The paper gives an overview on experimental observations of the failure behavior of electrically insulating and conducting cracks in piezoelectric ce- ramics.The experiments include the indentation fracture test,the b...The paper gives an overview on experimental observations of the failure behavior of electrically insulating and conducting cracks in piezoelectric ce- ramics.The experiments include the indentation fracture test,the bending test on smooth samples,and the fracture test on pre-notched(or pre-cracked)compact ten- sion samples.For electrically insulating cracks,the experimental results show a com- plicated fracture behavior under electrical and mechanical loading.Fracture data are much scattered when a static electric field is applied.A statistically based frac- ture criterion is required.For electrically conducting cracks,the experimental results demonstrate that static electric fields can fracture poled and depoled lead zirconate titanate ceramics and that the concepts of fracture mechanics can be used to mea- sure the electrical fracture toughness.Furthermore,the electrical fracture toughness is much higher than the mechanical fracture toughness.The highly electrical fracture toughness arises from the greater energy dissipation around the conductive crack tip under purely electric loading,which is impossible under mechanical loading in the brittle ceramics.展开更多
Instrumented and Vickers indentation testing and microstructure analysis were used to investigate zirconia toughened alumina (ZTA) and silicon carbide (SIC). Several equations were studied to relate the Vickers in...Instrumented and Vickers indentation testing and microstructure analysis were used to investigate zirconia toughened alumina (ZTA) and silicon carbide (SIC). Several equations were studied to relate the Vickers indentation hardness, Young's modulus and crack behavior to the fracture toughness. The frac- ture in SiC is unstable and occurs primarily by cleavage leading to a relatively low toughness of 3 MPa m1/2, which may be inappropriate for multi-hit capability. ZTA absorbs energy by plastic deformation, pore collapse, crack deviation and crack bridging and exhibits time dependent creep. With a relatively high toughness around 6.6 MPa m1/2, ZTA is promising for multi-hit capability. The higher accuracy of median equations in calculating the indentation fracture toughness and the relatively high c/a ratios above 2.5 suggest median type cracking for both SiC and ZTA. The Young's modulus of both ceramics was most accurately measured at lower indentation loads of about 0.5 kgf, while more accurate hardness and fracture toughness values were obtained at intermediate and at higher indentation loads beyond 5 kgf, respectively. A strong indentation size effect (ISE) was observed in both materials. The load independent hardness of SiC is 2563 HV, putting it far above the standard armor hardness requirement of 1500 HV that is barely met by ZTA.展开更多
基金The project supported by an RGC grant from the Research Grant Council of the Hong Kong Special Administrative RegionChina
文摘The paper gives an overview on experimental observations of the failure behavior of electrically insulating and conducting cracks in piezoelectric ce- ramics.The experiments include the indentation fracture test,the bending test on smooth samples,and the fracture test on pre-notched(or pre-cracked)compact ten- sion samples.For electrically insulating cracks,the experimental results show a com- plicated fracture behavior under electrical and mechanical loading.Fracture data are much scattered when a static electric field is applied.A statistically based frac- ture criterion is required.For electrically conducting cracks,the experimental results demonstrate that static electric fields can fracture poled and depoled lead zirconate titanate ceramics and that the concepts of fracture mechanics can be used to mea- sure the electrical fracture toughness.Furthermore,the electrical fracture toughness is much higher than the mechanical fracture toughness.The highly electrical fracture toughness arises from the greater energy dissipation around the conductive crack tip under purely electric loading,which is impossible under mechanical loading in the brittle ceramics.
基金partially supported by the DRDC-Valcartier,via DND funded project A1-000968
文摘Instrumented and Vickers indentation testing and microstructure analysis were used to investigate zirconia toughened alumina (ZTA) and silicon carbide (SIC). Several equations were studied to relate the Vickers indentation hardness, Young's modulus and crack behavior to the fracture toughness. The frac- ture in SiC is unstable and occurs primarily by cleavage leading to a relatively low toughness of 3 MPa m1/2, which may be inappropriate for multi-hit capability. ZTA absorbs energy by plastic deformation, pore collapse, crack deviation and crack bridging and exhibits time dependent creep. With a relatively high toughness around 6.6 MPa m1/2, ZTA is promising for multi-hit capability. The higher accuracy of median equations in calculating the indentation fracture toughness and the relatively high c/a ratios above 2.5 suggest median type cracking for both SiC and ZTA. The Young's modulus of both ceramics was most accurately measured at lower indentation loads of about 0.5 kgf, while more accurate hardness and fracture toughness values were obtained at intermediate and at higher indentation loads beyond 5 kgf, respectively. A strong indentation size effect (ISE) was observed in both materials. The load independent hardness of SiC is 2563 HV, putting it far above the standard armor hardness requirement of 1500 HV that is barely met by ZTA.