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The Relationship between Genetic Polymorphisms of Three Gene Loci and Growth Characters of Haimen Goats
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作者 李拥军 李太坤 +3 位作者 张丽 李文婷 张浩 施健飞 《Agricultural Science & Technology》 CAS 2010年第6期112-114,182,共4页
[Objective] The paper aims to study the relationship between genetic polymorphisms of three gene loci and growth character of Haimen Goats to provide reference to promote Haimen Goat growth character and cultivate Hai... [Objective] The paper aims to study the relationship between genetic polymorphisms of three gene loci and growth character of Haimen Goats to provide reference to promote Haimen Goat growth character and cultivate Haimen Goat new strain of fast-growth.[Method] We processed analysis and related statistical analysis on three gene loci of Haimen Goats with PCR-RFLP and PCR-SSCP.[Result] The results suggested that there were two genotypes in MSTN gene IntronⅡ,GH gene exonⅠ and GH gene exonⅡ in Haimen Goats.Different genotypes of these gene loci had different effects on relative growth character of Haimen Goats.[Conclusion] This study had a significant meaning about promoting Haimen Goat avoirdupois by marker assistant option. 展开更多
关键词 Haimen goats MSTN GH POLYMORPHISMS growth character
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Growth characterization of anodic film on AZ91D magnesium alloy in an electrolyte of Na_2SiO_3 and KF 被引量:2
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作者 Weiping Li Liqun Zhu +1 位作者 Yihong Li Bo Zhao 《Journal of University of Science and Technology Beijing》 CSCD 2006年第5期450-455,共6页
Anodization of AZ91D magnesium alloy in the electrolyte solution of 0.5 mol/L of sodium silicate and 1.0 mol/L of potassium fluoride was investigated. The anodic films were characterized using optical microscopy (OM... Anodization of AZ91D magnesium alloy in the electrolyte solution of 0.5 mol/L of sodium silicate and 1.0 mol/L of potassium fluoride was investigated. The anodic films were characterized using optical microscopy (OM), scanning electron microscopy (SEM), and X-ray diffraction (XRD). The corrosion resistance of the various anodized alloys was evaluated by a fast corrosion test using the solution of hydrochloric acid and potassium dichromate. The results showed that the addition of KF resulted in the presence of NaF in the anodic film. The thickness of the anodic film formed under a constant current density of 20 mA/cm^2 for 16 rain at 60℃ exceeded 100 gm. The growth of the anodic film could be divided into three stages based on the anodizing time; the growth rate was much faster during stage Ⅱ than in stages I and Ⅲ. The anodic film exhibited the highest corrosion resistance for the AZ91 alloy, which is attributed to the fact that the anodization was maintained until the end of stage Ⅱ. 展开更多
关键词 magnesium alloy anodic film growth characterization chromate-free anodizing
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Growth Character of YBaCuO Thin Film Deposited by DC-planar Magnetron Sputtering
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作者 王超群 杨秉川 +1 位作者 王小平 王瑞坤 《Rare Metals》 SCIE EI CAS CSCD 1993年第1期57-61,共5页
The growth character and microstructure of high-T_c supereonducting YBCO thin films deposited on vari- ous substrates have been studied by X-ray diffraction, TEM and SEM.The results show that when the substrate temper... The growth character and microstructure of high-T_c supereonducting YBCO thin films deposited on vari- ous substrates have been studied by X-ray diffraction, TEM and SEM.The results show that when the substrate temperaturc is around 700~800℃ the films have a highly oriented texture with c-axis pependicular to the substrate. The structure of the single crystalline YBCO films grown epitaxially at optimal substrate tem- perature of 800℃ has been established by X-ray diffraction using Seemann-Bohlin geometry (SB). Brentano-Bragg geometry(BB),transmission Laue method and TEM. The lattice matching required for epitaxial growth is achievcd by azimuthal adjustment of the film plane with respect to the substrate plane. The sperior growth is demonstrated by film properties such as critical current density(2.4×10~6 A /cm^2,3.4× 10~6 A/cm^2 and 4.7×l0~6 A/cm^2) for films deposited on YSZ[(Zr(Y)O_2],SrTiO_3 and LaAIO_3 respectively at 77 K and zero fie1d. 展开更多
关键词 SUPERCONDUCTOR Thin film BaCuO growth character Microstructure
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Growth characteristics of spherical titanium oxide nanoparticles during the rapid gaseous detonation reaction 被引量:4
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作者 Ning Luo Hongwen Jing +3 位作者 Zhanguo Ma Yingchao Wang Guilei Sun Weidong Liu 《Particuology》 SCIE EI CAS CSCD 2016年第3期102-107,共6页
The nanosize grain growth characteristics of spherical single-crystal titanium oxide (TiO2) during the rapid gaseous detonation reaction are discussed. Based on the experimental conditions and the Chapman-Jouguet th... The nanosize grain growth characteristics of spherical single-crystal titanium oxide (TiO2) during the rapid gaseous detonation reaction are discussed. Based on the experimental conditions and the Chapman-Jouguet theory, the Kruis model was introduced to simulate the growth characteristics of spherical TiO2 nanoparticles obtained under high pressure, high temperature and by rapid reaction. The results show that the numerical analysis can satisfactorily predict the growth characteristics of spherical TiO2 nanoparticles with diameters of 15-300 nm at different affecting factors, such as concentration of particles, reaction temperature and time, which are in agreement with the obtained experimental results. We found that the increase of the gas-phase reaction temperature, time, and particle concentration affects the growth tendency of spherical nanocrystal TiO2, which provides effective theoretical support for the controllable synthesis of multi-scale nanoparticles. 展开更多
关键词 Gaseous phase detonation chemistry Chapman-Jouguet theoryKruis model Particle growth characterization
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Single Crystal Growth and Physical Property Characterization of Non-centrosymmetric Superconductor PbTaSe_2 被引量:2
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作者 龙雨佳 赵凌霄 +6 位作者 王培培 杨槐馨 李建奇 子海 任治安 任聪 陈根富 《Chinese Physics Letters》 SCIE CAS CSCD 2016年第3期103-106,共4页
We report on the single crystal growth and superconducting properties of PbTaSe2 with the non-centrosymmetric crystal structure. By using the chemicM vapor transport technique, centimeter-size single crystals are succ... We report on the single crystal growth and superconducting properties of PbTaSe2 with the non-centrosymmetric crystal structure. By using the chemicM vapor transport technique, centimeter-size single crystals are success- fully obtained. The measurement of temperature dependence of electricaJ resistivity p(T) in both normal and superconducting states indicates a quasi-two-dimensional electronic state in contrast to that of polycrystalline samples. Specific heat C(T) measurement reveals a bulk superconductivity with Tc ≈ 3.75K and a specific heat jump ratio of 1.42. All these results are in agreement with a moderately electron-phonon coupled, type-g Bardeen-Cooper-Schrieffer superconductor. 展开更多
关键词 of on in Single Crystal growth and Physical Property characterization of Non-centrosymmetric Superconductor PbTaSe2 IS that for BCS were been HIGH with
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Selective Area Growth and Characterization of GaN Nanorods Fabricated by Adjusting the Hydrogen Flow Rate and Growth Temperature with Metal Organic Chemical Vapor Deposition 被引量:1
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作者 任鹏 韩刚 +6 位作者 付丙磊 薛斌 张宁 刘喆 赵丽霞 王军喜 李晋闽 《Chinese Physics Letters》 SCIE CAS CSCD 2016年第6期145-149,共5页
CaN nanorods are successfully fabricated by adjusting the flow rate ratio of hydrogen (H2)/nitrogen (N2) and growth temperature of the selective area growth (SAG) method with metal organic chemical vapor deposit... CaN nanorods are successfully fabricated by adjusting the flow rate ratio of hydrogen (H2)/nitrogen (N2) and growth temperature of the selective area growth (SAG) method with metal organic chemical vapor deposition (MOCVD). The SAG template is obtained by nanospherical-lens photolithography. It is found that increasing the flow rate of 1-12 will change the CaN crystal shape from pyramid to vertical rod, while increasing the growth temperature will reduce the diameters of GaN rods to nanometer scale. Finally the CaN nanorods with smooth lateral surface and relatively good quality are obtained under the condition that the H2:N2 ratio is 1:1 and the growth temperature is 1030℃. The good crystal quality and orientation of GaN nanorods are confirmed by high resolution transmission electron microscopy. The cathodoluminescence spectrum suggests that the crystal and optical quality is also improved with increasing the temperature. 展开更多
关键词 of or IS as RATE GAN Selective Area growth and characterization of GaN Nanorods Fabricated by Adjusting the Hydrogen Flow Rate and growth Temperature with Metal Organic Chemical Vapor Deposition by with
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Multiphasic characterization of a plant growth promoting bacterial strain, Burkholderia sp.7016 and its effect on tomato growth in the field 被引量:13
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作者 GAO Miao ZHOU Jian-jiao +3 位作者 WANG En-tao CHEN Qian XU Jing SUN Jian-guang 《Journal of Integrative Agriculture》 SCIE CAS CSCD 2015年第9期1855-1863,共9页
Aiming at searching for plant growth promoting rhizobacteria (PGPR), a bacterium strain coded as 7016 was isolated from soybean rhizosphere and was characterized in the present study. It was identiifed as Burkholderia... Aiming at searching for plant growth promoting rhizobacteria (PGPR), a bacterium strain coded as 7016 was isolated from soybean rhizosphere and was characterized in the present study. It was identiifed as Burkholderia sp. based on 16S rDNA sequence analysis, as wel as phenotypic and biochemical characterizations. This bacterium presented nitrogenase activity, 1-aminocyclopropane-1-carboxylic acid (ACC) deaminase activity and phosphate solubilizing ability;inhibited the growth of Sclerotinia sclerotiorum, Gibberel a zeae and Verticil ium dahliae;and produced smal quantities of indole acetic acid (IAA). In green house experiments, signiifcant increases in shoot height and weight, root length and weight, and stem diameter were observed on tomato plants in 30 d after inoculation with strain 7016. Result of 16S rDNA PCR-DGGE showed that 7016 survived in the rhizosphere of tomato seedlings. In the ifeld experiments, Burkholderia sp. 7016 enhanced the tomato yield and signiifcantly promoted activities of soil urease, phosphatase, sucrase, and catalase. Al these results demonstrated Burkholderia sp. 7016 as a valuable PGPR and a candidate of biofertilizer. 展开更多
关键词 PGPR Burkholderia sp. multiphasic characterization promoting growth BIOFERTILIZER
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Preparation and characterization of AlN seeds for homogeneous growth 被引量:5
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作者 Li Zhang Haitao Qi +2 位作者 Hongjuan Cheng Lei Jin Yuezeng Shi 《Journal of Semiconductors》 EI CAS CSCD 2019年第10期104-107,共4页
Large size AlN bulk crystal has been grown on SiC heterogeneous seed by physical vapor transport (PVT). The properties of AlN wafer were characterized by high resolution X-ray diffraction (HRXRD), Raman spectroscopy, ... Large size AlN bulk crystal has been grown on SiC heterogeneous seed by physical vapor transport (PVT). The properties of AlN wafer were characterized by high resolution X-ray diffraction (HRXRD), Raman spectroscopy, etched method and atomic force microscope (AFM). Growth mechanism of AlN crystal grown on heterogeneous SiC seeds was proposed. Crystallization quality of AlN samples were improved with the growth process, which is associated with the growth mechanism. AlN single wafer has excellent crystallization quality, which is indicated by HRXRD showing the (0002),(1012) XRD FWHM of 76.3,52.5 arcsec, respectively. The surface of the AlN wafer is measured by AFM with a roughnessof 0.15 nm, which is a promising seed for AlN homogeneous growth. 展开更多
关键词 heterogeneous growth ALN SEEDS CRYSTALLIZATION quality characterIZATION
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Growth and Characterization of InAs1-xSbx with Different Sb Compositions on GaAs Substrates
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作者 孙庆灵 王禄 +6 位作者 王文奇 孙令 李美成 王文新 贾海强 周均铭 陈弘 《Chinese Physics Letters》 SCIE CAS CSCD 2015年第10期89-92,共4页
InAs1-xSbx with different compositions is grown by molecular beam epitaxy on (100)-oriented semi-insulating GaAs substrates. The increase of Sb content in the epilayer results in the deterioration of crystal quality... InAs1-xSbx with different compositions is grown by molecular beam epitaxy on (100)-oriented semi-insulating GaAs substrates. The increase of Sb content in the epilayer results in the deterioration of crystal quality and surface morphology. Hall measurements show that the carrier concentration increases with the composition of Sb. The electron mobility decreases initially, when Sb composition exceeds a certain value, and the mobility increases slightly. In this work, we emphasize the comparison of crystal quality, surface morphology and electrical properties of epilayers with different Sb compositions. 展开更多
关键词 growth and characterization of InAs x)Sb_x with Different Sb Compositions on GaAs Substrates SB
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Growth and Characterization of InSb Thin Films on GaAs(001) without Any Buffer Layers by MBE
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作者 赵晓蒙 张杨 +4 位作者 崔利杰 关敏 王保强 朱战平 曾一平 《Chinese Physics Letters》 SCIE CAS CSCD 2017年第7期177-181,共5页
We report the growth of InSb layers directly on GaAs (001) substrates without any buffer layers by molecular beam epitaxy (MBE). Influences of growth temperature and V/Ⅲ flux ratios on the crystal quality, the su... We report the growth of InSb layers directly on GaAs (001) substrates without any buffer layers by molecular beam epitaxy (MBE). Influences of growth temperature and V/Ⅲ flux ratios on the crystal quality, the surface morphology and the electrical properties of InSb thin films are investigated. The InSb samples with room- temperature mobility of 44600cm2/Vs are grown under optimized growth conditions. The effect of defects in InSb epitaxial on the electrical properties is researched, and we infer that the formation of In vacancy (VIn) and Sb anti-site (SbIn) defects is the main reason for concentrations changing with growth temperature and Sb2/In flux ratios. The mobility of the InSb sample as a function of temperature ranging from 90 K to 360K is demonstrated and the dislocation scattering mechanism and phonon scattering mechanism are discussed. 展开更多
关键词 growth and characterization of InSb Thin Films on GaAs MBE
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Growth and characterization of ferroelectric Tb_2(MoO_4)_3 crystal
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作者 徐民 于永贵 +1 位作者 张怀金 王继扬 《Journal of Rare Earths》 SCIE EI CAS CSCD 2009年第2期192-195,共4页
By using Tb407 and MoO3 as starting materials, ferroelectric Tb2(MoO4)3 crystal was grown by the Czochralski method. The as-grown crystal was pale green color, transparent and crack-free. X-ray powder diffraction (... By using Tb407 and MoO3 as starting materials, ferroelectric Tb2(MoO4)3 crystal was grown by the Czochralski method. The as-grown crystal was pale green color, transparent and crack-free. X-ray powder diffraction (XRPD), transmission spectrum, dielectric constant and polarization-electric field (P-E) hysteresis loop measurements were performed to characterize the crystal. The XRPD confirmed the as-grown crystal to be Tb2(MoO4)3. The transmission spectrum of the crystal showed that its transmittance in the entire visible and most near-infrared region was more than 70% except for an absorption peak around 486 nm. Obvious dielectric anomaly could be observed at low frequencies with increasing temperature through the dielectric constant measurement and the Curie temperature of Tb2(MoO4)3 crystal was determined to be 162.3℃ The unsaturated P-E hysteresis loops indicated that it was difficult for the ferroelectric domains in Tb2(MoO4)3 crystal to array regularly with repeated switching of the electric field. 展开更多
关键词 Tb2(MoO4)3 single crystal Czochralski growth characterIZATION rare earths
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Growth and Characterization of Gamma Glycine Single Crystals Grown from Alpha Glycine in the Presence of Sodium Acetate
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作者 T. Baraniraj P. Philominathan 《Journal of Minerals and Materials Characterization and Engineering》 2011年第4期351-356,共6页
A nonlinear optical crystal of gamma glycine was grown by slow evaporation solution growth technique using deionized water and sodium acetate. The functional groups and vibrational frequencies were identified using FT... A nonlinear optical crystal of gamma glycine was grown by slow evaporation solution growth technique using deionized water and sodium acetate. The functional groups and vibrational frequencies were identified using FTIR spectral analysis. The cell parameters were determined from single crystal X-ray diffraction analysis. Thermogravimetric analysis (TGA) and differential thermal analysis (DTA) were used to study its thermal properties. The optical transmittance window and lower cutoff wavelength have been identified by UV-absorption spectrum analysis. Second harmonic generation (SHG) efficiency measurement was carried out by powder Kurtz method. 展开更多
关键词 Nonlinear optical crystal solution growth TECHNIQUE characterIZATION TECHNIQUE second harmonic generation
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Growth and Characterization of AlInAs on InP Substrate by Molecular Beam Epitaxy
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作者 陈建新 李爱珍 邱建华 《Rare Metals》 SCIE EI CAS CSCD 1994年第2期118-121,共4页
AlxIn1-xAs with 0.47&lex&le0.62 onto (100) oriented InP substrate was grown by molecular beam epitaxy (MBE) and characterized with X-ray double crystal diffraction, low temperature photoluminescence and an ele... AlxIn1-xAs with 0.47&lex&le0.62 onto (100) oriented InP substrate was grown by molecular beam epitaxy (MBE) and characterized with X-ray double crystal diffraction, low temperature photoluminescence and an electron probe. Results show their high qualities. Strain and residual stress were studied in detail. 展开更多
关键词 ALUMINUM ARSENIC characterIZATION Crystal growth INDIUM Molecular beam epitaxy
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Phenotypic, Stress Tolerance and Plant Growth Promoting Characteristics of Rhizobial Isolates from Selected Wild Legumes of Semiarid Region, Tirupati, India 被引量:1
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作者 Y. Bhargava J. S. R. Murthy +1 位作者 T. V. Rajesh Kumar M. Narayana Rao 《Advances in Microbiology》 2016年第1期1-12,共12页
Rhizobia are vital for nitrogen input, fertility of soil and legume plant growth. Knowledge on rhizobial diversity from arid and semiarid areas is important for dry land agriculture in the context of climatic change a... Rhizobia are vital for nitrogen input, fertility of soil and legume plant growth. Knowledge on rhizobial diversity from arid and semiarid areas is important for dry land agriculture in the context of climatic change and for economic utilization. This study provides morphological, biochemical, stress tolerance and plant growth promoting characteristics of fifteen rhizobial isolates from the nodules of same number of wild legumes and one isolate from cultivated Arachis hypogea from semi-arid region, Tirupati. The bacterial isolates were confirmed as rhizobia based on colony morphology and biochemical tests. Based on the colour change of YMA-BTB medium, eight isolates were identified as slow growers and six were fast growers. The isolates differed in growth pattern, colony morphology, antibiotic resistance at higher concentrations and uniformity in utilization of carbon and nitrogen sources. The isolates are tolerant to NaCl up to one percent, displayed normal growth at temperatures 28℃ - 30℃, at neutral pH and poor growth at pH 5and 9. The isolates varied in the production of EPS and IAA, positive for phosphate solubilization and siderophore formation. This functional diversity displayed by the isolates can be utilised for the legume crop production by cross inoculation. 展开更多
关键词 Wild Legumes Rhizobia characterization Stress Tolerance Plant growth Promotion
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Growth and Characterization of Ethylene Diamine Tetra Acetate (EDTA) Doped Lithium Sulphate Monohydrate Crystals
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作者 R. Manimekalai A. Puhal Raj C. Ramachandra Raja 《Optics and Photonics Journal》 2012年第3期216-221,共6页
Nonlinear optical single crystals of Ethylene Diamine Tetra Acetate (EDTA) doped lithium sulphate monohydrate are successfully grown by using slow evaporation technique at room temperature with double distilled water ... Nonlinear optical single crystals of Ethylene Diamine Tetra Acetate (EDTA) doped lithium sulphate monohydrate are successfully grown by using slow evaporation technique at room temperature with double distilled water as solvent. In order to know its suitability for device fabrication, different characterization analyses have been performed. The single crystal X-ray diffraction (XRD) and powder X-ray diffraction methods are used for identifying the structural parameters of grown crystals. It is found that the addition of dopant doesn’t change the crystal structure. The range and percentage of optical transmission as well as absorption are ascertained by recording UV-Vis-NIR spectrum. No absorption in the entire visible region implies that it is a potential candidate for optoelectronic applications. The modes of vibration of different groups present in the crystals are identified by FT-IR technique. To understand the thermal properties, thermo gravimetric and differential thermal analyses (TGA & DTA) were carried out. The melting point was confirmed by differential scanning calorimetric (DSC) analysis. The amount of dopant included into the crystals was estimated by colorimetric method. The second harmonic generation efficiency measured by Kurtz powder technique is 0.53 times that of potassium dihydrogen orthophosphate. 展开更多
关键词 Nonlinear Optical Crystal growth from Solution characterIZATION Semi Organic Material
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Synthesis, Growth and Material Characterization of Bis L-Alanine Triethanol Amine (BLATEA) Single Crystals Grown by Slow Evaporation Technique
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作者 T. Vela P. Selvarajan T. H. Freeda 《Journal of Minerals and Materials Characterization and Engineering》 2011年第10期959-972,共14页
Bis L-alanine Triethanol amine (BLATEA) salt was synthesized by solution method and it was subjected to solubility studies. Using the solubility data, the saturated solution of the synthesized salt was prepared and si... Bis L-alanine Triethanol amine (BLATEA) salt was synthesized by solution method and it was subjected to solubility studies. Using the solubility data, the saturated solution of the synthesized salt was prepared and single crystals of Bis L-alanine Triethanol amine (BLATEA) were grown from aqueous solution by slow evaporation technique. X-ray diffraction (XRD) study was carried out to confirm the crystal structure. FTIR study reveals the functional groups of the sample. UV-Visible transmittance and absorption spectra were recorded for the sample to analyze the transparency of the grown crystal. Vickers micro hardness values were measured for the sample and from the microhardness study it is observed that BLATEA crystal is a soft material. SHG generation study was carried out to confirm the NLO activity of grown sample and also BLATEA crystal has been analyzed with dielectric 展开更多
关键词 NLO CRYSTAL CRYSTAL growth Single CRYSTAL characterization XRD FTIR MICROHARDNESS dielectric constant activation energy
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Growth and Characterization of GaInP Layers on GaAs Substrates by MOCVD
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作者 余庆选 彭瑞伍 +1 位作者 励翠云 任尧成 《Rare Metals》 SCIE EI CAS CSCD 1993年第4期264-266,共3页
GaInP is an important material in fabrication of optoelectronic and microwave devices. Growth process of GaInP by MOCVD (metal-organic chemical vapor deposition) was investigated, and the effect of growth parameters o... GaInP is an important material in fabrication of optoelectronic and microwave devices. Growth process of GaInP by MOCVD (metal-organic chemical vapor deposition) was investigated, and the effect of growth parameters on the epilayer properties was discussed. It is found that the distribution coefficient of indium is close to unity, while the growth temperature of GaInP is 700°C. The background concentration at 300K is 5.34×1015cm-3 and Hall mobility is 2.27×103cm2&middotV-1&middotS-1. 展开更多
关键词 characterIZATION Chemical vapor deposition growth (materials) Semiconductor materials SUBSTRATES
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Synthesis, Growth, Crystal Structure and Characterization of the o-Toluidinium Picrate
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作者 Kandasamy Mohana Priyadarshini Angannan Chandramohan Thangarak Uma Devi 《Journal of Crystallization Process and Technology》 2013年第4期123-129,共7页
A new organic charge transfer molecular complex salt of o-toluidinium picrate (OTP) was synthesised and the single crystals were grown by the slow solvent evaporation solution growth technique using methanol as a solv... A new organic charge transfer molecular complex salt of o-toluidinium picrate (OTP) was synthesised and the single crystals were grown by the slow solvent evaporation solution growth technique using methanol as a solvent at room temperature. Formation of the new crystal has been confirmed by single crystal X-ray diffraction (XRD) and NMR spectroscopic techniques. The crystal structure determined by single crystal X-ray diffraction indicates that both the cation and the anion are interlinked to each other by three types of intermolecular hydrogen bonds, namely N(4)-H(4A)···O(7), N(4)-H(4B)···O(5) and N(4)-H(4C)···O(7). The title compound (OTP) crystallizes in monoclinic crystal system with the centrosymmetric space group P21/c. Fourier transform infrared (FT IR) spectral analysis was used to confirm the presence of various functional groups in the grown crystal. The optical properties were analyzed by the UV-Vis-NIR and fluorescence emission studies. 展开更多
关键词 Single Crystal Organic MOLECULES Solution growth X-Ray DIFFRACTION characterIZATION Nonlinear Optical
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低维InP材料的表征和生长机理研究
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作者 牛艳萍 马淑芳 +6 位作者 董浩琰 阳智 郝晓东 韩斌 吴胜利 董海亮 许并社 《发光学报》 EI CAS CSCD 北大核心 2024年第5期779-793,共15页
磷化铟作为一种重要的Ⅲ-Ⅴ半导体材料,由于其独特的光学和电学特性,近年来备受关注。大量的研究表明,它在光电子、催化、医学等领域具有潜在的应用前景。但目前在低维InP纳米材料的可控制备和大规模合成研究中还存在一些问题有待解决... 磷化铟作为一种重要的Ⅲ-Ⅴ半导体材料,由于其独特的光学和电学特性,近年来备受关注。大量的研究表明,它在光电子、催化、医学等领域具有潜在的应用前景。但目前在低维InP纳米材料的可控制备和大规模合成研究中还存在一些问题有待解决。针对上述问题,采用化学气相沉积法(CVD)在Si/SiO_(2)衬底上成功地制备了大量高质量的InP纳米线,并用原位生长法在多晶InP衬底上生长了大量的InP纳米柱。利用扫描电子显微镜(SEM)观察所制备的纳米材料的形貌,纳米线表面光滑,直径在30~65 nm之间,纳米线组成的薄膜厚度约为35μm;纳米柱直径分布为550~850 nm,纳米柱组成的薄膜厚度约为12μm。利用能量色散谱(EDS)和X射线光电子能谱(XPS)分析了所制备的纳米材料的成分为InP。用拉曼光谱法测定了纳米材料的化学结构,并做了进一步的分析。透射电子显微镜(TEM)用于观察纳米材料的微观结构。研究发现,本研究制备的纳米线具有很高的结晶度,沿着[111]方向生长。使用选区电子衍射(SAED)分析纳米线晶体特性时发现了清晰的衍射点,表明其为单晶结构。使用光致发光光谱仪(PL)分析其发光特性,并进一步分析。最后,我们讨论了纳米线和纳米柱的形成机制,纳米线的生长遵循气-液-固(VLS)机制,纳米柱的生长遵循固-液-固(SLS)机制。这些研究为控制InP纳米材料的制备和大规模生产提供了更多可能性。 展开更多
关键词 磷化铟 纳米线 纳米柱 材料特性 生长机制
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金属锂枝晶生长机制及抑制方法进展
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作者 黄月 顾宇 商虹 《云南大学学报(自然科学版)》 CAS CSCD 北大核心 2024年第4期720-726,共7页
锂金属是高能量密度锂电池的理想负极材料,然而,锂枝晶的生长严重阻碍了其实际应用.文章介绍了锂枝晶的主要生长模型(固态电解质膜保护生长模型、电荷诱导生长模型、薄膜生长模型等)、影响因素(温度、电流密度、电极过电位、固态电解质... 锂金属是高能量密度锂电池的理想负极材料,然而,锂枝晶的生长严重阻碍了其实际应用.文章介绍了锂枝晶的主要生长模型(固态电解质膜保护生长模型、电荷诱导生长模型、薄膜生长模型等)、影响因素(温度、电流密度、电极过电位、固态电解质膜、沉积基底等)和先进表征技术(原位表征),并综述了近年来抑制锂枝晶生长的方法及研究进展(稳定沉积主体及表面修饰、固体电解质膜改性、使用高盐浓度和纳米化电解液、固体电解质等),最后,对锂金属电池的应用进行了评价和展望. 展开更多
关键词 锂枝晶 生长模型 影响因素 表征技术 抑制方法
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