The effect of anisotropy on microstructure and high temperature stress rupture property of Ni3Al base single crystal alloy was investigated. The single crystal specimens were produced by screw selection crystal method...The effect of anisotropy on microstructure and high temperature stress rupture property of Ni3Al base single crystal alloy was investigated. The single crystal specimens were produced by screw selection crystal method. The microstructures were examined by OM, SEM, TEM and X-ray EDS techniques. The stress rupture tests were carried out in air by constant load creep machines under 1 100℃and 130 MPa. The experimental results show that the dendrites preferential orientation deviates certain angles to heat flow orientation, and the secondary arms occur for different crystallographic orientations. The single crystal alloy with different orientations shows obvious anisotropy during tensile stress rupture tests under 1 100℃and 130 MPa. The <111> orientation specimen has the best stress rupture life of 211 h. The high ductility at 1 100℃of the <001> orientation specimen may be attributed to the most multiple equivalent slip systems.展开更多
Active control of turbine blade tip clearance for aircraft engine continues to be a concern in engine opera- tion, because turbine blades are subjected to wear and therefore cause an increasing tip clearance between t...Active control of turbine blade tip clearance for aircraft engine continues to be a concern in engine opera- tion, because turbine blades are subjected to wear and therefore cause an increasing tip clearance between the rotating blades and the shroud and also reduce the engine efficiency. In this work, a Ni-rich Ni3A1 coating with γ＇/γ two-phase microstructure was deposited by electron beam physical vapor deposition （EB-PVD）, which worked as repairing the worn blade tips of single crystal blades. Nb molten pool was used to increase the molten pool tem- perature and thus to enhance the deposition rate. The microstructures and mechanical properties can be modified by the deposition temperatures and the following heat treatments. All coatings consist of γ＇ and γ phases. At deposition temperature of 600 ℃, a dense microstructure can be achieved to produce a coating with grain size of 1 μm and microhardness of -HV 477. After being heated for 4 h at a temperature of 1,100 ℃, the coatings have a more uniform microstructure, and microhardness maintains at a high level of -HV 292. Effect of Hf and Zr on EB-PVD Ni3Al repair coating will be further investigated.展开更多
文摘The effect of anisotropy on microstructure and high temperature stress rupture property of Ni3Al base single crystal alloy was investigated. The single crystal specimens were produced by screw selection crystal method. The microstructures were examined by OM, SEM, TEM and X-ray EDS techniques. The stress rupture tests were carried out in air by constant load creep machines under 1 100℃and 130 MPa. The experimental results show that the dendrites preferential orientation deviates certain angles to heat flow orientation, and the secondary arms occur for different crystallographic orientations. The single crystal alloy with different orientations shows obvious anisotropy during tensile stress rupture tests under 1 100℃and 130 MPa. The <111> orientation specimen has the best stress rupture life of 211 h. The high ductility at 1 100℃of the <001> orientation specimen may be attributed to the most multiple equivalent slip systems.
基金supported by the Postdoctoral Science Foundation of China(No.2013M540037)
文摘Active control of turbine blade tip clearance for aircraft engine continues to be a concern in engine opera- tion, because turbine blades are subjected to wear and therefore cause an increasing tip clearance between the rotating blades and the shroud and also reduce the engine efficiency. In this work, a Ni-rich Ni3A1 coating with γ＇/γ two-phase microstructure was deposited by electron beam physical vapor deposition （EB-PVD）, which worked as repairing the worn blade tips of single crystal blades. Nb molten pool was used to increase the molten pool tem- perature and thus to enhance the deposition rate. The microstructures and mechanical properties can be modified by the deposition temperatures and the following heat treatments. All coatings consist of γ＇ and γ phases. At deposition temperature of 600 ℃, a dense microstructure can be achieved to produce a coating with grain size of 1 μm and microhardness of -HV 477. After being heated for 4 h at a temperature of 1,100 ℃, the coatings have a more uniform microstructure, and microhardness maintains at a high level of -HV 292. Effect of Hf and Zr on EB-PVD Ni3Al repair coating will be further investigated.
