[Objectives] To determine the content of 10 kinds of inorganic elements(Pb,Cu,As,Cd,Hg,Zn,Fe,Mn,Sr and Cr) in samples of Paris polyphylla Smith var. yunnanensis( Franch.) Hand.-Mazz.( and polygerm varieties) produced ...[Objectives] To determine the content of 10 kinds of inorganic elements(Pb,Cu,As,Cd,Hg,Zn,Fe,Mn,Sr and Cr) in samples of Paris polyphylla Smith var. yunnanensis( Franch.) Hand.-Mazz.( and polygerm varieties) produced in different areas. [Methods] The wet digestion and technique of inductively coupled plasma optical emission spectrometry( ICP-OES) were used. [Results] Under the experimental conditions,elements were not related to each other,and several kinds of elements could be measured at the same time. The content of Pb exceeding the standard only in sample S4 of P. polyphylla Smith var. yunnanensis( and polygerm varieties),Hg was not detected in all samples,and the rest heavy metals did not exceed the limit. [Conclusions] This study was expected to provide a certain reference for the development and utilization of P. polyphylla Smith var. yunnanensis( and polygerm varieties).展开更多
[Objectives] To make original plant and microscopic identification and study the traits of Paris polyphylla Smith var. yunnanensis( Franch.) Hand.-Mazz.( polygerm varieties) produced in Gaoligong Mountain areas,and pr...[Objectives] To make original plant and microscopic identification and study the traits of Paris polyphylla Smith var. yunnanensis( Franch.) Hand.-Mazz.( polygerm varieties) produced in Gaoligong Mountain areas,and provide experimental data for their identification and application. [Methods] The original plant powder was used,and paraffin sections and physicochemical properties were identified. [Results]P. polyphylla Smith var. yunnanensis( polygerm varieties) produced in Gaoligong Mountain areas showed obvious microscopic features and physicochemical properties. [Conclusions] This study was expected to provide certain reference for identification of original plant and medicine and formulation of quality standard for P. polyphylla Smith var. yunnanensis( polygerm varieties) produced in Gaoligong Mountain areas,and provided basis for their further research and development.展开更多
目的对重楼属药用植物狭叶重楼(Paris.polyphylla.Smith var stenophylla Franch)的化学成分进行研究,为拓宽重楼属药用植物的资源提供科学依据。方法采用硅胶柱层析,大孔吸附树脂,葡聚糖凝胶SephadexLH-20及反相硅胶RP-C18中压液相柱...目的对重楼属药用植物狭叶重楼(Paris.polyphylla.Smith var stenophylla Franch)的化学成分进行研究,为拓宽重楼属药用植物的资源提供科学依据。方法采用硅胶柱层析,大孔吸附树脂,葡聚糖凝胶SephadexLH-20及反相硅胶RP-C18中压液相柱层析等技术分离纯化其主要化合物,根据理化性质、波谱数据鉴定其结构。结果从狭叶重楼乙醇提取物中分离并鉴定了5个甾体皂苷类单体化合物:重楼皂苷:Diosgenin-3-O-α-L-rhamnopyranosyl-(l→2)-[α-L-arabinofuranosyl-(1→4)]-β-D-glucopyranoside;重楼皂苷V:Diosgenin-3-O-α-L-rhamnopyranosyl-(l→2)-β-D-glucopyranoside;重楼皂苷:Pennogenin-3-O-α-L-rhamnopyranosyl(1→2)-β-D-glu-copyranoside;重楼皂苷:Pennogenin-3-O-α-L-rhamnopyranosyl-(1→4)-α-L-rhamnopyranosyl-(1→4)-[α-L-rhamnopyranosyl-(l→2)]-β-D-glucopyranoside;重楼皂苷H:Pennoge-nin-3-O-α-L-rhamnopyranosyl-(l→2)-[α-L-arabinofuranosyl-(1→4)]-β-D-Glucopyranoside。结论首次从狭叶重楼中分离并鉴定出5个甾体皂苷类化合物。展开更多
基金Supported by Key Sci-Tech Project of Sichuan Provincial Science and Technology Department(2016FZ0045)Fundamental Research Funds for the Central Universities of Southwest Minzu University(2018NZD10)
文摘[Objectives] To determine the content of 10 kinds of inorganic elements(Pb,Cu,As,Cd,Hg,Zn,Fe,Mn,Sr and Cr) in samples of Paris polyphylla Smith var. yunnanensis( Franch.) Hand.-Mazz.( and polygerm varieties) produced in different areas. [Methods] The wet digestion and technique of inductively coupled plasma optical emission spectrometry( ICP-OES) were used. [Results] Under the experimental conditions,elements were not related to each other,and several kinds of elements could be measured at the same time. The content of Pb exceeding the standard only in sample S4 of P. polyphylla Smith var. yunnanensis( and polygerm varieties),Hg was not detected in all samples,and the rest heavy metals did not exceed the limit. [Conclusions] This study was expected to provide a certain reference for the development and utilization of P. polyphylla Smith var. yunnanensis( and polygerm varieties).
基金Supported by Key Sci-Tech Project of Sichuan Provincial Science and Technology Department(2016FZ0045)Fundamental Research Funds for the Central Universities of Southwest Minzu University(2018NZD10)
文摘[Objectives] To make original plant and microscopic identification and study the traits of Paris polyphylla Smith var. yunnanensis( Franch.) Hand.-Mazz.( polygerm varieties) produced in Gaoligong Mountain areas,and provide experimental data for their identification and application. [Methods] The original plant powder was used,and paraffin sections and physicochemical properties were identified. [Results]P. polyphylla Smith var. yunnanensis( polygerm varieties) produced in Gaoligong Mountain areas showed obvious microscopic features and physicochemical properties. [Conclusions] This study was expected to provide certain reference for identification of original plant and medicine and formulation of quality standard for P. polyphylla Smith var. yunnanensis( polygerm varieties) produced in Gaoligong Mountain areas,and provided basis for their further research and development.
文摘目的对重楼属药用植物狭叶重楼(Paris.polyphylla.Smith var stenophylla Franch)的化学成分进行研究,为拓宽重楼属药用植物的资源提供科学依据。方法采用硅胶柱层析,大孔吸附树脂,葡聚糖凝胶SephadexLH-20及反相硅胶RP-C18中压液相柱层析等技术分离纯化其主要化合物,根据理化性质、波谱数据鉴定其结构。结果从狭叶重楼乙醇提取物中分离并鉴定了5个甾体皂苷类单体化合物:重楼皂苷:Diosgenin-3-O-α-L-rhamnopyranosyl-(l→2)-[α-L-arabinofuranosyl-(1→4)]-β-D-glucopyranoside;重楼皂苷V:Diosgenin-3-O-α-L-rhamnopyranosyl-(l→2)-β-D-glucopyranoside;重楼皂苷:Pennogenin-3-O-α-L-rhamnopyranosyl(1→2)-β-D-glu-copyranoside;重楼皂苷:Pennogenin-3-O-α-L-rhamnopyranosyl-(1→4)-α-L-rhamnopyranosyl-(1→4)-[α-L-rhamnopyranosyl-(l→2)]-β-D-glucopyranoside;重楼皂苷H:Pennoge-nin-3-O-α-L-rhamnopyranosyl-(l→2)-[α-L-arabinofuranosyl-(1→4)]-β-D-Glucopyranoside。结论首次从狭叶重楼中分离并鉴定出5个甾体皂苷类化合物。