[TiO2],t and pH are named as the independent variables and the percentage of decolor(DC%)as the dependent variable.A Box-Behnken design and U12(6×4×3)design with three factors were established to form the tr...[TiO2],t and pH are named as the independent variables and the percentage of decolor(DC%)as the dependent variable.A Box-Behnken design and U12(6×4×3)design with three factors were established to form the training set and the validation set,respectively.And back propagation neural network(BPNN)model is adopted in order to establish the model of photo-catalytic degradation about weak acidic dyes mixture of the GRS big red and weak acid red R.The best result shows that the correlation coefficient(R)is 0.9345 and the mean relative error between the predictive value and experimental value(MRE(%))is 3.23,for training set;the value of R is 0.9257,MRE(%)is 2.75,for the validation set.Besides,we discussed the influences of the pH,[TiO2],and t vs.DC% by the BPNN model.The optimized experimental condition obtained is pH=5.0,[TiO2]=1.50g/L,and t=40min based on the BPNN model,and combination with optimization of nonlinear constraints programming.The experimental value of DC is 99.23%,the predictive value is 98.98%,and the relative error is-0.25% between the predictive value and the experimental value,in the optimized experimental condition.Above all these indicate that the model can not only simulate the system of photo-catalytic degradation commendably but also can obtain the optimal experimental conditions.展开更多
ISO9001:2000 and TS 16949 have become the major quality system management models in present traditional and Hi-tech industries. The Measurement System Analysis (MSA) Reference Manual, on the other hand, is one of the ...ISO9001:2000 and TS 16949 have become the major quality system management models in present traditional and Hi-tech industries. The Measurement System Analysis (MSA) Reference Manual, on the other hand, is one of the core tools in ISO/TS 16949. MSA aims to evaluate Gauge Repeatability and Reproducibility (GR&R) where the control, monitoring, and maintenance of the measurement process are required in measurement systems so that the measurement capability could be ensured under statistical control. An ideal measurement system should present the statistical characteristic of zero error on any measured product. Nevertheless, such an ideal measurement system hardly exists. Managers therefore have to adopt such measurement systems with unsatisfactory statistical characteristics. Traditional MSA indexes are constructed with definite observed values. Nevertheless, measurements with observed values are not entirely error-free. For this reason, this study proposes to research three cases in a case company and apply the integration of Fuzzy Theory and GR&R to discuss the differences in the evaluation index GR&R and the Number of Distinct Categories (NDC). Substituting fuzzy numbers for definite numbers found that the data of %GR&R were increased and NDC was decreased after fuzzification. Such results verify that the fuzzified %GR&R and NDC become stricter in the determination criterion. The research outcomes could assist the case company in improving the reference data of measurement systems and promoting the measurement quality.展开更多
测量系统分析（Measurement Systems Analysis,MSA）是实验室内部质量控制常用的一种手段及方法,文章主要介绍了熔融指数仪的稳定性分析,以及重复性与再现性分析（R＆R）,通过分析,测量系统是可控的,％GRR为26.302％,介于10 ％～30％之...测量系统分析（Measurement Systems Analysis,MSA）是实验室内部质量控制常用的一种手段及方法,文章主要介绍了熔融指数仪的稳定性分析,以及重复性与再现性分析（R＆R）,通过分析,测量系统是可控的,％GRR为26.302％,介于10 ％～30％之间,而且重复性大于再现性;区别分类数ndc为5.展开更多
文摘[TiO2],t and pH are named as the independent variables and the percentage of decolor(DC%)as the dependent variable.A Box-Behnken design and U12(6×4×3)design with three factors were established to form the training set and the validation set,respectively.And back propagation neural network(BPNN)model is adopted in order to establish the model of photo-catalytic degradation about weak acidic dyes mixture of the GRS big red and weak acid red R.The best result shows that the correlation coefficient(R)is 0.9345 and the mean relative error between the predictive value and experimental value(MRE(%))is 3.23,for training set;the value of R is 0.9257,MRE(%)is 2.75,for the validation set.Besides,we discussed the influences of the pH,[TiO2],and t vs.DC% by the BPNN model.The optimized experimental condition obtained is pH=5.0,[TiO2]=1.50g/L,and t=40min based on the BPNN model,and combination with optimization of nonlinear constraints programming.The experimental value of DC is 99.23%,the predictive value is 98.98%,and the relative error is-0.25% between the predictive value and the experimental value,in the optimized experimental condition.Above all these indicate that the model can not only simulate the system of photo-catalytic degradation commendably but also can obtain the optimal experimental conditions.
文摘ISO9001:2000 and TS 16949 have become the major quality system management models in present traditional and Hi-tech industries. The Measurement System Analysis (MSA) Reference Manual, on the other hand, is one of the core tools in ISO/TS 16949. MSA aims to evaluate Gauge Repeatability and Reproducibility (GR&R) where the control, monitoring, and maintenance of the measurement process are required in measurement systems so that the measurement capability could be ensured under statistical control. An ideal measurement system should present the statistical characteristic of zero error on any measured product. Nevertheless, such an ideal measurement system hardly exists. Managers therefore have to adopt such measurement systems with unsatisfactory statistical characteristics. Traditional MSA indexes are constructed with definite observed values. Nevertheless, measurements with observed values are not entirely error-free. For this reason, this study proposes to research three cases in a case company and apply the integration of Fuzzy Theory and GR&R to discuss the differences in the evaluation index GR&R and the Number of Distinct Categories (NDC). Substituting fuzzy numbers for definite numbers found that the data of %GR&R were increased and NDC was decreased after fuzzification. Such results verify that the fuzzified %GR&R and NDC become stricter in the determination criterion. The research outcomes could assist the case company in improving the reference data of measurement systems and promoting the measurement quality.
文摘测量系统分析（Measurement Systems Analysis,MSA）是实验室内部质量控制常用的一种手段及方法,文章主要介绍了熔融指数仪的稳定性分析,以及重复性与再现性分析（R＆R）,通过分析,测量系统是可控的,％GRR为26.302％,介于10 ％～30％之间,而且重复性大于再现性;区别分类数ndc为5.
