According to the deficiency of experiment system for gas adsorption and desorption in coal mass, a large scale experiment system is developed independently by researchers. This experiment system is composed of primary...According to the deficiency of experiment system for gas adsorption and desorption in coal mass, a large scale experiment system is developed independently by researchers. This experiment system is composed of primary and auxiliary boxes, power transmission system, mining system, loading system, gas charging system, data monitoring and intelligent acquisition system. The maximum experiment coal consumption is 1200 kg, the mining system is developed to conduct experiment for gas desorption under excavating disturbance, and the plane-charging cribriform ventilation device is developed to realize uniform ventilation for experiment coal sample, which is accord with the actual gas source situation of coal bed. The desorption characteristics of gas in coal are experimentally studied under the conditions of nature and mining using the experiment system. The results show that, compare with nature condition, the permeability of coal and the velocity of gas desorption could significantly increase under the influence of coal pressure relief and destruction caused by mining, and the degree of gas desorption could somewhat increase too. Finally, pressure relief gas extraction of current seam and adjacent seams after mining in a certain coal mine of Yangquan mining area are introduced, and the gas desorption experiment results is verified by analyzing the effect of gas extraction.展开更多
In order to reveal the temperature change in coal gas desorption process,the temperature variation in coal gas desorption process under different particle sizes is analyzed with infrared thermal imager.The infrared vi...In order to reveal the temperature change in coal gas desorption process,the temperature variation in coal gas desorption process under different particle sizes is analyzed with infrared thermal imager.The infrared video signals obtained by the experiment are processed with SAT.Then the infrared radiation signals are processed by EMD with Hilbert–Huang and the infrared radiation noise is effectively removed.The research results show that the desorption process,with the change of the temperature,is an endothermic process.The coal absorbs heat when the gas is desorbed and the temperature drops.The coal body temperature drop range is obviously related to coal particle size.The smaller the particle size is,the bigger the temperature drop becomes.The temperature variation curves in the process of coal gas desorption under different particle sizes are fitted,and they comply with the exponential function.The research results lay the theoretical and experimental foundation for non-contact prediction on working face of coal and gas outburst with infrared thermal image technology.展开更多
To solve the issues of calculating gas loss quantity during sampling,simulated gas desorption process of the consumingly destruct coal with the assembly simulation testing device.Through an analysis of the simulation ...To solve the issues of calculating gas loss quantity during sampling,simulated gas desorption process of the consumingly destruct coal with the assembly simulation testing device.Through an analysis of the simulation test datum using SPSS software, established a new formula that can be better description on gas desorption process,more accurate calculation of the gas loss quantity during sampling process,and calculating re- leasable gas quantity during a certain period.Aimed at the new formula,the best time of taking sample is confirmed 3 minutes for consumingly destruct coal,the computative error is less than 10%.Through experiment at laboratory and locale,the new formula could well describe consumingly destruct coal gas desorption law,and it has high calculation preci- sion of gas loss quantity in sampling and desorption quanlity.展开更多
Based on the evolution of geological dynamics and spatial chaos theory, we proposed the advanced prediction an advanced prediction method of a gas desorption index of drill cuttings to predict coal and gas outbursts. ...Based on the evolution of geological dynamics and spatial chaos theory, we proposed the advanced prediction an advanced prediction method of a gas desorption index of drill cuttings to predict coal and gas outbursts. We investigated and verified the prediction method by a spatial series data of a gas desorption index of drill cuttings obtained from the 113112 coal roadway at the Shitai Mine. Our experimental results show that the spatial distribution of the gas desorption index of drill cuttings has some chaotic charac- teristics, which implies that the risk of coal and gas outbursts can be predicted by spatial chaos theory. We also found that a proper amount of sample data needs to be chosen in order to ensure the accuracy and practical maneuverability of prediction. The relative prediction error is small when the prediction pace is chosen carefully. In our experiments, it turned out that the optimum number of sample points is 80 and the optimum prediction pace 30. The corresponding advanced prediction pace basically meets the requirements of engineering applications.展开更多
For the question of applying high-pressure water injection to increase gas extraction efficiency by increasing the permeability of water to drive gas action, an independently designed gas desorption experimental measu...For the question of applying high-pressure water injection to increase gas extraction efficiency by increasing the permeability of water to drive gas action, an independently designed gas desorption experimental measuring device was used under the condition of external solution invasion. The law of water effect on gas desorption was obtained after water invasion through experiment for the first time. The results show that water's later invasion not only can make the quantity of gas dcsorp- tion greatly reduced, but also can make gas desorption end early. Therefore, when evaluating the applications of high-pressure water injection to increase gas extraction efficiency, we should take water damaging effects on gas desorption into account.展开更多
Adsorption-desorption experiments on CO2-CH4 gas mixtures with varying compositions have been conducted to study the fractionation characteristics of CO2-CH4 on Haishiwan coal samples. These were carried out at consta...Adsorption-desorption experiments on CO2-CH4 gas mixtures with varying compositions have been conducted to study the fractionation characteristics of CO2-CH4 on Haishiwan coal samples. These were carried out at constant temperature but different equilibrium pressure conditions. Based on these experimental results, the temporal evolution of component fractionation in the field was investigated. The results show that the CO2 concentration in the adsorbed phase is always greater than that in the original gas mixture during the desorption process, while CH4 shows the opposite characteristics. This has confirmed that CO2 , with a greater adsorption ability has a predominant position in the competition with CH4 under different pressures. Where gas drainage is employed, the ratio of CO2 to CH4 varies with time and space in floor roadways used for gas drainage, and in the ventilation air in Nos.1 and 2 coal seams, which is consistent with laboratory results.展开更多
In this study, laboratory experiments are conducted to investigate the rapid decompression and desorption induced energetic failure in coal using a shock tube apparatus. Coal specimens are recovered from Colorado at a...In this study, laboratory experiments are conducted to investigate the rapid decompression and desorption induced energetic failure in coal using a shock tube apparatus. Coal specimens are recovered from Colorado at a depth of 610 m. The coal specimens are saturated with the strong sorbing gas CO2 for a certain period and then the rupture disc is suddenly broken on top of the shock tube to generate a shock wave propagating upwards and a rarefaction wave propagating downwards through the specimen.This rapid decompression and desorption has the potential to cause energetic fragmentation in coal.Three types of behaviors in coal after rapid decompression are found, i.e. degassing without fragmentation, horizontal fragmentation, and vertical fragmentation. We speculate that the characteristics of fracture network(e.g. aperture, spacing, orientation and stiffness) and gas desorption play a role in this dynamic event as coal can be considered as a dual porosity, dual permeability, dual stiffness sorbing medium. This study has important implications in understanding energetic failure process in underground coal mines such as coal gas outbursts.展开更多
Investigation of temperature effect on mechanical parameters of coal is very important for understanding the mechanical response of coal bed at high temperature.It is especially benefcial for mitigating the thermal-in...Investigation of temperature effect on mechanical parameters of coal is very important for understanding the mechanical response of coal bed at high temperature.It is especially benefcial for mitigating the thermal-induced disasters occurred in those coal mines suffering from heat hazard.In this work,coal samples,obtained from the No.2442 working face of Baijiao Coal Mine,were subjected to uniaxial compression ranging from 20 to 40℃ with an interval of 5℃.The apparatus used was designed to obtain deformation of a stressed sample,as well as the emission of gases desorbing from coal matrix.The adsorbed gas desorption caused by heating is measured during the entire testing.It is evident that the concentrations of releasing gas(containing methane,carbon dioxide and ethane)slightly rise with increasing temperature.Gas movement observed is closely related to the deformation of coal sample.Both uniaxial compressive strength and elastic modulus of coal samples tend to reduce with temperature.It reveals that increasing temperature can not only result in thermal expansion of coal,but also lead to desorption of preexisting gas in coal which can in turns harden coal due to shrinks of the coal matrix.Even though desorption of adsorbed gas can contribute to the hardening effect for the heated coal,by comparison to the results,it could be inferred that the softening of coal resulted from thermal expansion still predominates changes in mechanical characters of coal sample with temperature at the range from20 to 40℃.展开更多
In this study, we selected 9 typical coal samples with different metamorphic grades as the study subjects,measured their initial 30-min gas desorption at 30℃ and different pressure using a self-developed gas adsorpti...In this study, we selected 9 typical coal samples with different metamorphic grades as the study subjects,measured their initial 30-min gas desorption at 30℃ and different pressure using a self-developed gas adsorption/desorption device. Based on the characteristics of gas desorption from coal samples, we proposed a direct fitting method for measurement of gas content in coalbed, analyzed the effects of sampling time on the measurement results and determined the reasonable sampling time of coal samples with different metamorphic grades at different gas adsorption pressure at equilibrium. The results show that (1)the error of gas contents obtained using the direct fitting method relative to that obtained using indirect method is less than 10%, which meets the actual on-site requirements and verifies the feasibility of the direct fitting method;(2) when the relative error is controlled within ±10%, the reasonable sampling time of coal samples is linearly related to the gas adsorption pressure at equilibrium;(3) the reasonable sampling time of coal samples with the same metamorphic grade exhibits a shortening trend with increasing gas adsorption pressure at equilibrium;(4) for coal samples with similar gas adsorption pressure at equilibrium, the reasonable sampling time of coal samples displays a shortening trend with increasing metamorphic grade. Overall, the study provides a basis for improving the measurement accuracy of gas content in coalbed.展开更多
Mine gas extraction in China is difficult due to the characteristics such as micro-porosity,low-permeability and high adsorption of coal seams.The pulsed mechanismof a high-pressure pulsed water jet was studied throug...Mine gas extraction in China is difficult due to the characteristics such as micro-porosity,low-permeability and high adsorption of coal seams.The pulsed mechanismof a high-pressure pulsed water jet was studied through theoretical analysis,experimentand field measurement.The results show that high-pressure pulsed water jet has threedynamic properties.What's more,the three dynamic effects can be found in low-permeabilitycoal seams.A new pulsed water jet with 200-1 000 Hz oscillation frequency andpeak pressure 2.5 times than average pressure was introduced.During bubble collapsing,sound vibration and instantaneous high pressures over 100 MPa enhanced the cuttingability of the high-pressure jet.Through high-pressure pulsed water jet drilling and slotting,the exposure area of coal bodies was greatly enlarged and pressure of the coal seamsrapidly decreased.Therefore,the permeability of coal seams was improved and gas absorptionrate also decreased.Application results show that gas adsorption rate decreasedby 30%-40%and the penetrability coefficient increased 100 times.This proves that high-pressurepulsed water is more efficient than other conventional methods.展开更多
By testing the temperature of the coal and the stress of the working surface, we got the variation law of coal temperature and coal stress during the excavation. The result shows that the activities of mining affect t...By testing the temperature of the coal and the stress of the working surface, we got the variation law of coal temperature and coal stress during the excavation. The result shows that the activities of mining affect the coal temperature, the fluctuation of coal temperature and the coal stress is synchronous. During the smooth change of crustal stress, the coal temperature basically keeps unchanged, when the dynamic phenomenon appears, the coal temperature changes, as well the coal stress. Therefore, we can use the online coal temperature monitoring system to test the coal temperature of the working surface continuously, and it can provide basic information for forecasting coal mine power disaster before it happens.展开更多
基金Acknowledgments This work is supported by the National Key Basic Research Program of China (2013CB227903) and the National Natural Science Foundation of China (U1361209).
文摘According to the deficiency of experiment system for gas adsorption and desorption in coal mass, a large scale experiment system is developed independently by researchers. This experiment system is composed of primary and auxiliary boxes, power transmission system, mining system, loading system, gas charging system, data monitoring and intelligent acquisition system. The maximum experiment coal consumption is 1200 kg, the mining system is developed to conduct experiment for gas desorption under excavating disturbance, and the plane-charging cribriform ventilation device is developed to realize uniform ventilation for experiment coal sample, which is accord with the actual gas source situation of coal bed. The desorption characteristics of gas in coal are experimentally studied under the conditions of nature and mining using the experiment system. The results show that, compare with nature condition, the permeability of coal and the velocity of gas desorption could significantly increase under the influence of coal pressure relief and destruction caused by mining, and the degree of gas desorption could somewhat increase too. Finally, pressure relief gas extraction of current seam and adjacent seams after mining in a certain coal mine of Yangquan mining area are introduced, and the gas desorption experiment results is verified by analyzing the effect of gas extraction.
基金provided by the National Natural Science Foundation of China (No.51174157)the Doctor Start-up Fund of Xi’an University of Science and Technology of China (No.2013QDJ005)the Research Development Fund of Xi’an University of Science and Technology of China (No.201244)
文摘In order to reveal the temperature change in coal gas desorption process,the temperature variation in coal gas desorption process under different particle sizes is analyzed with infrared thermal imager.The infrared video signals obtained by the experiment are processed with SAT.Then the infrared radiation signals are processed by EMD with Hilbert–Huang and the infrared radiation noise is effectively removed.The research results show that the desorption process,with the change of the temperature,is an endothermic process.The coal absorbs heat when the gas is desorbed and the temperature drops.The coal body temperature drop range is obviously related to coal particle size.The smaller the particle size is,the bigger the temperature drop becomes.The temperature variation curves in the process of coal gas desorption under different particle sizes are fitted,and they comply with the exponential function.The research results lay the theoretical and experimental foundation for non-contact prediction on working face of coal and gas outburst with infrared thermal image technology.
基金the National Natural Science Foundation of China(50474011)Key Project of Chinese National Programs for Fundamental Research and Development(973 Program 2006CB202204)+1 种基金Creation Foundation for Extraordinary Scholars in Henan Province of China(0421000400)Major Project of Science and Technology Tackle Key Problem in Henan Province of China(0421000400)
文摘To solve the issues of calculating gas loss quantity during sampling,simulated gas desorption process of the consumingly destruct coal with the assembly simulation testing device.Through an analysis of the simulation test datum using SPSS software, established a new formula that can be better description on gas desorption process,more accurate calculation of the gas loss quantity during sampling process,and calculating re- leasable gas quantity during a certain period.Aimed at the new formula,the best time of taking sample is confirmed 3 minutes for consumingly destruct coal,the computative error is less than 10%.Through experiment at laboratory and locale,the new formula could well describe consumingly destruct coal gas desorption law,and it has high calculation preci- sion of gas loss quantity in sampling and desorption quanlity.
基金Financial support for this work, provided by the National Basic Research Program of China (No.2011CB201204)the National Youth Science Foundation Program (No.50904068)+1 种基金the Heilongjiang Science & Technology Scientific Research Foundation Program for the Eighth Introduction of Talent (No.06-26)the National Engineering Research Center for Coal Gas Control
文摘Based on the evolution of geological dynamics and spatial chaos theory, we proposed the advanced prediction an advanced prediction method of a gas desorption index of drill cuttings to predict coal and gas outbursts. We investigated and verified the prediction method by a spatial series data of a gas desorption index of drill cuttings obtained from the 113112 coal roadway at the Shitai Mine. Our experimental results show that the spatial distribution of the gas desorption index of drill cuttings has some chaotic charac- teristics, which implies that the risk of coal and gas outbursts can be predicted by spatial chaos theory. We also found that a proper amount of sample data needs to be chosen in order to ensure the accuracy and practical maneuverability of prediction. The relative prediction error is small when the prediction pace is chosen carefully. In our experiments, it turned out that the optimum number of sample points is 80 and the optimum prediction pace 30. The corresponding advanced prediction pace basically meets the requirements of engineering applications.
文摘For the question of applying high-pressure water injection to increase gas extraction efficiency by increasing the permeability of water to drive gas action, an independently designed gas desorption experimental measuring device was used under the condition of external solution invasion. The law of water effect on gas desorption was obtained after water invasion through experiment for the first time. The results show that water's later invasion not only can make the quantity of gas dcsorp- tion greatly reduced, but also can make gas desorption end early. Therefore, when evaluating the applications of high-pressure water injection to increase gas extraction efficiency, we should take water damaging effects on gas desorption into account.
基金financially supported by the Natural Science Foundation for the Youth of China (No. 41202118)the Fundamental Research Funds for the Central Universities (No.2012QNB03)
文摘Adsorption-desorption experiments on CO2-CH4 gas mixtures with varying compositions have been conducted to study the fractionation characteristics of CO2-CH4 on Haishiwan coal samples. These were carried out at constant temperature but different equilibrium pressure conditions. Based on these experimental results, the temporal evolution of component fractionation in the field was investigated. The results show that the CO2 concentration in the adsorbed phase is always greater than that in the original gas mixture during the desorption process, while CH4 shows the opposite characteristics. This has confirmed that CO2 , with a greater adsorption ability has a predominant position in the competition with CH4 under different pressures. Where gas drainage is employed, the ratio of CO2 to CH4 varies with time and space in floor roadways used for gas drainage, and in the ventilation air in Nos.1 and 2 coal seams, which is consistent with laboratory results.
基金a partial result of funding by NIOSH under contract200-2008-25702the National Science Foundation under grant EAR-0842134
文摘In this study, laboratory experiments are conducted to investigate the rapid decompression and desorption induced energetic failure in coal using a shock tube apparatus. Coal specimens are recovered from Colorado at a depth of 610 m. The coal specimens are saturated with the strong sorbing gas CO2 for a certain period and then the rupture disc is suddenly broken on top of the shock tube to generate a shock wave propagating upwards and a rarefaction wave propagating downwards through the specimen.This rapid decompression and desorption has the potential to cause energetic fragmentation in coal.Three types of behaviors in coal after rapid decompression are found, i.e. degassing without fragmentation, horizontal fragmentation, and vertical fragmentation. We speculate that the characteristics of fracture network(e.g. aperture, spacing, orientation and stiffness) and gas desorption play a role in this dynamic event as coal can be considered as a dual porosity, dual permeability, dual stiffness sorbing medium. This study has important implications in understanding energetic failure process in underground coal mines such as coal gas outbursts.
基金Financial support for this work,provided by the National Natural Science Foundation of China(Nos.41202194,41172116 and 51074099)the Natural Science Foundation of Shandong Province(No.ZR2012EEQ021)are gratefully acknowledged
文摘Investigation of temperature effect on mechanical parameters of coal is very important for understanding the mechanical response of coal bed at high temperature.It is especially benefcial for mitigating the thermal-induced disasters occurred in those coal mines suffering from heat hazard.In this work,coal samples,obtained from the No.2442 working face of Baijiao Coal Mine,were subjected to uniaxial compression ranging from 20 to 40℃ with an interval of 5℃.The apparatus used was designed to obtain deformation of a stressed sample,as well as the emission of gases desorbing from coal matrix.The adsorbed gas desorption caused by heating is measured during the entire testing.It is evident that the concentrations of releasing gas(containing methane,carbon dioxide and ethane)slightly rise with increasing temperature.Gas movement observed is closely related to the deformation of coal sample.Both uniaxial compressive strength and elastic modulus of coal samples tend to reduce with temperature.It reveals that increasing temperature can not only result in thermal expansion of coal,but also lead to desorption of preexisting gas in coal which can in turns harden coal due to shrinks of the coal matrix.Even though desorption of adsorbed gas can contribute to the hardening effect for the heated coal,by comparison to the results,it could be inferred that the softening of coal resulted from thermal expansion still predominates changes in mechanical characters of coal sample with temperature at the range from20 to 40℃.
基金the support of the National Natural Science Foundation of China(Nos.51674158,51604168 and 51504142)the Natural Science Foundation of Shandong Province(No.ZR2016EEQ18)+2 种基金the SDUST Research Fund(No.2015JQJH105)the Qingdao Postdoctoral Applied Research Project(No.2015204)the Taishan Scholar Talent Team Support Plan for Advantaged&Unique Discipline Areas
文摘In this study, we selected 9 typical coal samples with different metamorphic grades as the study subjects,measured their initial 30-min gas desorption at 30℃ and different pressure using a self-developed gas adsorption/desorption device. Based on the characteristics of gas desorption from coal samples, we proposed a direct fitting method for measurement of gas content in coalbed, analyzed the effects of sampling time on the measurement results and determined the reasonable sampling time of coal samples with different metamorphic grades at different gas adsorption pressure at equilibrium. The results show that (1)the error of gas contents obtained using the direct fitting method relative to that obtained using indirect method is less than 10%, which meets the actual on-site requirements and verifies the feasibility of the direct fitting method;(2) when the relative error is controlled within ±10%, the reasonable sampling time of coal samples is linearly related to the gas adsorption pressure at equilibrium;(3) the reasonable sampling time of coal samples with the same metamorphic grade exhibits a shortening trend with increasing gas adsorption pressure at equilibrium;(4) for coal samples with similar gas adsorption pressure at equilibrium, the reasonable sampling time of coal samples displays a shortening trend with increasing metamorphic grade. Overall, the study provides a basis for improving the measurement accuracy of gas content in coalbed.
基金Supported by the National Natural Science Foundation of China(50604019)the Innovation Team Foundation of China(50621403)
文摘Mine gas extraction in China is difficult due to the characteristics such as micro-porosity,low-permeability and high adsorption of coal seams.The pulsed mechanismof a high-pressure pulsed water jet was studied through theoretical analysis,experimentand field measurement.The results show that high-pressure pulsed water jet has threedynamic properties.What's more,the three dynamic effects can be found in low-permeabilitycoal seams.A new pulsed water jet with 200-1 000 Hz oscillation frequency andpeak pressure 2.5 times than average pressure was introduced.During bubble collapsing,sound vibration and instantaneous high pressures over 100 MPa enhanced the cuttingability of the high-pressure jet.Through high-pressure pulsed water jet drilling and slotting,the exposure area of coal bodies was greatly enlarged and pressure of the coal seamsrapidly decreased.Therefore,the permeability of coal seams was improved and gas absorptionrate also decreased.Application results show that gas adsorption rate decreasedby 30%-40%and the penetrability coefficient increased 100 times.This proves that high-pressurepulsed water is more efficient than other conventional methods.
文摘By testing the temperature of the coal and the stress of the working surface, we got the variation law of coal temperature and coal stress during the excavation. The result shows that the activities of mining affect the coal temperature, the fluctuation of coal temperature and the coal stress is synchronous. During the smooth change of crustal stress, the coal temperature basically keeps unchanged, when the dynamic phenomenon appears, the coal temperature changes, as well the coal stress. Therefore, we can use the online coal temperature monitoring system to test the coal temperature of the working surface continuously, and it can provide basic information for forecasting coal mine power disaster before it happens.