A series of impact tests of sandwich samples were completed using a large-diameter split Hopkinson pressure bar (SHPB)device at different velocities. The interlayer is made of foam concrete, loess or sand. The stress ...A series of impact tests of sandwich samples were completed using a large-diameter split Hopkinson pressure bar (SHPB)device at different velocities. The interlayer is made of foam concrete, loess or sand. The stress peak value decay, energy decay and waveform dispersion characters are studied by comparing the incident waves with the transmission waves. The tests indicate that the foam concrete has the best capabilities of shock resistance and energy absorption, the loess comes second, and the sand takes third place.展开更多
Methacrylate-based monolithic column was prepared in fused-silica capillary (80 ′ 0.32 mm i.d.) by in situ polymerizetion reaction using glycidyl methacrylate as monomer;ethylene dimethacrylate as crosslinker;1-propa...Methacrylate-based monolithic column was prepared in fused-silica capillary (80 ′ 0.32 mm i.d.) by in situ polymerizetion reaction using glycidyl methacrylate as monomer;ethylene dimethacrylate as crosslinker;1-propanol, 1,4-butanediol, and water as porogenic solvents. The monolith matrix was modified with trimethylamine to create strong anion exchanger via ring opening reaction of epoxy groups. The morphology of the monolithic column was studied by using Scanning Electron Microscope (SEM). This column had good mechanical stability and permeability. The effects of various mobile phases for separation of inorganic anions were investigated. Iodate, bromate, nitrite, bromide, and nitrate were separated within 11 min using100 mMpotassium chloride as mobile phase and detected at 210 nm. This method showed good precision of retention time, acceptable linearity and good sensitivity. Under the optimum condition, the RSD of the retention time was in the range of 1.09%-1.75% (n = 6). The calibration curve showed linear relationships between the peak area and the concentration. The limits of detection (LOD) and the limits of quantitation (LOQ) were between 0.08-0.18 mM and 0.26-0.61 mM, respectively. This method was applied to the determination of inorganic anions in tap water and ground water samples.展开更多
Advances in developing high entropy alloys and ceramics with improved physical properties have greatly broadened their application field from aerospace industry,public transportation to nuclear plants.In this review,w...Advances in developing high entropy alloys and ceramics with improved physical properties have greatly broadened their application field from aerospace industry,public transportation to nuclear plants.In this review,we describe the concept of entropy engineering as applicable to inorganic non-metallic glasses,especially for tailoring and enhancing their mechanical,electrical,and optical properties.We also present opportunities and challenges in calculating entropy of inorganic non-metallic glass systems,correlating entropy to glass formation,and in developing functional inorganic non-metallic glasses via the entropy concept.展开更多
Acetonitrile inorganic salt aqueous two-phase extraction method was established for the determination of triazine herbicides(simeton,cyanazine,desmetryn,terbumeton,terbuthylazine and dimethametryn)in environmental wat...Acetonitrile inorganic salt aqueous two-phase extraction method was established for the determination of triazine herbicides(simeton,cyanazine,desmetryn,terbumeton,terbuthylazine and dimethametryn)in environmental water samples by high-performance liquid chromatography(HPLC).The extraction solvents types and volume of acetonitrile,the inorganic salt types and amount of(NH_(4))_(2)SO_(4),extraction time and pH of sample solution were optimized by single-factor experiment and central composite design.Under the optimum extraction conditions,all linear ranges were obtained with coefficients of determination(r)≥0.9993.The limits of detection for this proposed method were in the range of 0.16-0.28μg/L for six triazine herbicides.The developed method has been successfully applied to the analysis of target triazine herbicides from lake,canal and moat in real-world water samples.The recoveries of target analytes were in the range from 87.0 to 110.9%and the relative standard deviation was lower than 7.3%.展开更多
文摘A series of impact tests of sandwich samples were completed using a large-diameter split Hopkinson pressure bar (SHPB)device at different velocities. The interlayer is made of foam concrete, loess or sand. The stress peak value decay, energy decay and waveform dispersion characters are studied by comparing the incident waves with the transmission waves. The tests indicate that the foam concrete has the best capabilities of shock resistance and energy absorption, the loess comes second, and the sand takes third place.
文摘Methacrylate-based monolithic column was prepared in fused-silica capillary (80 ′ 0.32 mm i.d.) by in situ polymerizetion reaction using glycidyl methacrylate as monomer;ethylene dimethacrylate as crosslinker;1-propanol, 1,4-butanediol, and water as porogenic solvents. The monolith matrix was modified with trimethylamine to create strong anion exchanger via ring opening reaction of epoxy groups. The morphology of the monolithic column was studied by using Scanning Electron Microscope (SEM). This column had good mechanical stability and permeability. The effects of various mobile phases for separation of inorganic anions were investigated. Iodate, bromate, nitrite, bromide, and nitrate were separated within 11 min using100 mMpotassium chloride as mobile phase and detected at 210 nm. This method showed good precision of retention time, acceptable linearity and good sensitivity. Under the optimum condition, the RSD of the retention time was in the range of 1.09%-1.75% (n = 6). The calibration curve showed linear relationships between the peak area and the concentration. The limits of detection (LOD) and the limits of quantitation (LOQ) were between 0.08-0.18 mM and 0.26-0.61 mM, respectively. This method was applied to the determination of inorganic anions in tap water and ground water samples.
基金financial support from the National Key Research and Development Program of China(Grant No.2020YFB1805901)the National Science Fund for Distinguished Young Scholars(Grant No.62125502)+5 种基金the National Natural Science Foundation of China(Grant No.51972113)the Key Program of Guangzhou Scientific Research Special Project(Grant No.201904020013)the Key Research and Development Program of Guangzhou(Grant No.202007020003)the Science and Technology Project of Guangdong Province(Grant No.2021A0505030004)the Local Innovative and Research Teams Project of Guangdong Pearl River Talents Program(Grant No.2017BT01×137)the Fundamental Research Funds for the Central University.
文摘Advances in developing high entropy alloys and ceramics with improved physical properties have greatly broadened their application field from aerospace industry,public transportation to nuclear plants.In this review,we describe the concept of entropy engineering as applicable to inorganic non-metallic glasses,especially for tailoring and enhancing their mechanical,electrical,and optical properties.We also present opportunities and challenges in calculating entropy of inorganic non-metallic glass systems,correlating entropy to glass formation,and in developing functional inorganic non-metallic glasses via the entropy concept.
基金the major project of Natural Science Foundation of Jiangsu Higher Education Institutions of China(no:15KJA610003)Natural Science Foundation of Jiangsu Province(no.BK20160359)Natural Science and Technology Program on Water Pollution Control and Treatment(2017ZX07205-2).
文摘Acetonitrile inorganic salt aqueous two-phase extraction method was established for the determination of triazine herbicides(simeton,cyanazine,desmetryn,terbumeton,terbuthylazine and dimethametryn)in environmental water samples by high-performance liquid chromatography(HPLC).The extraction solvents types and volume of acetonitrile,the inorganic salt types and amount of(NH_(4))_(2)SO_(4),extraction time and pH of sample solution were optimized by single-factor experiment and central composite design.Under the optimum extraction conditions,all linear ranges were obtained with coefficients of determination(r)≥0.9993.The limits of detection for this proposed method were in the range of 0.16-0.28μg/L for six triazine herbicides.The developed method has been successfully applied to the analysis of target triazine herbicides from lake,canal and moat in real-world water samples.The recoveries of target analytes were in the range from 87.0 to 110.9%and the relative standard deviation was lower than 7.3%.
