In-situ characterization of non-aqueous nano-dispersion systems（NANDS） by freeze-etching transmission electron microscope（FETEM） was reported.To improve just-for-once successive rate of specimen preparation and ge...In-situ characterization of non-aqueous nano-dispersion systems（NANDS） by freeze-etching transmission electron microscope（FETEM） was reported.To improve just-for-once successive rate of specimen preparation and get good characterization results,an improving specimen preparation method of freezing etching was developed.Size,distribution and morphology of NANDS were directly visualized.Some information of particle dispersion feature and particle density can also be obtained.Reproductivity of the FETEM characterization is excellent.Comparing with laser scattering method,which is liable to give positive error especially for small size particle anchoring disperser,FETEM characterization can give more accurate measurement of particle size.Moreover,FETEM can give dispersion feature of nanoparticle in non-aqueous medium.展开更多
The flow field in a typical inward-turning inlet was visualized using the Planar Laser Scattering(PLS)method in a shock tunnel with a nominal Mach number of 6.The opaque inlet,which is truncated at a series of section...The flow field in a typical inward-turning inlet was visualized using the Planar Laser Scattering(PLS)method in a shock tunnel with a nominal Mach number of 6.The opaque inlet,which is truncated at a series of sections,and the following transparent isolator,are combined to enable the optical access at different streamwise locations.The sequential PLS images provide a tomography-like flow visualization,which confirm the existence of streamwise Counter-rotating Vortex Pairs(CVPs)in both external and internal flow field of the inlet.Generation mechanisms of these CVPs are unraveled with the help of a numerical simulation,among which the cowl notch plays an important role in the generation of surface trailing CVPs along the centerline of the cowl.Moreover,the cowl shock sweeps the internal boundary layer towards the body side,which ultimately accumulates low-momentum flow on the body side in forms of a large CVP propagating downstream through the isolator.The CVPs formed in the shape-transition are responsible for the nonuniform flow field of the inward-turning inlet.This study indicates that the V-shaped cowl notch affects the downstream flow significantly and,therefore,should be examined thoroughly in practical applications.展开更多
基金Funded by National Natural Science Foundation of China(No.50572121) Key Pre-research Foundation of Weapon and Equipment(No. 9140A27010206JB35)
文摘In-situ characterization of non-aqueous nano-dispersion systems（NANDS） by freeze-etching transmission electron microscope（FETEM） was reported.To improve just-for-once successive rate of specimen preparation and get good characterization results,an improving specimen preparation method of freezing etching was developed.Size,distribution and morphology of NANDS were directly visualized.Some information of particle dispersion feature and particle density can also be obtained.Reproductivity of the FETEM characterization is excellent.Comparing with laser scattering method,which is liable to give positive error especially for small size particle anchoring disperser,FETEM characterization can give more accurate measurement of particle size.Moreover,FETEM can give dispersion feature of nanoparticle in non-aqueous medium.
基金supported by the National Natural Science Foundation of China(Nos.11772325,11872356 and 11621202)。
文摘The flow field in a typical inward-turning inlet was visualized using the Planar Laser Scattering(PLS)method in a shock tunnel with a nominal Mach number of 6.The opaque inlet,which is truncated at a series of sections,and the following transparent isolator,are combined to enable the optical access at different streamwise locations.The sequential PLS images provide a tomography-like flow visualization,which confirm the existence of streamwise Counter-rotating Vortex Pairs(CVPs)in both external and internal flow field of the inlet.Generation mechanisms of these CVPs are unraveled with the help of a numerical simulation,among which the cowl notch plays an important role in the generation of surface trailing CVPs along the centerline of the cowl.Moreover,the cowl shock sweeps the internal boundary layer towards the body side,which ultimately accumulates low-momentum flow on the body side in forms of a large CVP propagating downstream through the isolator.The CVPs formed in the shape-transition are responsible for the nonuniform flow field of the inward-turning inlet.This study indicates that the V-shaped cowl notch affects the downstream flow significantly and,therefore,should be examined thoroughly in practical applications.
