The microstructure analysis was employed for the ferrific stainless steel (SUS430) with the carbon content from 0.029wt% to 0.100wt% under the simulated heating process condition. The higher carbon sample (430H) c...The microstructure analysis was employed for the ferrific stainless steel (SUS430) with the carbon content from 0.029wt% to 0.100wt% under the simulated heating process condition. The higher carbon sample (430H) contains the duplex phase microstructure at the temperature of 1150℃; on the other hand, the lower carbon content sample (430L) does not touch two phase area even at the temperature of 1450℃ and has the single phase ferritic microstructure. The carbon content need be well controlled for the 430 ferritic stainless steel since it can significantly affect the heating process curve, and the heating process may not be done in the two phase area due to the uncontrolled carbon content. With the low carbon content and the proper soaking time, the grain size is not sensitive to the heating process temperature and the soaking time. In the present heat treatment experiments, the soaking time is about 10 min, and the processing parameters can be chosen according to the requirement of the gross energy, the efficiency and the continual forming. 2008 University of Science and Technology Beijing. All rights reserved.展开更多
The temperature distribution of steel plates is affected by heating rates and heating curves in the process of induction heating.The magnetic flux density inside the induction furnace was measured,the distribution of ...The temperature distribution of steel plates is affected by heating rates and heating curves in the process of induction heating.The magnetic flux density inside the induction furnace was measured,the distribution of magnetic flux density was analyzed and the uniform area of the induction heating temperature distribution was ascertained.The locations for measuring temperature were set and the temperature in different processes was measured.The influence of heating rates and heating curves on the temperature difference of steel plates was studied.The experimental results showed that the steel plates’ temperature difference increased with the increase of the heating rate.The temperature difference was obviously affected by different heating curves when the heating rate was the same.A suitable heating curve would be beneficial to reduction of steel plates’ temperature difference.展开更多
SrMoO4 nanoplates were synthesized by a facile reverse microemulsion method at room temperature.Energy evolution of this in situ growth process was monitored by means of a microcalorimeter.A sharp exothermic peak for ...SrMoO4 nanoplates were synthesized by a facile reverse microemulsion method at room temperature.Energy evolution of this in situ growth process was monitored by means of a microcalorimeter.A sharp exothermic peak for the initial reaction and two discontinuous relatively weak exothermic peaks for the subsequent crystal growth emerged on the microcalorimetric heat flow curve.Based on the in situ thermokinetic data,the rate constants of the nucleation process and crystallization process at 298.15 K were calculated to be 4.078×10-3 and 5.033×10-4 s-1,respectively.The growth mechanism and energy evolution were investigated.展开更多
Obtaining small carbides is crucial but difficult for high-speed steels.A new approach for refining carbide dimensions in M42 super hard high-speed steel by increasing cooling rate and spheroidizing treatment was prop...Obtaining small carbides is crucial but difficult for high-speed steels.A new approach for refining carbide dimensions in M42 super hard high-speed steel by increasing cooling rate and spheroidizing treatment was proposed.The morphologies and properties of eutectic carbides formed at different cooling rates were investigated by means of scanning electron microscopy(SEM),energy dispersive spectroscopy(EDS),X-ray diffraction(XRD),transmission electron microscopy(TEM),electron back-scattered diffraction(EBSD)and differential scanning calorimeter(DSC).The results show that eutectic carbides change from a lamellar shape into a curved-rod shape as cooling rate increases.Despite different morphologies,the two carbides are both of M2C type with a hexagonal close-packed structure and display a single crystal orientation in one eutectic colony.The morphology of M2C mainly depends on the growing process of eutectic carbides,which is strongly influenced by cooling rate.Compared with lamellar carbides,M2C carbides with curved-rod shapes are less stable,and decompose into M6 C and MC at lower temperatures.They are more inclined to spheroidize during heating,which ultimately and distinguishably refines the carbide dimensions.As small carbides are much easier to dissolve into matrices during austenization,the process described herein improves the supersaturation of alloying elements in martensite,which leads to an increment of hardness in M42 steel.展开更多
文摘The microstructure analysis was employed for the ferrific stainless steel (SUS430) with the carbon content from 0.029wt% to 0.100wt% under the simulated heating process condition. The higher carbon sample (430H) contains the duplex phase microstructure at the temperature of 1150℃; on the other hand, the lower carbon content sample (430L) does not touch two phase area even at the temperature of 1450℃ and has the single phase ferritic microstructure. The carbon content need be well controlled for the 430 ferritic stainless steel since it can significantly affect the heating process curve, and the heating process may not be done in the two phase area due to the uncontrolled carbon content. With the low carbon content and the proper soaking time, the grain size is not sensitive to the heating process temperature and the soaking time. In the present heat treatment experiments, the soaking time is about 10 min, and the processing parameters can be chosen according to the requirement of the gross energy, the efficiency and the continual forming. 2008 University of Science and Technology Beijing. All rights reserved.
文摘The temperature distribution of steel plates is affected by heating rates and heating curves in the process of induction heating.The magnetic flux density inside the induction furnace was measured,the distribution of magnetic flux density was analyzed and the uniform area of the induction heating temperature distribution was ascertained.The locations for measuring temperature were set and the temperature in different processes was measured.The influence of heating rates and heating curves on the temperature difference of steel plates was studied.The experimental results showed that the steel plates’ temperature difference increased with the increase of the heating rate.The temperature difference was obviously affected by different heating curves when the heating rate was the same.A suitable heating curve would be beneficial to reduction of steel plates’ temperature difference.
基金Supported by the National Natural Science Foundation of China(No.20963001)the Major Project of Natural Science Foundation of Guangxi Province,China(No.0991001Z)
文摘SrMoO4 nanoplates were synthesized by a facile reverse microemulsion method at room temperature.Energy evolution of this in situ growth process was monitored by means of a microcalorimeter.A sharp exothermic peak for the initial reaction and two discontinuous relatively weak exothermic peaks for the subsequent crystal growth emerged on the microcalorimetric heat flow curve.Based on the in situ thermokinetic data,the rate constants of the nucleation process and crystallization process at 298.15 K were calculated to be 4.078×10-3 and 5.033×10-4 s-1,respectively.The growth mechanism and energy evolution were investigated.
基金Item Sponsored by National Natural Science Foundation of China(51301038,51201031,51371050)Industry-Academia-Research Program of Jiangsu Province of China(BY2014127-03)+1 种基金Natural Science Foundation of Jiangsu Province of China(BK20141306)Jiangsu Province Key Laboratory of High-end Structural Materials of China(hsm1404)
文摘Obtaining small carbides is crucial but difficult for high-speed steels.A new approach for refining carbide dimensions in M42 super hard high-speed steel by increasing cooling rate and spheroidizing treatment was proposed.The morphologies and properties of eutectic carbides formed at different cooling rates were investigated by means of scanning electron microscopy(SEM),energy dispersive spectroscopy(EDS),X-ray diffraction(XRD),transmission electron microscopy(TEM),electron back-scattered diffraction(EBSD)and differential scanning calorimeter(DSC).The results show that eutectic carbides change from a lamellar shape into a curved-rod shape as cooling rate increases.Despite different morphologies,the two carbides are both of M2C type with a hexagonal close-packed structure and display a single crystal orientation in one eutectic colony.The morphology of M2C mainly depends on the growing process of eutectic carbides,which is strongly influenced by cooling rate.Compared with lamellar carbides,M2C carbides with curved-rod shapes are less stable,and decompose into M6 C and MC at lower temperatures.They are more inclined to spheroidize during heating,which ultimately and distinguishably refines the carbide dimensions.As small carbides are much easier to dissolve into matrices during austenization,the process described herein improves the supersaturation of alloying elements in martensite,which leads to an increment of hardness in M42 steel.