Geological characteristics of unconventional tight oil reservoir (10^(9) t): A case study of Upper Cretaceous Qingshankou Formation, northern Songliao Basin, NE China

The Daqing exploration area in the northern Songliao Basin has great potential for unconventional oil and gas resources,among which the total resources of tight oil alone exceed 109 t and is regarded as an important resource base of Daqing oilfield.After years of exploration in the Qijia area,Songliao Basin,NE China,tight oil has been found in the Upper Cretaceous Qingshankou Formation.To work out tight oil’s geological characteristics,taking tight oil in Gaotaizi oil layers of the Upper Cretaceous Qingshankou Formation in northern Songliao Basin as an example,this paper systematically analyzed the geological characteristics of unconventional tight oil in Gao3 and Gao4 layers of the Qijia area,based on the data of the geological survey,well drilling journey,well logging,and test.It is that three sets of hydrocarbon source rocks(K2qn1,K2qn2+3,and K2n1)develop in the examined area,and exhibit excellent type I and II kerogens,high organic matter abundance,and moderate maturity.The reservoir is generally composed of thin-bedded mudstone,siltstone,and sandstone,and presents poor porosity(average 8.5 vol.%)and air permeability(average 4 mD).The main reservoir space primarily includes intergranular pores,secondary soluble pores,and intergranular soluble pores.Three types of orifice throats were identified,namely fine throat,extra-fine throat,and micro-fine throat.The siltstone is generally oil-bearing,the reservoirs with slime and calcium become worse oil-bearing,and the mudstone has no obvious oil-bearing characteristics.The brittleness indices of the sandstone in the tight oil reservoir range from 40%to 60%,and those of the mudstone range from 40%to 45%,indicating a better brittleness of the tight oil reservoir.Based on the study of typical core hole data,this paper gives a comprehensive evaluation of the properties of the tight oil and establishes a tight oil single well composite bar chart as well as the initial evaluation system with the core of properties in the tight oil reservoir.This study has theoretical guiding significance and practical application value for tight oil exploration and evaluation in the Qijia area.

Design of a Simulator for Enhanced Oil Recovery Process Using a Nigerian Reservoir as a Case Study

This study involves the applications of different numerical techniques in a more general way to the design of a simulator for an enhanced oil recovery process with surfactant assisted water flooding. The data from a hypothetical oil well and a Nigerian oil well were used for the validation of the simulator. The process is represented by a system of nonlinear partial differential equations: the continuity equation for the transport of the components and Darcy’s equation for the phase flow. The orthogonal collocation, finite difference and coherence theory techniques were used in solving the equations that characterized the multidimensional, multiphase and multicomponent flow problem. Matlab computer programs were used for the numerical solution of the model equ- ations. The predicted simulator, obtained from the resulting numerical exercise confers uncondi- tional stability and more insight into the physical reservoir description. The results of the ortho- gonal collocation solution were compared with those of finite difference and coherence solutions. The results indicate that the concentration of surfactants for orthogonal collocation show more features than the predictions of the coherence solution and the finite difference, offering more opportunities for further understanding of the physical nature of the complex problem. We have found out that the partition of the three components between the two-phases determines other physical property data and hence the oil recovery. The oil recovery for the Nigerian oil reservoir is higher than the recovery predicted for the hypothetical crude. The displacement mechanism for the multicomponent and multiphase system is stable in the Nigerian oil reservoir due to the mod- erate value of the oil/water viscosity instead of the hypothetical reservoir with high value of oil/water ratio.

Classification of microscopic pore-throats and the grading evaluation on shale oil reservoirs

On the basis of the characterization of microscopic pore-throats in shale oil reservoirs by high-pressure mercury intrusion technique, a grading evaluation standard of shale oil reservoirs and a lower limit for reservoir formation were established. Simultaneously, a new method for the classification of shale oil flow units based on logging data was established. A new classification scheme for shale oil reservoirs was proposed according to the inflection points and fractal features of mercury injection curves: microscopic pore-throats(less than 25 nm), small pore-throats(25-100 nm), medium pore-throats(100-1 000 nm) and big pore-throats(greater than 1 000 nm). Correspondingly, the shale reservoirs are divided into four classes, I, II, III and IV according to the number of microscopic pores they contain, and the average pore-throat radii corresponding to the dividing points are 150 nm, 70 nm and 10 nm respectively. By using the correlation between permeability and pore-throat radius, the permeability thresholds for the reservoir classification are determined at 1.00× 10^(-3) μm^2, 0.40×10^(-3) μm^2 and 0.05×10^(-3) μm^2 respectively. By using the exponential relationship between porosity and permeability of the same hydrodynamic flow unit, a new method was set up to evaluate the reservoir flow belt index and to identify shale oil flow units with logging data. The application in the Dongying sag shows that the standard proposed is suitable for grading evaluation of shale oil reservoirs.

Enrichment model and major controlling factors of below-source tight oil in Lower Cretaceous Fuyu reservoirs in northern Songliao Basin,NE China

Based on the geochemical,seismic,logging and drilling data,the Fuyu reservoirs of the Lower Cretaceous Quantou Formation in northern Songliao Basin are systematically studied in terms of the geological characteristics,the tight oil enrichment model and its major controlling factors.First,the Quantou Formation is overlaid by high-quality source rocks of the Upper Cretaceous Qingshankou Formation,with the development of nose structure around sag and the broad and continuous distribution of sand bodies.The reservoirs are tight on the whole.Second,the configuration of multiple elements,such as high-quality source rocks,reservoir rocks,fault,overpressure and structure,controls the tight oil enrichment in the Fuyu reservoirs.The source-reservoir combination controls the tight oil distribution pattern.The pressure difference between source and reservoir drives the charging of tight oil.The fault-sandbody transport system determines the migration and accumulation of oil and gas.The positive structure is the favorable place for tight oil enrichment,and the fault-horst zone is the key part of syncline area for tight oil exploration.Third,based on the source-reservoir relationship,transport mode,accumulation dynamics and other elements,three tight oil enrichment models are recognized in the Fuyu reservoirs:(1)vertical or lateral migration of hydrocarbon from source rocks to adjacent reservoir rocks,that is,driven by overpressure,hydrocarbon generated is migrated vertically or laterally to and accumulates in the adjacent reservoir rocks;(2)transport of hydrocarbon through faults between separated source and reservoirs,that is,driven by overpressure,hydrocarbon migrates downward through faults to the sandbodies that are separated from the source rocks;and(3)migration of hydrocarbon through faults and sandbodies between separated source and reservoirs,that is,driven by overpressure,hydrocarbon migrates downwards through faults to the reservoir rocks that are separated from the source rocks,and then migrates laterally through sandbodies.Fourth,the differences in oil source conditions,charging drive,fault distribution,sandbody and reservoir physical properties cause the differential enrichment of tight oil in the Fuyu reservoirs.Comprehensive analysis suggests that the Fuyu reservoir in the Qijia-Gulong Sag has good conditions for tight oil enrichment and has been less explored,and it is an important new zone for tight oil exploration in the future.

Exploration Technology for Complex Sandstone Reservoirs in the Developed Area of Shengli Oilfield

Jiyang depression, which is the main oil productive area of Shengli oil field, is located at the southeast part of the Bohai Bay Basin and is a terrestrial lacustrine rift subsidence basin formed in the late Mesozoic with fully developed fault system. The main hydrocarbon productive formations of this depression are the terrestrial clastic rocks of the Tertiary, which are of strong lateral variation. The complex fault reservoirs and subtle lithological reservoirs distributed extensively and are becoming the main exploration targets in recent years. The exploration and development practice in these years has formed the exploration technologies, mainly including detailed study and description of low grade faults, delineation of microstructures, facies constrained formation description and prediction and low resistivity oil bearing formation’s identification. These exploration technologies have resulted in remarkable effectiveness on the reserve and oil production increments.

Effect of CO_(2)flooding in an oil reservoir with strong bottom-water drive in the Tahe Oilfield,Tarim Basin,Northwest China

The dissolution and diffusion of CO_(2)in oil and water and its displacement mechanism were investigated by laboratory experiment and numerical simulation for Block 9 in the Tahe oilfield,a sandstone oil reservoir with strong bottom-water drive in Tarim Basin,Northwest China.Such parameters were analyzed as solubility ratio of CO_(2)in oil,gas and water,interfacial tension,in-situ oil viscosity distribution,remaining oil saturation distribution,and oil compositions.The results show that CO_(2)flooding could control water coning and increase oil production.In the early stage of the injection process,CO_(2)expanded vertically due to gravity differentiation,and extended laterally under the action of strong bottom water in the intermediate and late stages.The CO_(2)got enriched and extended at the oil-water interface,forming a high interfacial tension zone,which inhibited the coning of bottom water to some extent.A miscible region with low interfacial tension formed at the gas injection front,which reduced the in-situ oil viscosity by about 50%.The numerical simulation results show that enhanced oil recovery(EOR)is estimated at 5.72%and the oil exchange ratio of CO_(2)is 0.17 t/t.

Remaining Oil Distribution Law and Potential Tapping Strategy of Horizontal Well Pattern in Narrow Oil Rim Reservoir with Gas Cap and Edge Water

For thin oil rim reservoir with gas cap and edge water, it is helpful to improve the development effect to find out the distribution law of remaining oil in this kind of reservoirs. For this reason, taking the narrow oil rim reservoir with gas cap and edge water of Oilfield A in Bohai Sea as a case, the main controlling factors, including reservoir structure, fault, gas cap energy, edge water energy and well pattern, affecting the distribution of residual oil in this kind of reservoir were analyzed by using the data of core, logging, paleogeomorphology and production. Then, the distribution law of remaining oil was summarized. Generally, the remaining oil distribution is mainly potato-shaped or strip-shaped in plane. Vertically, it depends on the energy of gas cap and edge water. For the reservoir with big gas gap and weak edge water, the remaining oil mainly lies in the bottom of oil column. And for the reservoir with small gas gap and strong edge water, the remaining oil mainly locates at the top of oil column. Aiming at different distribution modes of remaining oil, the corresponding potential tapping strategies of horizontal wells are put forward: in the late stage of development, for the reservoir with big gas gap and weak edge water, the remaining oil concentrates at the bottom of the oil column, and the position of horizontal well should be placed at the lower 1/3 to the lower 1/5 of the oil column;for the reservoir with small gas cap and strong edge water, the remaining oil locates at the top of the oil column, and the position of horizontal well should be put at the upper 1/5 to the upper 1/3 of the oil column height, vertically. Based on the study on remaining oil of Oilfield A, a potential tapping strategy of well pattern thickening and vertical position optimization of horizontal well was proposed. This strategy guided the efficient implementation of the comprehensive adjustment plan of the oilfield. Moreover, 18 infill development wells were implemented in Oilfield A, and the average production of the infill wells is 2.1 times that of the surrounding old wells. It is estimated that the ultimate recovery factor of the oilfield will reach 33.9%, which is 2.3% higher than that before infilling wells. This study can be used for reference in the development of similar reservoirs.

Quantitative prediction of oil saturation of unconsolidated sandstone reservoir based on time-lapse seismic “relative difference method”: Taking Zeta oil field in West Africa as an example

In view of the disadvantage that the absolute difference of time-lapse seismic(the difference between monitoring data and base data) is not only related to the change of oil saturation, but also closely related to the thickness of reservoir, a time-lapse seismic "relative difference method"(the ratio of monitoring data to base data) not affected by the thickness of reservoir but only related to the change of fluid saturation, is proposed through seismic forward modeling after fluid displacement simulation. Given the same change of fluid saturation, the absolute difference of time-lapse seismic conforms to the law of "tuning effect" and seismic reflection of "thin bed", and the remaining oil prediction method based on absolute difference of time-lapse seismic is only applicable to the reservoirs with uniform thickness smaller than the tuning thickness or with thickness greater than the tuning thickness. The relative difference of time-lapse seismic is not affected by reservoir thickness, but only related to the change of fluid saturation. It is applicable to all the deep-sea unconsolidated sandstone reservoirs which can exclude the effect of pressure, temperature, pore type and porosity on seismic. Therefore, the relation between the relative difference of time-lapse seismic and the change of fluid saturation, which is obtained from seismic forward modeling after Gassmann fluid displacement simulation, can be used to quantitatively predict the change of reservoir water saturation and then the distribution of the remaining oil. The application of this method in deep sea Zeta oil field in west Africa shows that it is reasonable and effective.

Pore structure differences of the extra-low permeability sandstone reservoirs and the causes of low resistivity oil layers: A case study of Block Yanwumao in the middle of Ordos Basin, NW China

The influence of pore structure difference on rock electrical characteristics of reservoir and oil reservoir was analyzed taking Triassic Chang 6 reservoir in Block Yanwumao in the middle of Ordos Basin as an example. The relationship between the pore structure difference and the low resistivity oil layer was revealed and demonstrated through core observation, lab experiments, geological research, well log interpretation and trial production etc. The results show that there were two kinds of oil layers in Chang 6 oil layer set, normal oil layer and low resistivity oil layer in the region, corresponding to two types of pore structures, pore type mono-medium and micro-fracture-pore type double-medium; the development of micro-fracture changed greatly the micro-pore structure of the reservoir, and the pore structure difference had an important influence on the rock electrical characteristics of the extra-low permeability sandstone reservoir and oil reservoir; the normal oil layers had obvious characteristics of pore-type mono-medium, and were concentrated in Chang 61, Chang 6232 and Chang 62; the low resistivity oil layers had obvious characteristics of micro-fracture-pore type double-medium, which were mainly distributed in Chang 612 and Chang 63. The mud filtrate penetrated deep into the oil layers along the micro-cracks, leading to sharp reduction of resistivity, and thus low resistivity of the oil layer; the low resistivity oil layers had better storage capacity and higher productivity than the normal oil layers.

A quantitative evaluation for well pattern adaptability in ultra-low permeability oil reservoirs:A case study of Triassic Chang 6 and Chang 8 reservoirs in Ordos Basin

Based on the previous studies and development practice in recent 10 years, a quantitative evaluation method for the adaptability of well patterns to ultra-low permeability reservoirs was established using cluster analysis and gray correlation method, and it includes 10 evaluation parameters in the four aspects of optimal evaluation parameters, determination of weights for evaluation parameters, development stage division, and determination of classification coefficients. This evaluation method was used to evaluate the well pattern adaptability of 13 main ultra-low permeability reservoirs in Triassic Chang 6 and Chang 8 of Ordos Basin. Three basic understandings were obtained: Firstly, the well pattern for ultra-low permeability type-I reservoirs has generally good adaptability, with proper well pattern forms and well pattern parameters. Secondly, square inverted nine-spot well pattern is suitable for reservoirs with no fractures; rhombic inverted nine-spot injection pattern is suitable for reservoirs with some fractures; and rectangular well pattern is suitable for reservoirs with rich fractures. Thirdly, for the ultra-low permeability type-Ⅱ and type-Ⅲ reservoirs, with the principles of well pattern form determination, the row spacing needs to be optimized further to improve the level of development of such reservoirs.

Impact of Reservoir Heterogeneity on Bitumen Content in the Mackay River Oil Sands,Athabasca(Canada)

The Lower Cretaceous Manville Group of Upper Mc Murray Formation is one of the main bitumen reservoirs in Athabasca.In this study,the relationship between reservoirs heterogeneity and bitumen geochemical characteristics were analyzed through core and microscopic observation,lab analysis,petrophysics and logging data.Based on the sedimentology framework,the formation environment of high-quality oil sand reservoirs and their significance for development were discussed.The results indicate that four types lithofacies were recognized in the Upper Mc Murray Formation based on their depositional characteristics.Each lithofacies reservoirs has unique physical properties,and is subject to varying degrees of degradation,resulting in diversity of bitumen content and geochemical composition.The tidal bar(TB)or tidal channel(TC)facies reservoir have excellent physical properties,which are evaluated as gas or water intervals due to strong degradation.The reservoir of sand bar(SB)facies was evaluated as oil intervals,due to its poor physical properties and weak degradation.The reservoir of mixed flat(MF)facies is composed of sand intercalated with laminated shale,which is evaluated as poor oil intervals due to its poor connectivity.The shale content in oil sand reservoir is very important for the reservoir physical properties and bitumen degradation degree.In the context of regional biodegradation,oil sand reservoirs with good physical properties will suffer from strong degradation,while oil sand reservoirs with relatively poor physical properties are more conducive to the bitumen preservation.

The mechanisms of thermal solidification agent promoting steam diversion in heavy oil reservoirs

At high cycles of steam huff&puff,oil distribution in reservoirs becomes stronger heterogeneity due to steam channeling.Thermal solidification agent can be used to solve this problem.Its solution is a lowviscosity liquid at normal temperature,but it can be solidified above 80℃.The plugging degree is up to 99%at 250℃.The sweep efficiency reaches 59.2%,which is 7.3%higher than pure steam injection.In addition,simultaneous injection of viscosity reducer and/or nitrogen foams can further enhance oil recovery.The mechanism of this technology depends on its strong plugging ability,which changes the flowing pattern of steam to effectively mobilize remaining oil.Viscosity reducer and nitrogen foams further expand the sweep range and extends the effective period.Therefore,thermal solidification agent can plug steam channeling paths and adjust steam flowing direction to significantly enhance oil recovery at high cycles of steam huff&puff.

Experimental analysis of matrix moveable oil saturation in tight sandstone reservoirs of the south Ordos Basin,China

Tight oil reservoirs in the south Ordos Basin are characterized by fractured,heterogeneous oil-bearing strata(an oil saturation of less than 55%on average),normal pressure(0.8±)and extra-low permeability(less than 0.3 mD).In the Chang 8 tight sandstone reservoir in Honghe oilfield,micro-and nanopores,especially those with a pore-throat radius of less than 1 mm,account for more than 90%.Fluid flow in the matrix is non-linear and crude oil flow rates are very low under normal pressure gradients.An improved understanding of oil mobility in a tight matrix is key to further development of normalpressure tight-oil resources in the continental basin.In this study,constant-velocity and high-pressure mercury injection experiments were conducted using samples of typical tight sandstone cores obtained from the south of Ordos Basin.A new method for reconstructing the full-scale pore-throat distribution characteristics of tight sandstone reservoirs was established successfully,based on which multistage centrifugal tests,tests of low-pressure differential displacement of oil by water,and nuclear magnetic resonance tests were conducted in order to obtain the distribution characteristics of moveable fluid in different pores.The moveable oil saturation(MOS)and degree of oil recovery(i.e.ratio of accumulative oil production to producing geologic reserves)of the core samples under different differential pressures for displacement were determined.As for the tight oil reservoirs in the south Ordos Basin,the moveable fluids are mainly stored in sub-micron(0.10-0.5 mm)pores.For Type I reservoirs(k>0.1 mD),the volume percentage of moveable fluid in pores with a radius larger than 0.5 mm is relatively high(greater than 40%).The degree of oil recovery of water flooding serves as the basis for forecasting recoverable reserves for tight oil reservoirs.Recoverable reserves under water flooding,mainly occur in pores with a radius greater than 0.5 mm.The contribution of Type I reserves to oil production is observed to be greater than 60%,and the degree of oil recovery reaches up to 17.1%.These results help improve our understanding on the evaluation and classification of Chang 8 tight sandstone reservoirs in Honghe oilfield and serve as theoretical basis for pilot tests to explore effective injection media and development methods to improve the matrix-driven pressure differences and displacement efficiency for oil.

Petroleum Source-Rock Evaluation and Hydrocarbon Potential in Montney Formation Unconventional Reservoir, Northeastern British Columbia, Canada

Source-rock characteristics of Lower Triassic Montney Formation presented in this study shows the total organic carbon (TOC) richness, thermal maturity, hydrocarbon generation, geographical distribution of TOC and thermal maturity (Tmax) in Fort St. John study area (T86N, R23W and T74N, R13W) and its environs in northeastern British Columbia, Western Canada Sedimentary Basin (WCSB). TOC richness in Montney Formation within the study area is grouped into three categories: low TOC ( 3.5 wt%), and high TOC (>3.5 wt% %). Thermal maturity of the Montney Formation source-rock indicates that >90% of the analyzed samples are thermally mature, and mainly within gas generating window (wet gas, condensate gas, and dry gas), and comprises mixed Type II/III (oil/gas prone kerogen), and Type IV kerogen (gas prone). Analyses of Rock-Eval parameters (TOC, S2, Tmax, HI, OI and PI) obtained from 81 samples in 11 wells that penetrated the Montney Formation in the subsurface of northeastern British Columbia were used to map source rock quality across the study area. Based on total organic carbon (TOC) content mapping, geographical distribution of thermal maturity (Tmax) data mapping, including evaluation and interpretation of Rock-Eval parameters in the study area, the Montney Formation kerogen is indicative of a pervasively matured petroleum system in the study area.

CO2 assisted steam flooding in late steam flooding in heavy oil reservoirs

To improve the oil recovery and economic efficiency in heavy oil reservoirs in late steam flooding,taking J6 Block of Xinjiang Oilfield as the research object,3D physical modeling experiments of steam flooding,CO2-foam assisted steam flooding,and CO2 assisted steam flooding under different perforation conditions are conducted,and CO2-assisted steam flooding is proposed for reservoirs in the late stage of steam flooding.The experimental results show that after adjusting the perforation in late steam flooding,the CO2 assisted steam flooding formed a lateral expansion of the steam chamber in the middle and lower parts of the injection well and a development mode for the production of overriding gravity oil drainage in the top chamber of the production well;high temperature water,oil,and CO2 formed stable low-viscosity quasi-single-phase emulsified fluid;and CO2 acted as a thermal insulation in the steam chamber at the top,reduced the steam partial pressure inside the steam chamber,and effectively improved the heat efficiency of injected steam.Based on the three-dimensional physical experiments and the developed situation of the J6 block in Xinjiang Oilfield,the CO2 assisted steam flooding for the J6 block was designed.The application showed that the CO2 assisted steam flooding made the oil vapor ratio increase from 0.12 to 0.16 by 34.0%,the oil recovery increase from 16.1%to 21.5%,and the final oil recovery goes up to 66.5%compared to steam flooding after perforation adjustment.

Synergistic anionic/zwitterionic mixed surfactant system with high emulsification efficiency for enhanced oil recovery in low permeability reservoirs

Emulsification is one of the important mechanisms of surfactant flooding. To improve oil recovery for low permeability reservoirs, a highly efficient emulsification oil flooding system consisting of anionic surfactant sodium alkyl glucosyl hydroxypropyl sulfonate(APGSHS) and zwitterionic surfactant octadecyl betaine(BS-18) is proposed. The performance of APGSHS/BS-18 mixed surfactant system was evaluated in terms of interfacial tension, emulsification capability, emulsion size and distribution, wettability alteration, temperature-resistance and salt-resistance. The emulsification speed was used to evaluate the emulsification ability of surfactant systems, and the results show that mixed surfactant systems can completely emulsify the crude oil into emulsions droplets even under low energy conditions. Meanwhile,the system exhibits good temperature and salt resistance. Finally, the best oil recovery of 25.45% is achieved for low permeability core by the mixed surfactant system with a total concentration of 0.3 wt%while the molar ratio of APGSHS:BS-18 is 4:6. The current study indicates that the anionic/zwitterionic mixed surfactant system can improve the oil flooding efficiency and is potential candidate for application in low permeability reservoirs.

Evaluation of reservoir environment by chemical properties of reservoir water‒A case study of Chang 6 reservoir in Ansai oilfield,Ordos Basin,China

The Ordos Basin is the largest continental multi-energy mineral basin in China,which is rich in coal,oil and gas,and uranium resources.The exploitation of mineral resources is closely related to reservoir water.The chemical properties of reservoir water are very important for reservoir evaluation and are significant indicators of the sealing of reservoir oil and gas resources.Therefore,the caprock of the Chang 6 reservoir in the Yanchang Formation was evaluated.The authors tested and analyzed the chemical characteristics of water samples selected from 30 wells in the Chang 6 reservoir of Ansai Oilfield in the Ordos Basin.The results show that the Chang 6 reservoir water in Ansai Oilfield is dominated by calcium-chloride water type with a sodium chloride coefficient of generally less than 0.5.The chloride magnesium coefficients are between 33.7 and 925.5,most of which are greater than 200.The desulfurization coefficients range from 0.21 to 13.4,with an average of 2.227.The carbonate balance coefficients are mainly concentrated below 0.01,with an average of 0.008.The calcium and magnesium coefficients are between 0.08 and 0.003,with an average of 0.01.Combined with the characteristics of the four-corner layout of the reservoir water,the above results show that the graphics are basically consistent.The study indicates that the Chang 6 reservoir in Ansai Oilfield in the Ordos Basin is a favorable block for oil and gas storage with good sealing properties,great preservation conditions of oil and gas,and high pore connectivity.

Mechanisms and experimental research of ion-matched waterflooding to enhance oil recovery in carbonate reservoirs: A case of Cretaceous limestone reservoirs in Halfaya Oilfield, Middle East

Based on systematically summarizing the achievements of previous ion-matched waterflooding researches,the diversity and synergy of oil recovery enhancement mechanisms and the interaction between mechanisms are examined according to two classification standards,and the influence of behaviors of different ions on different mechanisms and oil displacement efficiency are investigated.Ionic strength is proposed to characterize the behavior differences of univalent and divalent ions,the relationships between ionic strength,effective concentration,and mechanisms are established to characterize the ion behavior behind various mechanisms,and evaluate the performance of ion-matched injection water.The mechanisms of enhancing oil recovery by ion-matched waterflooding include:(1)The ion-matched water can reduce the ion strength and match the ion composition of formation water,thereby reducing the difference between the effective concentration of univalent ions and divalent ions on the surface of carbonate rocks,and improving the effective concentration of potential determining ions(especially SO42-).(2)It can improve wettability,oil-water interface properties,pore structure and physical properties of the reservoir,and finally enable the establishment of a new ionic equilibrium conducive to waterflooding while breaking the original equilibrium.In this study,experiments such as relative permeability curve,interfacial tension,and core-flooding were carried out on carbonate core samples from the Cretaceous Mishrif Formation reservoirs in Halfaya Oilfield,Middle East,a method for injection water evaluation was established and the injection water suitable for these reservoirs was selected:6 times diluted seawater.Compared with ordinary seawater,oil displacement efficiency can be increased by more than 4.60%and compared with the optimum dilution of formation water,oil displacement efficiency can be increased by 3.14%.

Research on thermal insulation materials properties under HTHP conditions for deep oil and gas reservoir rock ITP-Coring

Deep oil and gas reservoirs are under high-temperature conditions,but traditional coring methods do not consider temperature-preserved measures and ignore the influence of temperature on rock porosity and permeability,resulting in distorted resource assessments.The development of in situ temperaturepreserved coring(ITP-Coring)technology for deep reservoir rock is urgent,and thermal insulation materials are key.Therefore,hollow glass microsphere/epoxy resin thermal insulation materials(HGM/EP materials)were proposed as thermal insulation materials.The materials properties under coupled hightemperature and high-pressure(HTHP)conditions were tested.The results indicated that high pressures led to HGM destruction and that the materials water absorption significantly increased;additionally,increasing temperature accelerated the process.High temperatures directly caused the thermal conductivity of the materials to increase;additionally,the thermal conduction and convection of water caused by high pressures led to an exponential increase in the thermal conductivity.High temperatures weakened the matrix,and high pressures destroyed the HGM,which resulted in a decrease in the tensile mechanical properties of the materials.The materials entered the high elastic state at 150℃,and the mechanical properties were weakened more obviously,while the pressure led to a significant effect when the water absorption was above 10%.Meanwhile,the tensile strength/strain were 13.62 MPa/1.3%and 6.09 MPa/0.86%at 100℃ and 100 MPa,respectively,which meet the application requirements of the self-designed coring device.Finally,K46-f40 and K46-f50 HGM/EP materials were proven to be suitable for ITP-Coring under coupled conditions below 100℃ and 100 MPa.To further improve the materials properties,the interface layer and EP matrix should be optimized.The results can provide references for the optimization and engineering application of materials and thus technical support for deep oil and gas resource development.

Permeability Estimation of Shale Oil Reservoir with Laboratory-derived Data: A Case Study of the Chang 7 Member in Ordos Basin

The shale oil reservoir within the Yanchang Formations of Ordos Basin harbors substantial oil and gas resources and has recently emerged as the primary focus of unconventional oil and gas exploration and development.Due to its complex pore and throat structure,pronounced heterogeneity,and tight reservoir characteristics,the techniques for conventional oil and gas exploration and production face challenges in comprehensive implementation,also indicating that as a vital parameter for evaluating the physical properties of a reservoir,permeability cannot be effectively estimated.This study selects 21 tight sandstone samples from the Q area within the shale oil formations of Ordos Basin.We systematically conduct the experiments to measure porosity,permeability,ultrasonic wave velocities,and resistivity at varying confining pressures.Results reveal that these measurements exhibit nonlinear changes in response to effective pressure.By using these experimental data and effective medium model,empirical relationships between P-and S-wave velocities,permeability and resistivity and effective pressure are established at logging and seismic scales.Furthermore,relationships between P-wave impedance and permeability,and resistivity and permeability are determined.A comparison between the predicted permeability and logging data demonstrates that the impedance–permeability relationship yields better results in contrast to those of resistivity–permeability relationship.These relationships are further applied to the seismic interpretation of shale oil reservoir in the target layer,enabling the permeability profile predictions based on inverse P-wave impedance.The predicted results are evaluated with actual production data,revealing a better agreement between predicted results and logging data and productivity.