Porous C/C-SiC composites were prepared through a two-step chemical vapor infiltration process,and a multi-interlayer joint of Li20-MgO-Al2O3-SiO2(LMAS) was applied to join C/C-SiC composites and lithium aluminum si...Porous C/C-SiC composites were prepared through a two-step chemical vapor infiltration process,and a multi-interlayer joint of Li20-MgO-Al2O3-SiO2(LMAS) was applied to join C/C-SiC composites and lithium aluminum silicate(LAS) glass ceramics by means of a vacuum hot-pressing technique.Plenty of SiC whiskers were generated in the pores of low-density C/C composites during chemical vapor deposition process,which is essentia! to form a zigzag interface structure between C/C-SiC substrate and the LMAS interlayer.The average shear strength of the LMAS joint was improved from 12.17 to 19.91 MPa after changing the composites from high-density C/C composites(1.75 g/cm3) with a CVD-SiC coating to the C/C-SiC composites with a low density(1.48 g/cm3).The improvement of the joint strength is mainly attributed to the formation of the inlay structure at the SiC-C/C and SiC-LMAS interfaces.展开更多
Alumina specimens were joined together with thin aluminium interlayer at 750 and 900°C under different applied pressures and holding time in air. Flexural strength of the joints was then measured using a standard...Alumina specimens were joined together with thin aluminium interlayer at 750 and 900°C under different applied pressures and holding time in air. Flexural strength of the joints was then measured using a standard four-point bend test method. Characterization of the interface was carried out to correlate the increase in flexural strength with the applied pressure, holding temperature and time. The study showed that the strength of joint is affected by all three parameters, i.e., processing temperature, holding time as well as applied pressure.展开更多
基金funding supported from the National Natural Science Foundation of China(Grant Nos.51221001 and 51222207)the "111" Project(Grant No.B08040)the Foundation of the National Excellent Doctoral Dissertation of China(No.201036)
文摘Porous C/C-SiC composites were prepared through a two-step chemical vapor infiltration process,and a multi-interlayer joint of Li20-MgO-Al2O3-SiO2(LMAS) was applied to join C/C-SiC composites and lithium aluminum silicate(LAS) glass ceramics by means of a vacuum hot-pressing technique.Plenty of SiC whiskers were generated in the pores of low-density C/C composites during chemical vapor deposition process,which is essentia! to form a zigzag interface structure between C/C-SiC substrate and the LMAS interlayer.The average shear strength of the LMAS joint was improved from 12.17 to 19.91 MPa after changing the composites from high-density C/C composites(1.75 g/cm3) with a CVD-SiC coating to the C/C-SiC composites with a low density(1.48 g/cm3).The improvement of the joint strength is mainly attributed to the formation of the inlay structure at the SiC-C/C and SiC-LMAS interfaces.
文摘Alumina specimens were joined together with thin aluminium interlayer at 750 and 900°C under different applied pressures and holding time in air. Flexural strength of the joints was then measured using a standard four-point bend test method. Characterization of the interface was carried out to correlate the increase in flexural strength with the applied pressure, holding temperature and time. The study showed that the strength of joint is affected by all three parameters, i.e., processing temperature, holding time as well as applied pressure.