimen compliance method for determining JIC of high strength high fracture toughness steels is presented and a formula for calculatinff J-integral is proposed as follows.It is simple and v...A single three point bend specimen compliance method for determining JIC of high strength high fracture toughness steels is presented and a formula for calculatinff J-integral is proposed as follows.It is simple and valid for high strength high fracture toughness steels. The values of JIC and KIC measured by this method are in good agreement with those measured by standard test method.展开更多
A method to determine the design value of the extreme wave height is introduced in this paper. The method is, based on the theoretical distribution of wave heights or the experiential probability distribution of wave ...A method to determine the design value of the extreme wave height is introduced in this paper. The method is, based on the theoretical distribution of wave heights or the experiential probability distribution of wave heights, to calculate the mode of the extreme wave height and the design value with good assuredness. In fitting the experiential distribution of the observed wave heights, the paper adopts the simulating function of F(x) = 1 - exp[ ?axb exp( -cxd )] and the non-linear parameter in the function is determined by the Non-Linear Least Square Method. The practical application of the method has proved that it is not only simple and convenient, but also very effective in engineering design practice.展开更多
Proper matching of forestry machinery is important when raising mechanization levels for forestry production. In the matching process, forestry machinery needs not only expertise, but also improved methods for solving...Proper matching of forestry machinery is important when raising mechanization levels for forestry production. In the matching process, forestry machinery needs not only expertise, but also improved methods for solving problems. I propose combination of case-based reasoning (CBR) and rule-based reasoning (RBR) by calculating the similarity of quantitative parameters of various forestry machines in an analytical and hierarchical process. I calculated the similarity of machin-ery used in forest industries to enable better selection and matching of equipment. I propose a weight-value adjusting method based on sums of squares of deviations in which the individual parameter weights were modified in the process of application. During the process of system design, I put forward a design method knowledge base and generated a dynamic web reasoning framework to integrate the processes of forest industry machinery selection and weight-value adjustment. This enables expansion of the scope of the complete system and enhancement of the reasoning efficiency. I demonstrate the validity and practicability of this method using a practical example.展开更多
A fluoroimmunoassay method using unlabeled europium chelate is described.The principle is similar to that of fluoroimmunoassay method using lanthanide chelate as labels.The procedure is simple because labeling process...A fluoroimmunoassay method using unlabeled europium chelate is described.The principle is similar to that of fluoroimmunoassay method using lanthanide chelate as labels.The procedure is simple because labeling process is omitted.The detection limit is about 10^(10) mol/L antigen.The relative standard deviation of immunoassay is less than 10%.The recoveries of human serum albumin and estradiol protein conjugate are 96-105% and 111% respectively.展开更多
A fluoroimmunoassay method using unlabeled Terbium chelate is described.The principle is similar to that of fluoroimmunoassay method using lanthanide chelate as labels.The procedure is simpte because labeling process ...A fluoroimmunoassay method using unlabeled Terbium chelate is described.The principle is similar to that of fluoroimmunoassay method using lanthanide chelate as labels.The procedure is simpte because labeling process is unnecessary.The recovery of HSA and albumin in urine is 107% and 95% respectively.The standard deviation is tess than 10%.展开更多
This standard specifies the method summary, reagents, apparatus, sampling, procedure, test results calculation and permissible tolerance of the determination of magnesium oxide by CyDTA volumetric method.
A new method for the determination of components in mixed acids has been developed.The mathematical model is obtained from samples of known composition and is then used to predict the concentrations of components in u...A new method for the determination of components in mixed acids has been developed.The mathematical model is obtained from samples of known composition and is then used to predict the concentrations of components in unknown sample.The practical utility of this method is demonstrated for simultaneous determination of two systems of ternary mixed acids and the results are satisfactory.展开更多
文摘The acute toxic effects of ammonium sulphate to fresh-water catfish, Heteropneustes fossilis (H.fossilis) have been studied by determining LC50 values with 95% confidence limits, by the graphic method, the logistic method, the Spearman and Karber method and the trimmed Spearman-Karber method. The trimmed Spearman-Karber method was found the most ideal for ammonium salt toxicity test. The flaws in the trimmed Spearman-Karber method are also discussed.
文摘The present paper is addressed to the finite element method combined with dynamic photoelastic analysis of propagating cracks, that is, on the basis of [1] by Chien Wei-zang, finite elements which incorporate the propagating crack-tip singularity intrinsic to two-dimensional elasticity are employed. THe relation between crack opening length and time step obtained from dynamic photoelaslie analysis is used as a definite condition for solving the dynamic equations and simulating the crack propagations as well As an example, the impact response of dynamie-bending-test specimen is investigated and the dynamic stress-intensity factor obtained from the mentioned finite element analysis and dynamic photoelasticity is in reasonable agreement with each other.
基金the National Natural Science Foundation of China(51774119,51374095,and 51604092)the primary research projects of critical scientific research in Henan Colleges and Universities(19zx003)+1 种基金Program for Innovative Research Team in University of Ministry of Education of China(IRT_16R22)State Key Laboratory Cultivation Base for Gas Geology and Gas Control(Henan Polytechnic University)(WS2018A02)。
文摘Coal seam gas content is frequently measured in quantity during underground coal mining operation and coalbed methane(CBM)exploration as a significant basic parameter.Due to the calculation error of lost gas and residual gas in the direct method,the efficiency and accuracy of the current methods are not inadequate to the large area multi-point measurement of coal seam gas content.This paper firstly deduces a simplified theoretical dynamic model for calculating lost gas based on gas dynamic diffusion theory.Secondly,the effects of various factors on gas dynamic diffusion from coal particle are experimentally studied.And sampling procedure of representative coal particle is improved.Thirdly,a new estimation method of residual gas content based on excess adsorption and competitive adsorption theory is proposed.The results showed that the maximum error of calculating the losing gas content by using the new simplified model is only 4%.Considering the influence of particle size on gas diffusion law,the particle size of the collected coal sample is below 0.25 mm,which improves the measurement speed and reflects the safety representativeness of the sample.The determination time of gas content reduced from 36 to 3 h/piece.Moreover,the absolute error is 0.15–0.50 m^3/t,and the relative error is within 5%.A new engineering method for determining the coal seam gas content is developed according to the above research.
文摘GB/T 13245-91 1 Theme and Scope This standard specifies the method abstract, reagents, apparatus, specimen, analyzing procedure, result calculation and permissible tolerance used for determination of the total carbon with combustion gravimetric method.
文摘Degradation rate of feed proteins in rumen is a basic indicator of new intestinal protein system of ruminants. In this paper, determination methods of degradation rate in tureen including in-vivo method, nylon bag method and artificial rumen method are compared in order to provide a reference for animal nutrition.
基金Supported by the National Natural Science Foundation of China under Grant No 11172042
文摘The time-dependent Jones Wilkins-Lee equation products for aluminized explosives. To obtain the of state (JWL-EOS) is applied to describe detonation state time-dependent JWL-EOS parameters, cylinder tests and underwater explosion experiments are performed. According to the result of the wall radial velocity in cylinder tests and the shock wave pressures in underwater explosion experiments, the time-dependent JWL-EOS parameters are determined by iterating these variables in AUTODYN hydroeode simulations until the experimental values are reproduced. In addition, to verify the reliability of the derived JWL-EOS parameters, the aluminized explosive experiment is conducted in concrete. The shock wave pressures in the affected concrete bodies are measured by using manganin pressure sensors, and the rod velocity is obtained by using a high-speed camera. Simultaneously, the shock wave pressure and the rod velocity are calculated by using the derived time-dependent JWL equation of state. The calculated results are in good agreement with the experimental data.
文摘Sudan Red are the chemosynthesis dyes of series of azo, which are mainly used as coloring additives in ma- nufacturing of some products, such as the wax, the oil-dyes, the petrol, and etc. In the process of food production, Sudan Dyes are banned to be used as food dyes in our country.
基金supported by the H.W.Schaumann Stiftung(Hamburg,Germany)
文摘Background: Grain legumes represent a valuable energy source in pig diets due to their high starch content. The present study was conducted to determine the content and apparent ileal digestibility(AID) of starch in different grain legume cultivars for pigs by means of both a polarimetric and enzymatic method for starch determination.Methods: Three experiments were conducted with six barrows each which were fitted with ileal T-cannulas. In total, 18 diets including six different cultivars of faba beans(Vicia faba L.) and peas(Pisum sativum L.), five different cultivars of lupins(Lupinus luteus L., Lupinus angustifolius L.), and one diet with a soybean meal(SBM) were fed.Results: The starch content of faba beans and peas was greater(P < 0.05) when determined polarimetrically than enzymatically(438 vs. 345 g/kg dry matter(DM) in faba beans and 509 vs. 390 g/kg DM in peas, respectively).Considerable lower starch contents were obtained in lupins and SBM, with 82 and 48 g/kg DM(analyzed polarimetrically) and <1.1 and 3 g/kg DM(analyzed enzymatically), respectively. Mean values for contents of neutral detergent fiber(NDF) and acid detergent fiber(ADF) in grain legumes ranged from 111 and 79 g/kg DM in peas to248 and 207 g/kg DM in lupins, respectively. Contents of condensed tannins in the colored flowered faba bean cultivars ranged from 2.1 to 7.4 g/kg DM. The AID of starch was greater(P < 0.05) in pea than in faba bean cultivars,and using the polarimetric starch determination method resulted in greater(P < 0.05) digestibility values than using enzymatic starch analysis(84 vs. 80% in faba beans and 86 vs. 83% in peas). Moreover, AID of starch differed(P < 0.05)within pea cultivars and starch digestibility in faba beans decreased linearly(P < 0.05) as the content of condensed tannins increased. However, there was no relationship between contents of NDF and ADF and AID of starch in pea and faba bean cultivars.Conclusion: Both contents and AID of starch in grain legumes can vary as influenced by the analytical method used for starch determination. Generally, starch digestibility is greater when measured by polarimetric rather than enzymatic methods.
文摘A single three point bend specimen compliance method for determining JIC of high strength high fracture toughness steels is presented and a formula for calculatinff J-integral is proposed as follows.It is simple and valid for high strength high fracture toughness steels. The values of JIC and KIC measured by this method are in good agreement with those measured by standard test method.
文摘A method to determine the design value of the extreme wave height is introduced in this paper. The method is, based on the theoretical distribution of wave heights or the experiential probability distribution of wave heights, to calculate the mode of the extreme wave height and the design value with good assuredness. In fitting the experiential distribution of the observed wave heights, the paper adopts the simulating function of F(x) = 1 - exp[ ?axb exp( -cxd )] and the non-linear parameter in the function is determined by the Non-Linear Least Square Method. The practical application of the method has proved that it is not only simple and convenient, but also very effective in engineering design practice.
基金financially supported by the Fundamental Research Funds for the Central Universities Nos.DL12EB01-03the planning subject of "the Twelfth Five-Year-Plan" in National Science and Technology Nos.2012AA102003-2Heilongjiang Natural Science Fund in China Nos.F201116
文摘Proper matching of forestry machinery is important when raising mechanization levels for forestry production. In the matching process, forestry machinery needs not only expertise, but also improved methods for solving problems. I propose combination of case-based reasoning (CBR) and rule-based reasoning (RBR) by calculating the similarity of quantitative parameters of various forestry machines in an analytical and hierarchical process. I calculated the similarity of machin-ery used in forest industries to enable better selection and matching of equipment. I propose a weight-value adjusting method based on sums of squares of deviations in which the individual parameter weights were modified in the process of application. During the process of system design, I put forward a design method knowledge base and generated a dynamic web reasoning framework to integrate the processes of forest industry machinery selection and weight-value adjustment. This enables expansion of the scope of the complete system and enhancement of the reasoning efficiency. I demonstrate the validity and practicability of this method using a practical example.
基金This work was supported by National Natural Science Foundation of China.
文摘A fluoroimmunoassay method using unlabeled europium chelate is described.The principle is similar to that of fluoroimmunoassay method using lanthanide chelate as labels.The procedure is simple because labeling process is omitted.The detection limit is about 10^(10) mol/L antigen.The relative standard deviation of immunoassay is less than 10%.The recoveries of human serum albumin and estradiol protein conjugate are 96-105% and 111% respectively.
基金supported by National Commission of Natural Science Foundation of China.
文摘A fluoroimmunoassay method using unlabeled Terbium chelate is described.The principle is similar to that of fluoroimmunoassay method using lanthanide chelate as labels.The procedure is simpte because labeling process is unnecessary.The recovery of HSA and albumin in urine is 107% and 95% respectively.The standard deviation is tess than 10%.
文摘This standard specifies the method summary, reagents, apparatus, sampling, procedure, test results calculation and permissible tolerance of the determination of magnesium oxide by CyDTA volumetric method.
基金This project is supported by National Natural Science Foundation of China
文摘A new method for the determination of components in mixed acids has been developed.The mathematical model is obtained from samples of known composition and is then used to predict the concentrations of components in unknown sample.The practical utility of this method is demonstrated for simultaneous determination of two systems of ternary mixed acids and the results are satisfactory.