In this paper, a quaternary system of Mn0.43Ni0.9CuFe0.67O4 negative temperature coefficient (NTC) thermistor ceramic prepared by solid/solid reaction was sintered by microwave and conventional method, respectively....In this paper, a quaternary system of Mn0.43Ni0.9CuFe0.67O4 negative temperature coefficient (NTC) thermistor ceramic prepared by solid/solid reaction was sintered by microwave and conventional method, respectively. To characterize the sinterability of the samples, the densification parameter, porosity and grain size distribution of the bulk were determined. The crystal structure, phase compositions, morphology and impedance of the samples were analyzed by X-ray diffraction (XRD), scanning electron microscopy (SEM), energy-dispersive spectroscopy (EDS) and impedance analysis. The experimental results confirmed that the sinterability and electrical properties of ceramics were homogenously improved by microwave sintering.展开更多
基金financial support from the programs of seed money (No. K08141001)the sci-entific problem tackling (No. G06211002) foundations of Urumqi in China
文摘In this paper, a quaternary system of Mn0.43Ni0.9CuFe0.67O4 negative temperature coefficient (NTC) thermistor ceramic prepared by solid/solid reaction was sintered by microwave and conventional method, respectively. To characterize the sinterability of the samples, the densification parameter, porosity and grain size distribution of the bulk were determined. The crystal structure, phase compositions, morphology and impedance of the samples were analyzed by X-ray diffraction (XRD), scanning electron microscopy (SEM), energy-dispersive spectroscopy (EDS) and impedance analysis. The experimental results confirmed that the sinterability and electrical properties of ceramics were homogenously improved by microwave sintering.